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81.
82.
Jinguang?Xu Zhijian?TianEmail author Junwei?Wang Yunpeng?Xu Zhusheng?Xu Liwu?Lin 《Korean Journal of Chemical Engineering》2003,20(2):217-221
Hydrothermal synthesis by using urea hydrolysis at 1.0-3.0 MPa and 120-130 ‡C was employed to prepare Mn-substituted hexaaluminate
catalysts for methane combustion. The results from DTA-MS demonstrated that CO3- and Off anions co-exist in the hydrothermal reaction. XRD reveals that the components of carbonates and hydroxides in the
hydrothermal reaction are more favorable than those in the (NH4)2CO3 co-precipitation for the formation of the Mn-substituted hexaaluminate phase. After calcination at 1,200 ‡C for 2 h, LaMnAl11O19 is the major phase of the catalyst prepared by the hydrothermal synthesis method while LaAlO3 is the major one of the catalysts prepared by NH4OH and (NH4)2CO3 co-precipitation. The catalyst prepared by hydrothermal synthesis has higher activity than that prepared by NH4OH and (NH4)2CO3 co-precipitation. The major reason is that more Mn2+ ions have incorporated into the hexaaluminate lattice. The effect of drying methods on the formation of hexaaluminate phase
was also discussed. 相似文献
83.
Michail V. Kozlov Junwei Zhu Peter Philipp Wittko Francke Elena L. Zvereva Bill S. Hansson Christer Löfstedt 《Journal of chemical ecology》1996,22(3):431-454
The fifth abdominal segment of femaleEriocrania semipurpurella (Stephens) andE. sangii (Wood) contains a pair of exocrine glands. Hexane extracts of this segment were prepared from both species and analyzed by gas chromatography with simultaneous flame ionization and electroantennographic detection (EAD). For both species, the EAD active peaks were identified as nonan-2-one, (Z)-6-nonen-2-one, and (Z)-6-nonen-2-ol by means of mass spectrometry and comparison of retention indices with those of synthetic standards. Enantiomeric separation of chiral alcohols from the female extracts was achieved by gas chromatographic analysis on a cyclodextrin column. InE. semipurpurella, a mixture of (2S,6Z)-nonen-2-ol and (2R,6Z)-nonen-2-ol (2: I) was found, whereas inE. sangii (2S,6Z)-nonen-2-ol was the predominant enantiomer and only traces of theR enantiomer were indicated by the antennal response. In field tests, a blend of the three compounds was not attractive to conspecific males. A subtractive assay showed that the alcohol in various enantiomeric mixtures was the only attractive compound, whereas addition of (Z)-6-nonen-2-one to the alcohol completely inhibited the attraction of both species. A trapping experiment including a wide range of ratios between theR andS enantiomers showed that baits containing 95–100% of theS enantiomer were attractive to maleE. sangii, whereas males ofE. semipurpurella were attracted to all tested ratios of the enantiomers. However, the response profiles of maleE. semipurpurella differed between populations from southern Sweden, south Finland, and the Kola Peninsula in Russia. In south Sweden males were maximally attracted to a racemic mixture of the alcohols. At the Kola PeninsulaE. semipurpurella was attracted to baits containing 95–100% of theR enantiomer. In south Finland all tested ratios between 0 and 100%R enantiomer trappedE. semipurpurella, but the trap catches appeared to be bimodally distributed with peaks around 15 and 70%R enantiomer. The trapping results suggest the existence of pheromone races or sibling species among the specimens identified asE. semipurpurella.Dedicated to Prof. H. J. Bestmann on the occasion of his 70th birthday. 相似文献
85.
针对目前视觉SLAM方法鲁棒性差、耗时高,使系统定位不够精确的问题,提出了一种基于点线特征融合的视觉惯性SLAM算法。首先通过短线剔除和近似线段合并策略改进LSD(line segment detection)提取质量,以提高线特征检测的速率和准确度;然后在后端优化中有效融合了点、线和IMU数据,建立最小化目标函数进行优化,得到更精确的相机位姿;最后在EuRoC数据集和现实走廊场景进行了实验验证。实验表明,所提算法可以有效提升线特征提取的质量和速度,同时有效提高了SLAM系统的定位精度,获得更为丰富的点线结构地图。 相似文献
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In order to solve the problems of appearance change, scale and rotation change in the visual tracking, a two-level searching tracking algorithm based on Fast Fourier Transform(FFT)is proposed. It achieves two-level searching by establishing the object's kernel ridge regression model in the Cartesian coordinates and log-polar coordinates, respectively, and the efficiency can be improved by transforming the operation into the frequency domain based on FFT. First, the kernel ridge regression model is constructed in the Cartesian coordinate and the object's center position is obtained by the exhaustive search method based on the circular structure matrix. Then, it transforms the object area to the log-polar coordinates and searches the shift using the kernel ridge regression model in the log-polar coordinates. Finally, the object's state is calculated according to the searching results and the object's model is updated. Experimental results indicate that the proposed algorithm not only can obtain a distinct improvement in coping with the appearance change, scale and rotation change, but also have a high tracking efficiency. 相似文献
89.
在地磁导航中磁传感器会受到载体自身磁场的影响,为了提高磁场测量精度,需要对观测数据的载体磁场干扰进行精确补偿。在分析载体固有磁场和感应磁场数学模型的基础上,根据椭圆假设磁补偿方法的思路,提出了一种载体三维磁场干扰的补偿方法,并在椭球假设的基础上提出了载体磁场干扰补偿参数求解方法。该方法将载体磁场干扰补偿方法从二维拓展到三维,解除了载体二维运动姿态的限制。实验验证表明:该方法可以有效实现载体自身三维磁场干扰的补偿,从而提高地磁场的测量精度。 相似文献
90.
为研究H形柱传统弱轴连接节点的抗震性能,对已有缩尺试验进行了有限元模拟和8个足尺模型的有限元模拟分析.通过与缩尺试验模型相同尺寸的有限元模型对试验进行了模拟,两者吻合较好.并且对8个足尺有限元模型结果的分析和对比,得出了该种连接的抗震延性、塑性转动能力等相关结论.并给出了对该种连接不足之处的一些改进建议. 相似文献