PEPT study of particle cycle and residence time distributions in a Wurster fluid bed

Particle cycle and residence time distributions are critical factors in determining the coating quality in the Wurster process. Positron emission particle tracking experiments are performed to determine the cycle and residence times of particles in different regions of a Wurster fluid bed. The results show that particles tend to recirculate in and sneak out below from the Wurster tube. The experiments also show that a larger batch size leads to a shorter cycle time and a narrower cycle time distribution (CTD). It is possible to avoid recirculations and obtain a shorter cycle time and a narrower CTD by selecting the operating conditions appropriately or via equipment design. Experiments using binary mixtures of particles with a diameter ratio of 1.5 show that large particles have a longer cycle time than small particles and that the cycle time is shorter for mixtures with approximately equal amounts of small and large particles. © 2014 American Institute of Chemical Engineers AIChE J, 61: 756–768, 2015     

Hydrodynamics and steel tube wastage in a fluidized bed at elevated temperature

Hydrodynamic measurements were made in a bubbling fluidized bed operated at 550°C at three different excess gas velocities (0.15, 0.40 and ). The bed has a cross-sectional area of with an immersed tube bank consisting of 59 horizontal stainless steel tubes (AISI 304L), 21 of which are exchangeable, thus allowing erosion studies. Capacitance probe analysis was used to determine the mean bubble rise velocity, the mean bubble frequency, the mean pierced bubble length, the mean bubble volume fraction and the mean visible bubble flow rate. Tube wastage was calculated from roundness profiles obtained by stylus profilometry.A redistribution of the bubble flow towards the center of the bed occurs when the excess gas velocity is increased. Measurements along a target tube, situated next to the capacitance probe, usually show greater material wastage at the central part of the tube, since the mean bubble rise velocity and the mean visible bubble flow rate are higher there. It is suggested that the greater material degradation is also an effect of the through-flow of a particle-transporting gas stream in the bubbles. With increasing height above the distributor plate the circumferential wastage profiles for the lowest excess gas velocity show a gradual change from an erosion pattern with one maximum (Type B behavior) to a pattern with two maxima (Type A behavior). Power spectral density distributions of the fluctuating pressure signals show that this is a result of the formation of larger bubbles, when the fluidization regime is changed in the upper part of the bed. At the highest excess gas velocity the bubble flow becomes more constrained due to a more rapid coalescence of the bubbles and the tubes show Type A wastage profiles throughout the bed.     

Effect of additives on the melt rheology and thermal degradation of poly[(R)‐3‐hydroxybutyric acid]

Thermal degradation of poly[(R)−3‐hydroxybutyric acid] (PHB) during melt mixing results in random chain scission that produces shorter polymer chains containing crotonic and carboxyl end groups. One way of preventing this serious reduction of molar mass is to add agents that react with at least two of the newly generated end groups. Different types of commercially available additives known to react with carboxyl group, namely bis(3,4‐epoxycyclohexylmethyl) adipate (BECMA), 2,2'‐bis(2‐oxazoline) (BOX), trimethylolpropane tris(2‐methyl‐1‐aziridinepropionate) (PETAP), triphenyl phosphate (TPP), tris(nonylphenyl) phosphate (TNPP), polycarbodiimide (PCDI), and poly(methyl metharylate‐co‐glycidyl methacrylate) (GMA.MMA) were mixed with PHB by cocasting from solution in chloroform. Dynamic rheology as well as measurements of molar masses before and after dynamic analysis was used to evaluate the effect of the additives on the melt stability of PHB. Measurements of the dynamic shear modulus and the molar mass of molten PHB with the additives PCDI and GMA.MMA showed a minor improvement on the thermal stability. Furthermore, TPP and TNPP did not affect the thermal stability of PHB, whereas the presence of BECMA, BOX, and PETAP gave a strong decrease of the dynamic modulus compared with neat PHB. © 2014 The Authors Journal of Applied Polymer Science Published by Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 41836.     

Virtual-Holonomic-Constraints-Based Design of Stable Oscillations of Furuta Pendulum: Theory and Experiments

The Furuta pendulum consists of an arm rotating in the horizontal plane and a pendulum attached to its end. Rotation of the arm is controlled by a DC motor, while the pendulum is moving freely in the plane, orthogonal to the arm. Motivated, in particular, by possible applications for walking/running/balancing robots, we consider the Furuta pendulum as a system for which synchronized periodic motions of all the generalized coordinates are to be created and stabilized. The goal is to achieve, via appropriate feedback control action, orbitally exponentially stable oscillations of the pendulum of various shapes around its upright and downward positions, accompanied with oscillations of the arm. Our approach is based on the idea of stabilization of a particular virtual holonomic constraint imposed on the configuration coordinates, which has been theoretically developed recently. Here, we elaborate on the complete design procedure. The results are illustrated not only through numerical simulations but also through successful experimental tests.     

The motivation of information technology consultants: The struggle with social dimensions and identity

Increasingly, customer companies hire external information technology (IT) consultants, often on a special project basis. These consultants are employees of professional service firms, although they receive their assignments from the hiring companies, report to them, and are supervised by them. Using semistructured interviews with 12 IT consultants in Sweden, we examine the factors that influence their work motivation, including the effect of this dual allegiance—to the service firm and to the customer company. The data indicate that the primary motivators are the variety in tasks and the opportunity to influence and/or manage an entire project. Neither monetary incentives nor the consultancy firm norms are strong motivators. A factor that affects work behavior and motivation is the subordinate identity that IT consultants must assume with their powerful clients. The article concludes with practical suggestions for managers who seek to understand what motivates employees who work at a distance, under external control. © 2011 Wiley Periodicals, Inc.     

Security measure allocation for industrial control systems: Exploiting systematic search techniques and submodularity

To protect industrial control systems from cyberattacks, multiple layers of security measures need to be allocated to prevent critical security vulnerabilities. However, both finding the critical vulnerabilities and then allocating security measures in a cost‐efficient way become challenging when the number of vulnerabilities and measures is large. This paper proposes a framework that can be used once this is the case. In our framework, the attacker exploits security vulnerabilities to gain control over some of the sensors and actuators. The critical vulnerabilities are those that are not complex to exploit and can lead to a large impact on the physical world through the compromised sensors and actuators. To find these vulnerabilities efficiently, we propose an algorithm that uses the nondecreasing properties of the impact and complexity functions and properties of the security measure allocation problem to speed up the search. Once the critical vulnerabilities are located, the security measure allocation problem reduces to an integer linear program. Since integer linear programs are NP‐hard in general, we reformulate this problem as a problem of minimizing a linear set function subject to a submodular constraint. A polynomial time greedy algorithm can then be applied to obtain a solution with guaranteed approximation bound. The applicability of our framework is demonstrated on a control system used for regulation of temperature within a building.     

Joint optimization of communication rates and linear systems

We consider a linear control system in which several signals are transmitted over communication channels with bit rate limitations. With the coding and medium access schemes of the communication system fixed, the achievable bit rates are determined by the allocation of communications resources such as transmit powers and bandwidths, to different communication channels. We model the effect of bit rate limited communication channels by uniform quantization and the quantization errors are modeled by additive white noises whose variances depend on the achievable bit rates. We optimize the stationary performance of the linear system by jointly allocating resources in the communication system and tuning parameters of the controller.     

SearchFill: A stochastic optimization code for detecting atomic vacancies in crystalline and non-crystalline systems

We present an implementation of a stochastic optimization algorithm applied to location of atomic vacancies. Our method labels an empty point in space as a vacancy site, if the total spatial overlap of a “virtual sphere”, centered around the point, with the surrounding atoms (and other vacancies) falls below a tolerance parameter. A Metropolis-like algorithm displaces the vacancies randomly, using an “overlap temperature” parameter to allow for acceptance of moves into regions with higher overlap, thus avoiding local minima. Once the algorithm has targeted a point with low overlap, the overlap temperature is decreased, and the method works as a steepest descent optimization.Our method, with only two free parameters, is able to detect the correct number and coordinates of vacancies in a wide spectrum of condensed-matter systems, from crystals to amorphous solids, in fact in any given set of atomic coordinates, without any need of comparison with a reference initial structure.     

Organizational climate in air traffic control Innovative preparedness for implementation of new technology and organizational development in a rule governed organization

A positive and innovative organizational climate is of great importance in order to manage and adapt to change. Such a climate seldom evolves in organizations closely governed by rules and regulations. Because of ongoing organizational and technical changes within the Swedish Air Navigation Services Provider, a study concerning the organizational climate for changes and innovations was conducted to investigate the organization's capacity to cope with changes. Study locations were the two Swedish main air traffic control centers and parts of the civil aviation administration headquarters. In the study 390 subjects took part and the CCQ questionnaire was used to measure the organizational climate. The results show that the organizational climate is quite positive despite the rule-governed work. The results also show that administrative personnel assess the organizational climate as more positive than operative personnel. Comparisons between management positions did not result in any differences.     

Extracting 3D information on bone remodeling in the proximity of titanium implants in SRμCT image volumes

Bone-implant integration is measured in several ways. Traditionally and routinely, 2D histological sections of samples, containing bone and the biomaterial, are stained and analyzed using a light microscope. Such histological section provides detailed cellular information about the bone regeneration in the proximity of the implant. However, this information reflects the integration in only a very small fraction, a 10 μm thick slice, of the sample. In this study, we show that feature values quantified on 2D sections are highly dependent on the orientation and the placement of the section, suggesting that a 3D analysis of the whole sample is of importance for a more complete judgment of the bone structure in the proximity of the implant. We propose features describing the 3D data by extending the features traditionally used for 2D-analysis. We present a method for extracting these features from 3D image data and we measure them on five 3D SRμCT image volumes.We also simulate cuts through the image volume positioned at all possible section positions. These simulations show that the measurement variations due to the orientation of the section around the center line of the implant are about 30%.