Phosphorus‐containing polyaryloxydiphenylsilanes with high flame retardance arising from a phosphorus–silicon synergistic effect

Polyaryloxydiphenylsilanes were prepared from phosphorus‐containing diols and diphenydichlorolsilane through solution polymerization. With a stoichiometric imbalance in feed monomers, the resulting polymers exhibited moderate melting points and good processing properties. The polymers prepared showed initial decomposition temperatures above 340 °C, excellent thermal stability, high char yields at 850 °C and very high limited oxygen index values of 56–59. The polymers' char yields and their (P + Si) contents showed linear relationships. © 2003 Society of Chemical Industry     

移动运营商手机游戏业务的战略定位和发展策略探讨

分析了韩国、日本及国内运营商手机游戏业务的发展状况．探讨了手机游戏业务的模式．论述了该业务的战略定位和市场前景。从地区提供给移动通信市场对外部环境、产业链的准备是否充分以及运营商内部的资源和运营状况等三个方面阐明了手机游戏业务发展的关键因素。     

Combining ideal beamforming and Alamouti space-time block codes

The simplest Alamouti space-time block code is coupled with a larger number of transmit antennas via ideal beamforming to achieve higher diversity gain. It is shown that the combined system can remain both full diversity and full code rate without orthogonality loss. Simulation results show a significant performance gain over the conventional space-time block codes.     

节水灌溉实施办法探讨

从我国实际情况出发,探讨了节水灌溉及其技术体系的建立、节水模式的选择和相应的对策措施。     

加强安全监督管理 保障检修施工安全

通过严格外来施工队伍和人员的安全管理,加强直接作业票证的管理,落实监护人职责,开展项目危险性分析,强化现场监督等手段,从而加强了检修现场的安全管理,保证系统停车检修的圆满完成。     

Reliability investigation of 0.07-/spl mu/m InGaAs-InAlAs-InP HEMT MMICs with pseudomorphic In/sub 0.75/Ga/sub 0.25/As channel

The authors have investigated the reliability performance of G-band (183 GHz) monolithic microwave integrated circuit (MMIC) amplifiers fabricated using 0.07-/spl mu/m T-gate InGaAs-InAlAs-InP HEMTs with pseudomorphic In/sub 0.75/Ga/sub 0.25/As channel on 3-in wafers. Life test was performed at two temperatures (T/sub 1/ = 200 /spl deg/C and T/sub 2/ = 215 /spl deg/C), and the amplifiers were stressed at V/sub ds/ of 1 V and I/sub ds/ of 250 mA/mm in a N/sub 2/ ambient. The activation energy is as high as 1.7 eV, achieving a projected median-time-to-failure (MTTF) /spl ap/ 2 /spl times/ 10/sup 6/ h at a junction temperature of 125 /spl deg/C. MTTF was determined by 2-temperature constant current stress using /spl Delta/G/sub mp/ = -20% as the failure criteria. The difference of reliability performance between 0.07-/spl mu/m InGaAs-InAlAs-InP HEMT MMICs with pseudomorphic In/sub 0.75/Ga/sub 0.25/As channel and 0.1-/spl mu/m InGaAs-InAlAs-InP HEMT MMICs with In/sub 0.6/Ga/sub 0.4/As channel is also discussed. The achieved high-reliability result demonstrates a robust 0.07-/spl mu/m pseudomorphic InGaAs-InAlAs-InP HEMT MMICs production technology for G-band applications.     

Image registration by "Super-curves"

We solve the 2-D affine image registration problem by curve matching and alignment. Our approach starts with a super-curve, which is formed by superimposing two affine related curves in one coordinate system. We use B-spline fusion technique to find a single B-spline approximation of the super-curve and a registration between the two curves simultaneously. This approach achieves superior accuracy and efficiency in curve matching and alignment. We then address the occlusion problem by finding partial match between the curves segmented using inflections and cusps, which are affine invariant. The combination of edge detection and curve alignment lead to accurate image registration.     

SO2-4/ZrO2-SiO2的制备及其催化合成丁酸丁酯

采用分别沉淀/混合沉淀法、改性共沉淀法和以硅溶胶为硅源的共沉淀法制备了SO2-4/ZrO2-SiO2固体超强酸催化剂;考察了沉淀剂及沉淀终点的pH等制备条件对分别沉淀/混合沉淀法制备的SO2-4/ZrO2-SiO2催化剂催化合成丁酸丁酯活性的影响;探索了ZrO2-SiO2的制备方法、反应时间对SO2-4/ZrO2-SiO2催化剂活性的影响.实验结果表明,以硝酸铵为沉淀剂,当沉淀终点的pH为7～8时,采用分别沉淀/混合沉淀法制备的SO2-4/ZrO2-SiO2催化剂的活性较高(酯化率88.7%),但分别沉淀/混合沉淀法制备的ZrO2-SiO2组成不均匀;以硅溶胶为硅源采用共沉淀法制备的SO2-4/ZrO2-SiO2催化剂催化合成丁酸丁酯,在正丁醇0.48 mol、正丁酸0.40 mol、反应时间3 h、不添加任何带水剂的条件下,酯化率高达96.4%,该方法制备的催化剂稳定性和再生性能好,制备成本低.     

Bandpass filters with reconfigurable transmission zeros using varactor-tuned tapped stubs

In this letter, bandpass filters with one or two tunable transmission zeros are proposed. The reconfigurable transmission zeros are implemented through varactors in combination with tapped quarter-wavelength stubs. Based on mixed mode simulations including EM simulation and circuit simulation, the proposed filters were designed and fabricated on low-cost FR4 board. The measurement results verified the design concepts.     

燕皮传统加工工艺中碱液对肉糜特性的影响

燕皮是以猪肉和甘薯粉为原料,手工制成的薄如纸且经煮不烂的传统食品。在传统制作燕皮过程中添加山榉灰配制的碱液是影响肉糜品质的关键步骤。通过测定制作燕皮过程中各工序样品的氮溶解指数、持水性、乳化稳定性、pH值和粘度,利用SDS-PAGE分析样品中的蛋白质组分、利用光学显微镜观察它们的结构变化,证实植物碱液能够提高样品的氮溶解指数、持水性和乳化稳定性并且延迟了肉糜硬化。同时实验证明碳酸碱(Na2CO3或K2CO3)可替代传统工艺中的植物碱,为后续标准化、工业化生产提供可行条件。