浅谈电力行业金属监督质量管理的优化

如何通过金属监督质量管理的优化创新来更好地服务当前电力设备材料等级越来越高的需求,已经成为目前电力行业内金属监督质量管理工作面临的一项挑战性课题。文章主要分析了现阶段电力行业金属监督质量管理工作中普遍存在的问题、不足和难点,并明确金属监督质量管理工作的基本要求,最后提出了金属监督质量管理工作优化的相关措施,对电力行业金属监督质量管理工作提供有助益的参考。     

磁控溅射氧化钒薄膜的研究进展

氧化钒因其优秀的相变特性和电阻开关特性而广受关注,在氧化钒薄膜多种制备工艺中,磁控溅射法优势明显。本文总结了近年来国内外研究者对磁控溅射法制备氧化钒薄膜的基础工艺研究成果,概述了不同溅射工艺对二氧化钒薄膜结晶特性及光学、电学性能的影响,并对相关机理进行了简要分析。相关结论对氧化钒薄膜的性能提高和应用扩展有一定的指导意义。     

Crystal plane evolution of grain oriented alumina ceramics with high transparency

Transparent alumina ceramics with oriented grains were successfully prepared by slip casting under an assisted magnetic field and sintering at 1850 °C for 5 h in vacuum. In-line transmittance of the alumina ceramic shaped under 12 T reaches as high as 70.3% at 600 nm. Detailed crystal plane evolution of grain oriented alumina ceramics with the assistance of different magnitude magnetic field was studied by XRD characterization. The results indicate that complete textured structure could only be realized with a magnetic field strength above 12 T. Furthermore, the grain microstructure was observed by optical microscope in different directions.     

Al2O3对电子玻璃高温黏度及析晶性能的影响

研究了不同含量的Al2O3对电子玻璃高温黏度和析晶性能的影响。结果表明,随着氧化铝含量的增加,电子玻璃的高温黏度、成型温度均降低,但析晶黏度减小,与成型的砖尖黏度差值减小,不利于溢流下拉成型。     

Enhanced light emission of GaN-based diodes with a NiO(x)/graphene hybrid electrode

A NiO(x) buffer layer is introduced in GaN-based light-emitting diodes to form low resistance ohmic contacts between p-type GaN and graphene conductive electrodes, leading to improved performance with lower operating voltage and higher light output power.     

Preparation of tunable full-color emission carbon dots and their optical applications in ions detection and bio-imaging

In this work, we synthesized a series of novel carbon dots (CDs) by using phenylenediamines (three isomers: o-phenylenediamine, m-phenylenediamine, and p-phenylenediamine) as starting materials via facile solvothermal approach. As-prepared CDs could emit bright blue, green, yellow, orange, and red light with relatively high PLQY, individually. Optical properties could be controlled by simply varying reaction parameters. The luminescent mechanism was investigated and analyzed in detail. Finally, the blue-emitting CDs and green-emitting CDs showed many appealing properties, such as high sensitivity (limit of detection = 4.52 and 3.50 nmol/L), quick response (<2 minutes), broad response window (0-70 nmol/L), and excellent selectivity for detecting Cr⁶⁺ and Al³⁺ cations, respectively. Thus, they have potential to be developed as the corresponding optical probes. While as-prepared orange-emitting CDs could be applied as a bio-imaging reagent due to its long-wavelength emission, relatively high PLQY, low toxicity, excellent water solubility, and good biocompatibility.     

整体式转向梯形机构的优化设计

引入影响汽车行驶转向性能的轮胎侧偏、悬架侧倾和,前轮定位等主要因素,建立了汽车整体式转向梯形机构的优化数学模型,从四个方面对梯形机构进行优化设计。通过对这些结果的分析对比,得出了具有实用价值的结论。     

Highly transparent yttria ceramics with Nb2O5/Ta2O5 as novel sintering additives by pressureless vacuum sintering

Highly transparent yttria ceramics were fabricated by pressureless sintering with Nb₂O₅ or Ta₂O₅ as a novel sintering additive. The optical transmittance, microstructural evolution, and thermo-mechanical properties of the samples were investigated. The optimal doping concentrations of Nb₂O₅ and Ta₂O₅ are 0.3 and 0.2 at.%, respectively, which are much lower compared to those of previously reported counterparts. The transmittance of the sample with 0.3 at.% Nb₂O₅ reaches 81.6% at 1100 nm and 72.4% at 400 nm (2 mm in thickness), similar transmittance was obtained in the sample with 0.2 at.% Ta₂O₅. The microhardness (∼7 GPa), fracture toughness (∼0.85 MPa·m^1/2), and biaxial strength (∼200 MPa) of the present samples were confirmed to be comparable or even better compared to those of previously reported transparent yttria ceramics fabricated by pressureless sintering. Furthermore, the present samples, by virtue of the low doping concentrations, possessed relatively high thermal conductivity values (>10 W/m·K), which substantially guaranteed high thermal shock resistance.     

Fabrication of Transparent Dysprosium Aluminum Garnet (Dy3Al5O12) Ceramics via a Solid‐State Reaction Method

Polycrystalline, transparent Dy₃Al₅O₁₂ ceramics were firstly fabricated by a solid‐state reaction method using high‐purity Dy₂O₃ and Al₂O₃ powders. The fully dense Dy₃Al₅O₁₂ ceramic with an average grain size of less than 10 μm was obtained by vacuum sintering at 1820°C for 6 h. The in‐line transmittance of the optimized sample reaches 80% in the visible region. Scanning electron microscopy reveals that no secondary phases and almost no pores are observed at grain boundaries or triple junctions, and the fracture mode of the ceramic is mainly transgranular. The Dy₃Al₅O₁₂ ceramic is promising for magneto‐optical applications. Verdet constant of the Dy₃Al₅O₁₂ transparent ceramic is as high as ?0.41 min·(Oe·cm)^?1.