N,N''-取代邻苯二胺的合成

通过2-取代苯并咪唑盐的还原开环反应制备了8个N,N′-不同取代的邻苯二胺,并经1HNMR、IR、MS及元素分析表征,其中5个未见文献报道.这是一条由邻苯二胺和羧酸经2.取代苯并咪唑制取该类化合物的简洁合成路线.     

一次盐水设备运行总结

介绍了内蒙古海吉氯碱化工股份有限公司6万t/a离子膜烧碱装置一次盐水设备的运行情况和运行过程中存在的问题及相应的技改措施.     

一个用户接口管理系统

本文介绍了一个用户接口管理系统NUUIMS的设计和实现.重点叙述了该系统基于规范化目标用户接口模型的设计思想,系统组成及描述方法.文章也讨论了使用NUUIMS设计而成的用户接口的特点.     

基于ARIMA和支撑矢量机组合预测的惯性器件故障预报

文中提出一种基于ARIMA和支撑矢量机进行组合预测的方法,该方法综合运用ARIMA良好的线性拟合能力和支撑矢量机强大的非线性映射功能,将两种预测模型有机地组合在一起,综合各自优点,以期有效改善模型的拟合能力,获得最优预测效果.文中将该方法应用于某飞行器惯性器件的故障预报当中并进行了仿真实验.结果表明,这种方法相对于单项模型的预测具有更高的精度,对于复杂时间序列的分析和预测有很好的应用价值,在故障预报中具有广泛的应用前景.     

中国铜冶炼企业的竞争趋势及对策建议

文章分析了我国大型及中小型铜冶炼企业所面临竞争环境,提出了我国铜冶炼企业应采取的对策建议,即:联合进口原料;走大型企业联合之路,组建中国铜业集团;开发利用海外资源;加大国内资源勘探;继续进行技改、挖潜,提高企业竞争力等。     

Preparation and photochromism of nanocomposite thin film based on polyoxometalate and polyethyleneglycol

A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism.     

FeBP非晶态合金超细微粒的合成及其对PH3分解的催化作用

用化学还原法合成了FeBP非晶态合金超细微粒，用电感耦合等离子体光谱（ICP）、X射线粉末衍射（XRD）、透射电子显微镜（TEM）和差热分析（DSC）等手段对其进行了物性表征，并用微型催化反应装置考察了其对PH3分解的催化作用，结果表明，非晶态合金FeBP对PH3的分解具有良好的催化作用，能使PH3的分解温度从800℃以上降到500℃左右。490℃时分解率超过90％，540℃时达100％。     

基于μCLinux的NAT设备的设计与开发

NAT(网络地址翻译)技术有效地解决了IP地址紧缺的问题,为实现IPv4到IPv6的平滑过渡发挥了巨大的作用.在一个体积小、重量轻、价格低廉的嵌入式平台上实现NAT设备具有很好的实际意义.文中介绍了NAT技术的原理和实现过程,在自行设计的ARM7嵌入式硬件平台上基于μCLinux操作系统实现了NAT的功能,并通过实现其他相关功能,构建了完整的NAT设备,完成了小型网络接入Internet的方案.     

Tile-boundary artifact reduction using odd tile size and the low-pass first convention.

It is well known that tile-boundary artifacts occur in wavelet-based lossy image coding. However, until now, their cause has not been understood well. In this paper, we show that boundary artifacts are an inescapable consequence of the usual methods used to choose tile size and the type of symmetric extension employed in a wavelet-based image decomposition system. This paper presents a novel method for reducing these tile-boundary artifacts. The method employs odd tile sizes (2N + 1 samples) rather than the conventional even tile sizes (2N samples). It is shown that, for the same bit rate, an image compressed using an odd tile length low-pass first (OTLPF) convention has significantly less boundary artifacts than an image compressed using even tile sizes. The OTLPF convention can also be incorporated into the JPEG 2000 image compression algorithm using extensions defined in Part 2 of this standard.