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991.
正交法在PTA生产中粒径控制上的应用 总被引:2,自引:0,他引:2
介绍了正交试验法在PTA生产中粒径控制上的应用。对第一、二结晶器采用L9( 34)正交表进行试验 ,选出最优操作方案为第一结晶器液位为 2 6 %、压力为 3 6 0 0kPa ,第二结晶器液位为 45 .5 % ,压力为 2 40 0kPa ,结果是 :平均粒径从原来的 ( 118± 10 ) μm控制到 ( 118± 8) μm左右 ,粒径小于 45 μm的从原来的 2 0 %下降到 15 %左右 ,粒径 2 5 0 μm以下的由 93 %上升到95 %左右 相似文献
992.
Yeong-Koo?YeoEmail author Ki-Seok?Hwang Sung?Chul?Yi Hong?Kang 《Korean Journal of Chemical Engineering》2004,21(4):761-766
In this study a model for the drying process in paper production plants was developed based on the mass and heat balances
around drying cycles. Relationships for the heat transfer coefficients between the web and the air as well as between the
drying cylinder and the web were extracted from the closed-loop plant operation data. It was found that the heat transfer
coefficients could be represented effectively in terms of moisture content, basis weight and reel velocity. The effectiveness
of the proposed model was illustrated through numerical simulations. From the comparison with the operation data, the proposed
model represents the paper plant being considered with sufficient accuracy. 相似文献
993.
Hong?ZhangEmail author Lars?Saaby?Pedersen Dorther?Kristensen Jens?Adler-Nissen Hans?Christian Holm 《Journal of the American Oil Chemists' Society》2004,81(7):653-658
Lipozyme TL IM-catalyzed interesterification for the modification of margarine fats was carried out in a batch reactor at
70°C with a lipase dosage of 4%. Solid fat content (SFC) was used to monitor the reaction progress. Lipase-catalyzed interesterification,
which led to changes in the SFC, was assumed to be a first-order reversible reaction. Accordingly, the change in SFC vs. reaction
time was described by an exponential model. The model contained three parameters, each with a particular physical or chemical
meaning: (i) the initial SFC (SFC0), (ii) the change in SFC (ΔSFC) from the initial to the equilibrium state, and (iii) the reaction rate constant value (k). SFCo and ΔSFC were related to only the types of blends and the blend ratios. The rate constant k was related to lipase activity on a given oil blend. Evaluation of the model was carried out with two groups of oil blends,
i.e., palm stearin/coconut oil in weight ratios of 90∶10, 80∶20, and 70∶30, and soybean oil/fully hydrogenated soybean oil
in weight ratios of 80∶20, 65∶35, and 50∶50. Correlation coefficients higher than 0.99 between the experimental and predicted
values were observed for SFC at temperatures above 30°C. The model is useful for predicting changes in the SFC during lipase-catalyzed
interesterification with a selected group of oil blends. It also can be used to control the process when particular SFC values
are targeted. 相似文献
994.
995.
PC/TPU共混物的流变性能 总被引:5,自引:0,他引:5
用毛细管流变仪研究了聚碳酸酯(PC)及聚碳酸酯/热塑性聚氨酯弹性体(PC/TPU)共混物的流变性能。实验结果表明:PC熔体粘度对剪切速率(γ)不敏感,而对温度(T)敏感。温度升高,PC粘度降低。加入TPU大大改善了共混物的流动性能,使共混物的成型加工变得容易进行。当TPU含量为40份时,共混物的熔体粘度出现一极小值。加入不同第三组分对于降低共混物的熔体粘度效果不同,第三组分E对共混物有增粘作用 相似文献
996.
997.
为了辨识具有谐波减速器的柔性关节模型的关键参数,设计了一套基于多传感器融合的离线辨识方法,根据电机的位置传感器、电流传感器和关节力矩传感器的实验数据完成柔性关节模型关键参数的辨识.首先,建立采用谐波减速器柔轮输出的柔性关节模型;然后,使用正反转加载力矩的方法辨识出电机的力矩系数;并在空载的情况下,由关节力矩和电机输出力矩分别辨识出关节端和电机端的摩擦力;最后,采用敲击法初步辨识出关节的刚度和阻尼后,在关节位置受限条件下,逐渐增加电机输出力矩,得到柔性关节刚度和关节力矩的非线性关系.多次实验的结果显示,辨识出的参数具有较高的重复性,验证了该方法的有效性. 相似文献
998.
Experimental investigations were performed to see how the die exit geometry and the extrusion velocity influence on extrudate
swell and melt fracture for several polymer melts [low-density polyethylene, styrene-butadiene rubber (SBR) and SBR/HAF (carbon
black) compound]. Four different types of die exit geometry were considered; 0° (symmetric. usual capillary die), and 30°,
45° and 60° (asymmetric dies) were chosen for the die exit angle. Extrudate diameters were measured without draw-down under
isothermal condition. Polymer melts were extruded into an oil that has the same density and temperature as those of the extrudate.
Extrudate swells from dies with different diameters were correlated with volumetric flow rates. It was observed that the extrudate
swell increases with increasing volumetric flow rate and exhibits through a minimum value at about 45° die exit angle. As
to the fracture phenomena, it was observed that the critical shear for the onset of melt fracture increases with the increasing
die exit angle up to 45°. However, for 60° die exit angle, the onset of melt fracture is again similar to that of 0° exit
angle. 相似文献
999.
PVC新型改性剂AS的合成与应用 总被引:1,自引:0,他引:1
本文主要介绍PVC新型改性剂AS树脂的合成方法、产品性能及其在PVC异型材、管材、注射、压延片等加工领域中的应用。实验结果证明:该产品完全可以代替ACR加工助剂,并有很好的经济效益。 相似文献
1000.
Polyurethane macroiniferter/poly(methyl methacrylate) block copolymer dispersions with inverse core‐shell morphologies were obtained from 1,1,2,2,‐tetraphenylethane‐1,2‐diol, dimethylol propionic acid, 4,4′‐diphenylmethane diisocyanate, and poly(propylene glycol) via a living radical mechanism. Molecular weight, particle size and dispersion viscosity, and thermal, mechanical, and dynamic mechanical properties of the dispersion cast films are reported as a function of copolymerization time. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 1971–1975, 2003 相似文献