Synthesis and characterization of novel copolymers with the trimethylsilyl group for deep‐UV photoresists

N‐(4‐Acetoxyphenyl) maleimide (APMI) and three kinds of comonomers bearing a trimethylsilyl group were copolymerized at 60°C in the presence of azobisisobutyronitrile (AIBN) as an initiator in 1,4‐dioxane to obtain the three IP, IIP, and IIIP copolymers. These copolymers were removed from the acetoxy group in a transesterification process into new IVP, VP, and VIP copolymers with a pendant hydroxyl group. Two modified processes were adopted to prepare photoresists using these copolymers. The first process involved mixing the dissolution inhibitor, o‐nitrobenzyl cholate, with the new copolymers. Second, o‐nitrobenzyl cholate was introduced into the copolymers using 1,8‐diazabicyclo[5.4.0]undec‐7‐ene (DBU) in dimethylformamide (DMF). The cyclic maleimide structure is responsible for the high thermal stability of these copolymers. After irradiation using deep–UV light and development with aqueous Na₂CO₃ (0.01 wt %), the developed patterns showed positive images and exhibited good adhesion to the silicon wafer without using any adhesion promoter. The resolution of these resists was at least 0.8 μm and an oxygen‐plasma etching rate was 1/5.3 to that of hard‐baked HPR‐204. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2791–2798, 2002; DOI 10.1002/app.10255     

变速铣削的试验研究

通过试验考证了变速铣削的减振效果和机床电机电流的波动幅度，试验结果表明，变速铣削同样具有明显的减振效果。机床电机电流虽有波动，但波动幅度不大，不会影响电机的正常使用，变速铣削具有良好的应用前景。     

小型办公网络组网

通过实例,对小型办公网络组网中涉及到的需求设计、网络连接、网络设备、设备连接等进行了论述。     

THE SIMULATION OF THE SAR IMAGE OF INTERNAL SOLITARY WAVES IN ALBORAN SEA

1 .　ＩＮＴＲＯＤＵＣＴＩＯＮＯｃｅａｎｉｎｔｅｒｎａｌｗａｖｅｉｓａｋｉｎｄｏｆｇｒａｖｉｔｙｗａｖｅｇｅｎｅｒａｔｅｄｉｎｔｈｅｓｔｒａｔｉｆｉｅｄｏｃｅａｎ .Ｉｔｐｒｏｄｕｃｅｂｙｔｈｅｉｎｔｅｒａｃｔｉｏｎｏｆｔｉｄｅｃｕｒｒｅｎｔａｎｄｔｏｐｏｇｒａｐｈｙ ,ｓｅａｑｕａｋｅａｎｄｍｏｖｉｎｇｓｈｉｐｗｈｅｎｔｈｅｓｔｒｏｎｇ ,ｓｈａｌｌｏｗｐｙｃｎｏｃｌｉｎｅｉｓ ｐｒｅｓｅｎｔ.Ｔｈｅｉｎｔｅｒｎａｌｗａｖｅｓｉｎｔｈｅｃｏｎｔｉｎｅｎｔａｌｓｈｅｌｆａｒｅａｌｍｏｓｔｔｉｄｅｐｒｏｄ…     

MATLAB在离心式水泵性能曲线测定中的应用

长期以来 ,离心式水泵性能测定和曲线绘制工作无论是对生产厂家还是对用户都是很必要 ,但又是很繁杂的 .随着计算机技术的发展 ,数学正以其解决实际问题的卓越能力进入到各种领域 .从而使离心式水泵性能测定和曲线绘制工作得以简化 .MATLAB的出现又使离心式水泵的性能曲线的绘制达到了更加快速、准确、直观 .     

长幅外摆线轮齿廓曲线的优化圆弧

本文提出了用最优化圆弧代替长幅外摆线轮齿廓曲线的一种新型算法。该算法实用简单,拟合效果好,并可用于渐开线等其它类型曲线。     

Improved authenticated multiple-key agreement protocol

Recently, Harn and Lin (1998) developed a two-phase authenticated key agreement protocol which enables two parties to share multiple secret keys. The first phase of their protocol is the most important part and can be used to deliver a sequence of temporary random public keys to the other party in an authenticated approach. The authors demonstrate an improved version of this novel scheme after giving some cryptanalytic details of the original Harn-Lin scheme     

氟碳铈矿／直氟碳钙铈矿混层结构中新规则混层矿物的超微结构研究

用电子衍射和晶格像技术研究了钙稀土氟碳酸盐矿物中的氟碳铈矿（Ｂ）／直氟碳钙铈矿（Ｓ）混层结构，发现并确定了Ｂ＿４Ｓ＿４、Ｂ＿８Ｓ＿６、Ｂ＿１Ｓ＿６、Ｂ＿７Ｓ＿４和Ｂ＿２Ｓ＿１５种新规则混层矿物的对称性、晶胞参数及理论晶体化学式。根据所获得的高分辨晶格像真实而直观地揭示出该类Ｂ＿ｍＳ＿ｎ（ｍ＞ｎ）型新规则混层矿物的长周期有序堆垛结构特征及变化规律。     

脉冲激光LGA法钛表面氮化及其XRD和SEM微观分析

用调Ｑ－ＹＡＧ和ＸｅＣｌ脉冲激光在钛表面以激光气体合金化方法生成氮化钛层，用Ｘ射线衍射仪分析了不同激光能量、不同Ｎ２气压不同作用脉冲数等条件下ＴｉＮ的结晶取向、结晶形态、氮化程度，用扫描电镜观察了它们的微观结构，对脉冲激光的ＬＧＡ法机理进行了探讨，也发现了用ＬＧＡ法对Ｍｏ的氮化生成Ｍｏ２Ｎ．     

扩大3~＃高炉上料能力的软、硬件改进

济钢第一炼铁厂３~＃高炉，（３５０ｍ~３）大修后采用了工业计算机、液压传动等先进的控制系统，但由于设备工艺布局不合理，使先进的技术不能充分发挥效率。通过对软、硬件的部分改进，挖掘了控制系统的能力，达到了少投资多受益的目的。