液相合成纳米氧化锌及其光催化性能探讨

以硝酸锌和氢氧化钠为原料,分别以水和醇作为溶剂,采用液相直接沉淀法合成纳米氧化锌。在以水为反应溶剂条件下,研究了反应时间、反应温度、反应物浓度和反应物配比对纳米氧化锌中位径和形貌的影响,得到制备较小中位径及合适长径比纳米氧化锌的最优反应条件,即:反应时间为3 h、反应温度为70 ℃、锌离子浓度为0.5 mol/L、锌离子与氢氧根浓度比为1:2。在上述最优反应条件下,研究了不同醇溶剂对纳米氧化锌中位径、形貌及其光催化性能的影响。研究发现,随着溶剂碳链长度的增长,纳米氧化锌中位径呈现上下波动,无明显变化规律,形貌由球状向柱状发展,光催化性能总体不断减弱。     

基于WiFi无线通信的温湿度检测节点设计

基于AM2303温湿度传感器、STC15F104W单片机和WiFi模块设计了一种无线温湿度检测节点。介绍了AM2303及其通信协议、WiFi模块及其组网特性等,并且给出了读取AM2303数据的软件流程。经测试,该节点通信距离远,组网灵活,可很好地应用于粮库粮情检测等实际工作环境。     

石化企业供应链管理研究

介绍了国内外石化行业的供应链管理现状，对中石化电子化供应链方案进行了分析，并就中石化供应链管理存在的问题提出解决方案。     

保证云存储的数据安全

近几年来,云存储的使用越来越广泛,不仅是中小型企业,而且针对个体用户也可以购买云存储服务,但如何在云存储中保证数据的安全性和机密性,单靠云存储服务供应商的承诺是难以让人信服的。本文提出了一种保证数据安全的云存储框架,并且使用服务等级协议（SLA）作为用户和供应商之间的共同标准。此外,本文还提及了几种保证云存储数据安全的技术,这些技术可以被分成三类：存储保护,传输保护和授权保护。     

基于商业智能的小区日用水量预测模型研究

商业智能现在已广泛应用于各个领域,利用商业智能可以对趋势预测做出良好的支持,本文将其中一种常用商业智能的工具——数据仓库技术,应用于小区家庭的用水量预测研究。     

网络安全管理平台研究

信息网络的迅速发展普及应用,在给人们的工作、生活带来巨大便利的同时,也带来了许多安全隐患,出于政治、经济、文化等利益的需要或者好奇心的驱动,网络攻击事件层出不穷、屡见不鲜,且有愈演愈烈之势,轻者给个人或机构带来信息损害、经济利益损失,重者将会影响国家的政治、经济和文化安全.因此,信息网络安全问题已成为国内外研究重点.     

Observer‐based H ∞ output tracking control for networked control systems

This paper is concerned with observer‐based H _∞ output tracking control for networked control systems. An observer‐based controller is implemented through a communication network to drive the output of a controlled plant to track the output of a reference model. The inputs of the controlled plant and the observer‐based tracking controller are updated in an asynchronous way because of the effects of network‐induced delays and packet dropouts in the controller‐to‐actuator channel. Taking the asynchronous characteristic into consideration, the resulting closed‐loop system is modeled as a system with two interval time‐varying delays. A Lyapunov–Krasovskii functional, which makes use of information about the lower and upper bounds of the interval time‐varying delays, is constructed to derive a delay‐dependent criterion such that the closed‐loop system has a desired H _∞ tracking performance. Notice that a separation principle cannot be used to design an observer gain and a control gain due to the asynchronous inputs of the plant and the controller. Instead, a novel design algorithm is proposed by applying a particle swarm optimization technique with the feasibility of the stability criterion to search for the minimum H _∞ tracking performance and the corresponding gains. The effectiveness of the proposed method is illustrated by an example. Copyright © 2013 John Wiley & Sons, Ltd.     

H ∞ control for discrete‐time nonlinear Markov jump systems with multiplicative noise and sector constraint

This paper addresses the finite horizon H _∞ control problem for a class of discrete‐time nonlinear Markov jump systems with multiplicative noise and nonlinear feedback device. The system nonlinearity occurs in a random way specified by a Bernoulli process, whereas the actuator and sensor nonlinearities are restricted to a sector region. Both the state and the dynamic output feedback H _∞ controllers are devised in terms of difference LMIs. The proposed approach not only allows the resulting system to achieve a prescribed disturbance attenuation level, but also enables the output of actuator/sensor to meet the designated sector condition. Moreover, it is also shown that our approach is well‐adapted for dealing with the discrete‐time Markov jump systems with saturated actuator and sensor. Finally, a backward iterative algorithm is provided to solve the obtained difference LMIs and a numerical example is presented to verify the efficiency of the theoretical results. Copyright © 2013 John Wiley & Sons, Ltd.     

有机-无机(硅溶胶)复合涂料的制备

有机-无机(硅溶胶)复合涂料，既具有硅溶胶耐候性好、硬度高、附着力强、耐水、耐碱、耐沾污等特点，又具有有机聚合物成膜性好、韧性大、光泽高等特点。本法选用江阴国联化工有限公司生产的交联改性的苯乙烯-丙烯酸酯乳液与硅溶胶通过物理混拼法，并辅以适当的颜填料、助剂制备的涂料，可作为外墙封闭型底漆用于水泥砂浆、混凝土等硅酸盐基材及用于外墙装饰。文章还述及制备工艺及注意事项。     

堇青石陶瓷烧结工艺及机理研究

本文利用DSC、XRD技术，研究了MgO、Al2O3，和SiO2反应烧结制备堇青石陶瓷的机理。结果表明MgO和Al2O3在1155℃反应合成镁铝尖晶石(MgAl2O4)，进而在1317℃长时间保温与SiO2反应生成堇青石。