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101.
A Novel and Facile Route to Synthesize Atomic‐Layered MoS2 Film for Large‐Area Electronics
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Stephen Boandoh Soo Ho Choi Ji‐Hoon Park So Young Park Seungho Bang Mun Seok Jeong Joo Song Lee Hyeong Jin Kim Woochul Yang Jae‐Young Choi Soo Min Kim Ki Kang Kim 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(39)
High‐quality and large‐area molybdenum disulfide (MoS2) thin film is highly desirable for applications in large‐area electronics. However, there remains a challenge in attaining MoS2 film of reasonable crystallinity due to the absence of appropriate choice and control of precursors, as well as choice of suitable growth substrates. Herein, a novel and facile route is reported for synthesizing few‐layered MoS2 film with new precursors via chemical vapor deposition. Prior to growth, an aqueous solution of sodium molybdate as the molybdenum precursor is spun onto the growth substrate and dimethyl disulfide as the liquid sulfur precursor is supplied with a bubbling system during growth. To supplement the limiting effect of Mo (sodium molybdate), a supplementary Mo is supplied by dissolving molybdenum hexacarbonyl (Mo(CO)6) in the liquid sulfur precursor delivered by the bubbler. By precisely controlling the amounts of precursors and hydrogen flow, full coverage of MoS2 film is readily achievable in 20 min. Large‐area MoS2 field effect transistors (FETs) fabricated with a conventional photolithography have a carrier mobility as high as 18.9 cm2 V?1 s?1, which is the highest reported for bottom‐gated MoS2‐FETs fabricated via photolithography with an on/off ratio of ≈105 at room temperature. 相似文献
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Kyung Seob Lim Jun-Kyu Park Myung Ho Jeong Jae-Woon Nah Dae Sung Park Jong Min Kim Jung Ha Kim So Youn Lee Eun Jae Jang Suyoung Jang Hyun Kuk Kim Doo Sun Sim Keun-Ho Park Young Joon Hong Youngkeun Ahn Jung Chaee Kang 《Journal of materials science. Materials in medicine》2016,27(4):66
The aim of this study was to evaluate antiproliferative sirolimus- and antioxidative alpha-lipoic acid (ALA)-eluting stents using biodegradable polymer [poly-l-lactic acid (PLA)] in a porcine coronary overstretch restenosis model. Forty coronary arteries of 20 pigs were randomized into four groups in which the coronary arteries had a bare metal stent (BMS, n = 10), ALA-eluting stent with PLA (AES, n = 10), sirolimus-eluting stent with PLA (SES, n = 10), or sirolimus- and ALA-eluting stent with PLA (SAS, n = 10). A histopathological analysis was performed 28 days after the stenting. The ALA and sirolimus released slowly over 30 days. There were no significant differences between groups in the injury or inflammation score; however, there were significant differences in the percent area of stenosis (56.2 ± 11.78 % in BMS vs. 51.5 ± 12.20 % in AES vs. 34.7 ± 7.23 % in SES vs. 28.7 ± 7.30 % in SAS, P < 0.0001) and fibrin score [1.0 (range 1.0–1.0) in BMS vs. 1.0 (range 1.0–1.0) in AES vs. 2.0 (range 2.0–2.0) in SES vs. 2.0 (range 2.0–2.0) in SAS, P < 0.0001] between the four groups. The percent area of stenosis based on micro-computed tomography corresponded with the restenosis rates based on histopathological stenosis in different proportions in the four groups (54.8 ± 7.88 % in BMS vs. 50.4 ± 14.87 % in AES vs. 34.5 ± 7.22 % in SES vs. 28.9 ± 7.22 % in SAS, P < 0.05). SAS showed a better neointimal inhibitory effect than BMS, AES, and SES at 1 month after stenting in a porcine coronary restenosis model. Therefore, SAS with PLA can be a useful drug combination for coronary stent coating to suppress neointimal hyperplasia. 相似文献
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Kim Kihyeun Son Myungwoo Pak Yusin Chee Sang-Soo Auxilia Francis Malar Lee Byung-Kee Lee Sungeun Kang Sun Kil Lee Chaedeok Lee Jeong Soo Kim Ki Kang Jang Yun Hee Lee Byoung Hun Jung Gun-Young Ham Moon-Ho 《Nano Research》2018,11(7):3957-3957
Nano Research - The order of the authors in the original version of this article was unfortunately incorrect on the first page and the first page of the ESM. Instead of Myungwoo Son1, Yusin Pak1,... 相似文献
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Kien Tiek Wong Boris Brigljević Jeong Hyeon Lee So Yeon Yoon Seok Byum Jang Choe Earn Choong Inwook Nah Hyeongjun Kim Hyun-Seog Roh Sang Kyu Kwak Hankwon Lim Min Jang 《Small (Weinheim an der Bergstrasse, Germany)》2023,19(1):2204336
This study focuses on the applicability of single-atom Mo-doped graphitic carbon nitride (GCN) nanosheets which are specifically engineered with high surface area (exfoliated GCN), NH2 rich edges, and maximum utilization of isolated atomic Mo for propylene carbonate (PC) production through CO2 cycloaddition of propylene oxide (PO). Various operational parameters are optimized, for example, temperature (130 °C), pressure (20 bar), catalyst (Mo2GCN), and catalyst mass (0.1 g). Under optimal conditions, 2% Mo-doped GCN (Mo2GCN) has the highest catalytic performance, especially the turnover frequency (TOF) obtained, 36.4 h−1 is higher than most reported studies. DFT simulations prove the catalytic performance of Mo2GCN significantly decreases the activation energy barrier for PO ring-opening from 50–60 to 4.903 kcal mol−1. Coexistence of Lewis acid/base group improves the CO2 cycloaddition performance by the formation of coordination bond between electron-deficient Mo atom with O atom of PO, while NH2 surface group disrupts the stability of CO2 bond by donating electrons into its low-level empty orbital. Steady-state process simulation of the industrial-scale consumes 4.4 ton h−1 of CO2 with PC production of 10.2 ton h−1. Techno-economic assessment profit from Mo2GCN is estimated to be 60.39 million USD year−1 at a catalyst loss rate of 0.01 wt% h−1. 相似文献
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Hyunsik Choi Bolam Kim Sang Hoon Jeong Tae Yeon Kim Dong-Pyo Kim You-Kwan Oh Sei Kwang Hahn 《Small (Weinheim an der Bergstrasse, Germany)》2023,19(1):2204617
A variety of wound healing platforms have been proposed to alleviate the hypoxic condition and/or to modulate the immune responses for the treatment of chronic wounds in diabetes. However, these platforms with the passive diffusion of therapeutic agents through the blood clot result in the relatively low delivery efficiency into the deep wound site. Here, a microalgae-based biohybrid microrobot for accelerated diabetic wound healing is developed. The biohybrid microrobot autonomously moves at velocity of 33.3 µm s−1 and generates oxygen for the alleviation of hypoxic condition. In addition, the microrobot efficiently bound with inflammatory chemokines of interleukin-8 (IL-8) and monocyte chemoattractant protein-1 (MCP-1) for modulating the immune responses. The enhanced penetration of microrobot is corroborated by measuring fibrin clots in biomimetic wound using microfluidic devices and the enhanced retention of microrobot is confirmed in the real wounded mouse skin tissue. After deposition on the chronic wound in diabetic mice without wound dressing, the wounds treated with microrobots are completely healed after 9 days with the significant decrease of inflammatory cytokines below 31% of the control level and the upregulated angiogenesis above 20 times of CD31+ cells. These results confirm the feasibility of microrobots as a next-generation platform for diabetic wound healing. 相似文献