5Cr21Mn9Ni4WNb2N奥氏体耐热钢晶界碳化物

5Cr21Mn_9Ni_4WNb_2N耐热钢锻造后在1200℃以上加热时，NbC聚集成大块，在1200℃以下加热时，NbC薄膜（片）的析出倾向随加热温度降低而增大，1130℃及其以下加热时，粒状和细片状M_(23)C_6随加热温度降低而增多，而且NbC块可作为碳源退化成M_(23)C_6颗粒，过高或过低温度的锻造加热，因晶界NbC块过大或晶界NbC薄膜（片）过多而不利于锻造加工。     

一种Cr—Mn—Mo—B低碳低合金钢的热变形行为

利用ＴＨＥＲＭＣＭＡＳＴＯＲ－Ｚ热处理机对一种Ｃｒ－Ｍｎ－Ｍｏ－Ｂ钢的热变形行为进行了研究，绘制了真应力－应变曲线，得到了各变形工艺参数之间的定量关系，得出试验用钢的Ｑ值为３７３．７ｋｊ／ｍｏｌ。在此基础上给出了试验用钢的动态再结晶图，试验发现，试验用钢９００℃以上变形后，在奥氏体区冷过程中发生静态再结晶与晶粒长大，相变前晶粒尺寸与变形条件Ｚ的关系：ｄｒｅｃ＝２．８８×１０＾４×Ｚ＾－０．２０５。     

Oxidation Behavior of a Single-Crystal Ni-Base Superalloy in Air—II: At 1000, 1100, and 1150°C

The oxidation behavior of a single-crystal (SC) Ni-base superalloy was studied over the temperature range from 1000–1150°C and analysed by TGA, XRD, EDAX, and SEM. The results indicated that the SC Ni-base superalloy exhibited parabolic oxidation kinetics, which were controlled by the growth of the inner -Al₂O₃ layer. A mixed scale formed on the SC Ni-base superalloy after prolonged oxidation. The scale consisted of an outer layer of spinel, a sublayer of mainly -Al₂O₃ with small amount of spinel adjoined by a very thin and even discontinuous layer of CrTaO₄-rich oxide, and an inner -Al₂O₃ layer. The inner -Al₂O₃ layer provided good protection. No internal oxides or nitrides were observed below the inner -Al₂O₃ layer after 1000 hr at 1000°C, and after 200 hr at 1100 and 1150°C.     

新型倾斜板技术制备半固态铝合金坯料和浆料

采用自行设计的波浪型倾斜板,在斜板冷却条件下制备了组织和触变性能优良的半固态合金坯料。而在斜板加热条件下制备出了组织优良的半固态合金浆料。在采用波浪型的倾斜板制备半固态合金过程中,在熔体爆发形核与枝晶破碎的共同作用下,形成了细小球形的半固态合金组织,浇注温度、冷却强度、斜板倾角和斜板表面材质是影响半固态合金组织的主要因素。得出了本试验条件下制备AlMg3合金半固态坯料的浇注温度范围为660~690℃;制备AlSi6Mg2合金半固态坯料的浇注温度范围为660~680℃;制备AlSi6Mg2半固态合金浆料的合理工艺条件为:斜板预热温度为300℃时,合金浇注温度为680℃。     

不同形貌氢氧化镁的化学合成及影响因素

对不同形貌氢氧化镁的化学合成及外部生长环境进行了综述。尤其对影响氢氧化镁结晶性能和形貌起关键作用的因素，如碱性沉淀剂的选择、合成温度的确定、不同镁盐的影响、碱和镁盐的初始浓度及配比、水热处理、反应物的混合方式、晶形控制剂的加入等，进行了详细的阐述。     

Electrooxidation of formic acid on carbon supported PtxPd1−x (x = 0-1) nanocatalysts

In this work, carbon supported Pt_xPd_1−x (x = 0-1) nanocatalysts were investigated for formic acid oxidation. These catalysts were synthesized by a surfactant-stabilized method with 3-(N,N-dimethyldodecylammonio) propanesulfonate (SB12) as the stabilizer. They show better Pt/Pd dispersion and higher catalytic performance than the corresponding commercial catalysts. Furthermore, the electrocatalytic properties of Pt_xPd_1−x/C were found to depend strongly on the Pt/Pd deposition sequence and on the Pt/Pd atomic ratio. At a lower potential, formic acid oxidation current on co-deposited Pt_xPd_1−x/C catalysts increase with increasing Pd surface concentration. Nanoscale Pd/C is a promising formic acid oxidation catalyst candidate for the direct formic acid fuel cell.     

Irganox(R) HP-136的抗氧化机理及对聚丙烯加工稳定性的影响

介绍了Irganox(R) HP-136在PP加工中的作用,表明它能有效地捕获烷基自由基,与传统的受阻酚类及亚磷酸酯类抗氧剂复配与传统的二元抗氧稳定体系相比,具有添加量少、抗氧性能优等优点.比较了Irganox(R) HP-136(3-芳基-苯并呋喃酮)与传统抗氧剂的抗氧机理,并分析了在聚合物稳定体系中的作用.     

A 3D analysis of the joint torques developed during driver's ingress–egress motion

Providing an easy ingress–egress (I/E) movement remains a challenge for car designers. I/E has been largely studied in kinematics, but not in dynamics. This study proposes: (1) to evaluate and describe the motor torques developed in the lower limbs and lumbar joints during I/E motions and (2) to analyse the influence of the car geometry and subject anthropometry. An experiment was performed to observe 15 subjects of three anthropometrical groups getting in and out of a car mock-up simulating three different vehicle configurations. Motor torques were extracted using an inverse dynamics analysis. Both ingress and egress motions were primarily characterised by large torques. Overall, the taller a subject and the lower the seat of the vehicle were, the larger the peak torques were. Moreover, peak torques were higher for egress than ingress. These results are discussed in regard to the current knowledge on I/E ergonomics.     

压力流化床燃烧煤水混合燃料泵送给料技术在国外的研究进展

压力流化床燃烧技术近二十年来在世界上得到很大发展。煤的湿法给料系统具有比干法输送系统更简单，运行调节更可靠等优点。煤水混合物可泵送的水分在２５％左右，煤的粒度一般为０～６ｍｍ，表现为非牛顿的假塑性流体特性，通过级配来达到一定的稳定性和良好输送性能，且流动阻力低，不用添加剂即可实现泵送，它的应用使压力流化床的燃烧制备和输送系统成本大大降低。     

聚乙二醇-400催化合成橙花醚的研究

研究了利用多种相转移催化剂在不同条件下合成橙花醚。结果表明：采用聚乙二醇 ４００（ＰＥＧ ４００）为催化剂，当β 萘酚：溴乙烷：催化剂＝１：１２：００７（摩尔比）、温度为７６℃、反应７ｈ时，产率可高达９８１％。