In this article, a laser partially textured thrust bearing is theoretically and experimentally analyzed. An adiabatic model is developed in order to theoretically investigate the performances of the bearing. The bearing sample is partially textured both in radial and circumferential direction using the laser texturing process. The performance of the bearing (fluid film thickness and friction torque) is evaluated on a specially adapted test rig and the experimental results are compared with the theoretical model. A good agreement is found between the theoretical model and the experimental data. Also a comparison between a laser textured bearing and a bearing textured using the photolithographic method is presented. 相似文献
Diesel particulate filters (DPF) are indispensable parts of modern automotive exhaust gas aftertreatment systems due to the stringent emissions legislation. For a fuel-efficient control strategy, it would be beneficial to determine directly and in-operation their actual trapped soot mass. Two novel approaches—based on the electrical conductivity of trapped soot particles—emerged recently. By measuring the electrical resistance between different single walls inside the filter, the soot load is determined with local resolution. The microwave-based technique is a contactless approach that gives an integral value depending on the soot mass in the DPF. We present investigations on loading and regeneration of DPFs in a dynamometer test bench applying both methods. The results are compared with each other and correlated with the differential pressure and the soot mass. Especially the microwave-based technique has a potential for serial application. 相似文献
In this microwave study, the defect chemistry of ceria–zirconia solid solutions (CZO, Ce1−yZryO2−δ) was investigated at high temperatures by a resonant microwave method. Specifically, the effects of temperature and Zr content on the dielectric properties and defect chemistry mechanisms in CZO were analyzed. Experiments were performed on a series of different CZO powders (y = 0.2, 0.33, 0.50, 0.67). Measurements at 600°C and different oxygen partial pressures (pO2 = 10−26–0.2 bar) confirm a dominant n-type conduction of small-polarons in CZO due to the preferred formation of oxygen vacancies, which is also supported by a multimodal analysis. Polarization losses were found to be negligible in the GHz range. Furthermore, an increased relative permittivity was observed in CZO, which correlates with the concentration of oxygen vacancies in CZO. Our microwave study is the first to provide a comprehensive data set for the dielectric properties of CZO powder sample in a wide range of different conditions. In addition, the connection of dielectric properties to CZO defect chemistry mechanisms is presented. The results are in good agreement with findings in the literature and may contribute to a better understanding of microwave-based state diagnosis of CZO-based materials, as it discussed for three-way catalysts. 相似文献
Quantification of microvessels in tumors is mostly based on counts of vessel profiles in tumor hot spots. Drawbacks of this method include low reproducibility and large interobserver variance, mainly as a result of individual differences in sampling of image fields for analysis. Our aim was to test an unbiased method for quantifying microvessels in healthy and tumorous lymph nodes of dogs. The endothelium of blood vessels was detected in paraffin sections by a combination of immunohistochemistry (von Willebrand factor) and lectin histochemistry (wheat germ agglutinin) in comparison with detection of basal laminae by laminin immunohistochemistry or silver impregnation. Systematic uniform random sampling of 50 image fields was performed during photo-documentation. An unbiased counting frame (area 113,600 microm(2)) was applied to each micrograph. The total area sampled from each node was 5.68 mm(2). Vessel profiles were counted according to stereological counting rules. Inter- and intraobserver variabilities were tested. The application of systematic uniform random sampling was compared with the counting of vessel profiles in hot spots. The unbiased estimate of the number of vessel profiles per unit area ranged from 100.5 +/- 44.0/mm(2) to 442.6 +/- 102.5/mm(2) in contrast to 264 +/- 72.2/mm(2) to 771.0 +/- 108.2/mm(2) in hot spots. The advantage of using systematic uniform random sampling is its reproducibility, with reasonable interobserver and low intraobserver variance. This method also allows for the possibility of using archival material, because staining quality is not limiting as it is for image analysis, and artifacts can easily be excluded. However, this method is comparatively time-consuming. 相似文献
Summary: Hydrotalcite‐catalyzed polycondensation of BHET was studied by thermogravimetry to elucidate the kinetics. The reaction was found to follow second‐order kinetics with respect to hydroxyl end groups. The overall activation energy of the polycondensation was found to decrease with increasing catalyst concentration before it leveled out to the value of 93 kJ · mol−1 at high catalyst concentration. This is a result of the uncatalyzed reaction that takes place parallel to the catalyzed one. The activation energy of the uncatalyzed path was found to be 156 kJ · mol−1. IR spectroscopy and XRD showed that the monomer intercalates between the layers of hydrotalcite at the beginning of the reaction enabling the complexation of oxygen‐containing functional groups with the hydroxide groups of the catalyst. Based on these findings a polycondensation mechanism is proposed. One end group of the monomer is activated in the form of alkoxide that counterbalances the positive charge of the hydrotalcite layer. This alkoxide group attacks an ester carbonyl group fixed close to it, generating a new ester bond and a glycoxide species. The role of hydrotalcite is to activate the reactants, rendering the attacking hydroxyl group more nucleophilic and the ester carbonyl group more electrophilic, and at the same time fixing the reactant together in a favorable geometry.
Intercalation of BHET in the gallery of HT layers in a twisted alkoxide form. 相似文献
An Optoanalytic Method for the Determination of the Distribution and Orientation of Fibres in Steel Fibre Reinforced UHPC Micro steel fibres were often used to improve the ductility as well as to increase the tensile and bending strength of ultra high performance concrete (UHPC). The knowledge about the distribution and orientation of fibres is important to predict the load capacity of structures made of fibre reinforced UHPC. It is also relevant from economic and ecological point of view. Due to the multiplicity of influences, such as geometry, concrete properties and manufacture technology, it is necessary to investigate the distribution and orientation of fibres for individual application. At Leipzig University a practicable method was developed to determine the distribution and orientation of micro steel fibres in UHPC. 相似文献
It is my purpose in this editorial to offer some highly personal and likely controversial views on the state of statistics and the quality profession. These views are based on my personal experiences and prejudices-especially those of my 10 years as an independent statistical consultant. I wish to particularly absolve my current employer, Merck and Company, and my colleagues there of any guilt by association. The opinions rendered here are entirely my own and in no way represent Merck's practices or policies, Mea culpa. 相似文献
Scale-up of Distillation Columns. In spite of remarkable advances in the development of computer programs for calculations on distillation columns, it is frequently still impossible to design them without experimental testing. Economic constraints demand use of miniaturised test plant, thus enhancing the importance of laboratory measurements. A system is presented for scale-up of separation which required information from laboratory experiments, includes data from reference columns, and takes account of models of fluid dynamics and mass transfer. The special feature of this approach lies in the free choise of internals, both in the laboratory and in the designed column. 相似文献
The intermolecular bonding energies of polymeric materials can be employed in the evaluation of sliding under conditions determined predominantly by adhesion. The effect at the interface of these energies can be evaluated by reference to the surface energy and to its polar and dispersion-related components. Wetting angle measurements were used to determine the work of adhesion for a group of polymer-polymer material combinations. An exponential relationship exists between the work of adhesion and the coefficients of friction of these combinations, these coefficients of friction being determined primarily by adhesion. 相似文献