Refractive index profiling-state of the art

Problems associated with different calibration techniques and some instrumental effects that can determine instrumental accuracy are discussed. It is shown how transmission effects can be observed and used to generate a correction curve for refracted near-field instruments. High-quality fiber slices needed for axial interferometry were used to obtain refractive index differences on suitable fibers to ±1% with the measurements traceable to national standards. Interferometry was used to calibrate a multiple-step fiber which is available in 10-m lengths with a certificate of calibration. The limitations of the technique are discussed, and preliminary results of a study on the effects of residual stress and stress relief on measurements are given. Comparisons are made between measurements made by axial interferometry and refracted near field on a range of fibers. It is shown that commercial profilers can produce reliable measurements of refractive index difference, absolute refractive index, profile shape, and numerical aperture that agree well with measurements by other techniques     

The effect of additives on the thermal stability of poly(vinyl chloride)

The effect of a range of organic additives on the thermal stability of poly(vinyl chloride), both with and without a chloroparaffin extender, was studied using a number of experimental techniques. Of the additives used the best overall balance was provided by pentaerythritol, which increased stability when the extender was present and had no effect when it was absent. The congo red test emerged as the most suitable technique, being consistent and inexpensive and able to screen several additives simultaneously. Isothermal differential thermal analysis correlated with the congo red test but required more expensive equipment, was time-consuming and demanded good mixing of the poly(vinyl chloride) compound to give reproducible results. Thermogravimetry was not sufficiently sensitive and the heat stability test was the least useful of all.     

Characterization of GaAs layers grown on polycrystalline GaAs by LPE and current controlled LPE

It is the purpose of this paper to investigate the suitability and effectiveness of growth of thin GaAs layers on polycrystalline GaAs substrates by liquid phase epitaxy (LPE) and current controlled LPE (CCLPE). During each growth run LPE and CCLPE were used to grow thin GaAs layers on two large-grain polycrystalline GaAs substrates cut from the same wafer and simultaneously placed in the same growth system. The grain boundary was exposed by cleaving the samples perpendicular to the grain boundary. Notnarski contrast, SEM, C-V and Hall measurements were performed in order to determine the surface morphology, discontinuity of epilayer at the grain boundary, epilayer thickness unform-ity, resistivity (in directions parallel and perpendicular to the grain boundary), and dopant concentration. The CCLPE system was carefully designed so that growth would take place only by electrotransport in the absence of convection or Peltier cooling. The results indicate that CCLPE yields layers with improved surface morphology and thickness uniformity as compared to those grown by LPE. In some samples the epilayer was discontinuous at certain grain boundaries. Results are presented on CCLPE growth rate dependence upon grain orientation, current density, and continuity of the epilayer at the grain boundary.     

Latest Developments in the Batchwise Application of Hot-dyeing Reactive Dyes to Cellulosic Knitwear

A dyeing profile for a range of reactive dyes suitable for application to cellulosic knitwear is defined. Such a profile shows good level-dyeing, reproducibility and fastness properties together with potential for simplified dyeing processes.     

CoGaInS4: A new layered compound

We report on the synthesis results obtained for some compositions in the Co(GaxIn_1-x)₂S₄ family, whose intermediate member CoGaInS₄ is shown to display a layered structure. This result is discussed and compared with the literature.     

DRYING OF GRANULAR PARTICLES IN A MULTISTAGE INCLINED FLUIDIZED BED WITH MECHANICAL VIBRATION

A mathematical model for the drying rate of granular particles in a multistage inclined fluidized bed(IFB) is presented from the standpoint of simultaneous heat and mass transfer, with taking the effect of mechanical vibration added vertically into consideration.

Steady-state distributions for the temperatures and concentrations of the particles and the heating gas, and for the moisture content of the particles are numerically calculated based on the present model. The calculated results show fairly good agreement with the experimental data, which were obtained from the drying experiments of brick particles in a three-stage IFB using comparatively low temperature air(40-60°C) as the heating gas.

It has been found within the range of the experimental conditions employed that, the mechanical vibration added vertically enhances the over-all drying rate of the particles and its effect can be considered equivalent to an increase in the air velocity.     

Frequency response algorithms for H∞optimization with time domain constraints

A very broad framework for control system design is considered that encompasses frequency-response methodologies for H_∞ optimization that solve various aspects of the control design problem and that are less well known that state-space methods. The focus is on linear programming, Lawson's algorithm, and Trefethen's algorithm. A modified Lawson's algorithm is proposed and related to Trefethan's method. The modified algorithm is shown to be significantly faster than linear programming and Lawson's algorithm. It is also shown how to extend the modified Lawson's algorithm so as to handle time-domain constraints in addition to frequency-domain specifications, which distinguishes it from other H_∞ optimization methods. Some steps are taken toward dealing with time domain constraints within an H_∞ optimization framework     

On liquid motion in a circular cylinder with horizontal axis

Summary The flow pattern of the slosh motion of a homogeneous, nonviscous (inviscid) and incompressible fluid with a free surface, contained in a rigid circular canal, has been dealt with analytically and experimentally. The axis of the canal is perpendicular to the direction of gravity. Considered are transverse (lateral to axis) oscillations of the liquid. The shape of the free liquid surface is determined numerically by means of a simple procedure. Theoretically calculated streamlines (path lines) are found to be in good qualitative agreement with experimentally observed trajectories of small spheres, made of plastic material and immersed in the liquid. The plastic particles and the liquid (water with a solution of salt added) have the same density.