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101.
A positive‐working, aqueous‐base‐developable photosensitive polyimide precursor based on poly(amic ester)‐bearing phenolic hydroxyl groups and a diazonaphthoquinone photosensitive compound was developed. The poly(amic ester) was prepared from a direct polymerization of 2,2′‐bis‐(3‐amino‐4‐hydroxyphenyl)hexafluoropropane and bis(n‐butyl)ester of pyromellitic acid in the presence of phenylphosphonic dichloride as an activator. Subsequently, the thermal imidization of the poly(amic ester) precursor at 300°C produced the corresponding polyimide. The inherent viscosity of the precursor polymer was 0.23 dL/g. The cyclized polyimide showed a glass‐transition temperature at 356°C and a 5% weight loss at 474°C in nitrogen. The structures of the precursor polymer and the fully cyclized polymer were characterized by Fourier transform infrared spectroscopy and 1H‐NMR. The photosensitive polyimide precursor containing 25 wt % diazonaphthoquinone photoactive compound showed a sensitivity of 150 mJ/cm2 and a contrast of 1.65 in a 3 μm film with 1.25 wt % tetramethylammonium hydroxide developer. A pattern with a resolution of 10 μm was obtained from this composition. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 352–358, 2002 相似文献
102.
A thermally labile polymer, poly(propylene glycol), was modified to obtain PPG having an amino end group. PPG was incorporated into a partially aliphatic polyimide based on an alicyclic dianhydride, and this afforded triblock copolymers containing various amounts of PPG blocks. The thermal properties of the copolymers were investigated by thermogravimetric analysis and differential scanning calorimetry. The thermal decomposition of the PPG block in the copolymers was carried out at 240°C under various pressures to obtain porous polyimide films. The pores remained during the thermolysis under a reduced pressure of 710 mmHg, whereas they collapsed under (near) atmospheric pressure. The pore size increased as the amount of the PPG block in the copolymers increased. The dielectric constants of the porous polyimides varied from 2.60 to 2.42 with the original copolymer composition. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 532–538, 2006 相似文献
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Intelligent Service Robotics - 相似文献
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Chan-Ik?Park Han-Cheol?ChoeEmail author Chae-Heon?Chung 《Metals and Materials International》2004,10(6):549-553
Regardless of the type of performed restoration, in most cases, a screw connection is employed between the abutment and implant.
For this reason, implant screw loosening has remained a problem in restorative practices. The purpose of this study was to
compare the surface of coated/plated screws with titanium and gold alloy screws and to evaluate the physical properties of
coated/plated material after scratch tests via FE-SEM (field emission scanning electron microscopy) investigation. GoldTite,
titanium screws provided by 3i (Implant Innovation, USA) and TorqTite, titanium screws by Steri-Oss (Nobel Biocare, USA) and
gold screws and titanium screws by AVANA (Osstem Implant, Korea) were selected for this study. The surface, crest, and root
of the abutment screws were observed by FE-SEM. A micro-diamond needle was also prepared for the scratch test. Each abutment
screw was fixed, and a scratch on the surface of the head region was made at constant load and thereafter the fine trace was
observed with FE-SEM. The surface of GoldTite was smoother than that of other screws and it also had abundant ductility and
malleability compared with titanium and gold screws. The scratch tests also revealed that teflon particles were exfoliated
easily in the screw coated with teflon. The titanium screw had rough surface and low ductility. The clinical use of gold-plated
screws is recommended as a means of preventing screw loosening. 相似文献
106.
Tae-Sik Kim Young-Je An Kwang Ho Kim Won-Sub Chung Young-Rae Cho 《Metals and Materials International》2006,12(4):339-343
The effect of the dielectric constant (k) of bonding materials in a screen-printed carbon nanotube (CNT) cathode on the field
enhancement factor was investigated for high-efficiency CNT cathodes using the ANSYS software. The values obtained by a simulation
study were compared to the experimental results obtained for screen-printed CNT cathodes. The field enhancement factor increased
as the dielectric constant decreased, reaching a maximum value at a dielectric constant of 1, the value for a vacuum. The
findings indicate that the larger sheet resistance of the bonding materials, after the firing process, can be attributed to
the larger emission current of the CNT cathode. From these results, it was concluded that the best bonding materials for screen-printed
CNT cathodes should have a low dielectric constant and a high sheet resistance. This finding can be used as criteria for selecting
bonding materials for use in CNT pastes for highly efficient CNT cathodes. 相似文献
107.
Biing Hwa Yan Hsien Chung Tsai Fuang Yuan Huang Long Chorng Lee 《International Journal of Machine Tools and Manufacture》2005,45(3):251-259
Alumina particle reinforced 6061 aluminum matrix composites (Al2O3p/6061Al) have excellent physical and chemical properties than those of a traditional metal; however, their poor machinability lead to worse surface quality and serious cutting tool wear. In this study, wire electrical discharge machining (WEDM) is adopted in machining Al2O3p/6061Al composite. In the experiments, machining parameters of pulse-on time were changed to explore their effects on machining performance, including the cutting speed, the width of slit and surface roughness. Moreover, the wire electrode is easily broken during the machining Al2O3p/6061Al composite, so this work comprehensively investigates into the locations of the broken wire and the reason of wire breaking.The experimental results indicate that the cutting speed (material removal rate), the surface roughness and the width of the slit of cutting test material significantly depend on volume fraction of reinforcement (Al2O3 particles). Furthermore, bands on the machined surface for cutting 20 vol.% Al2O3p/6061Al composite are easily formed, basically due to some embedded reinforcing Al2O3 particles on the surface of 6061 aluminum matrix, interrupt the machining process. Test results reveal that in machining Al2O3p/6061Al composites a very low wire tension, a high flushing rate and a high wire speed are required to prevent wire breakage; an appropriate servo voltage, a short pulse-on time, and a short pulse-off time, which are normally associated with a high cutting speed, have little effect on the surface roughness. 相似文献
108.
Travel patterns have gradually changed from group travel to individual travel. An increasing number of people acquire travel information through various types of media. One of the alternative information sources is social media, which enables users to exchange information among members. However, one of the characteristics of social media is information sharing, not information search, which involves both giving (i.e. posting) and taking (i.e. selective reading, forwarding, replying, linking, and liking) information. Compared to the ‘giving’ side of information-sharing research, less effort has been spent on the ‘taking’ side of information research. Therefore, we investigate travel information adoption in social media as well as how individuals communicate with each other. We use the elaboration likelihood model, which measures the impact of central (e.g. argument quality) and peripheral (e.g. credibility) cues on traveller information-sharing behaviour corresponding with social presence on social media. The results of an empirical analysis of 527 respondents, who were experienced in travel information adoption via social media, were examined. Our findings revealed that argument quality had a positive effect on perceived usefulness and source credibility positively affected perceived usefulness and social relationships. Perceived usefulness had a significant positive effect on social relationships. Both perceived usefulness and social relationships affected travel information adoption. Lastly, the levels of argument quality and source credibility perceived by social media members were found to differ according to the level of social presence. 相似文献
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