Morphological reversible contour representation

In this paper, a novel morphological reversible contour representation of discrete binary images is proposed. A binary image is represented by a set of nonoverlapping multilevel contours and a residual image. In this proposed representation, the total number of pixels representing an image is far less than the total number of pixels obtained by the seed-based morphological contour-skeleton lossless representation. The proposed contour representation is simple, unique, and general without restrictions on the binary image to be represented. The resulting multicontour image component is robust to noise. An efficient differential chain contour coding scheme is employed to further compress the represented image. The proposed method yields very low bit rates compared to the existing morphological techniques. An automatic filling procedure, which properly fills a proper multicontour image according to its topological structure without need of seed points, is proposed     

A GC–MS study of the addition reaction of aryl amines with acrylic monomers

Previous studies have shown that the interaction of carboxylic acid groups with the amine functionalities of aryl amines, especially secondary and tertiary aryl amines, can lead to the free-radical polymerization of acrylic monomers such as methyl methacrylate. In this study, the Michael addition reaction of primary and secondary aryl amines with acrylic monomers such as acrylic acid (AA) was investigated. Equivalent amounts of either p-toluidine (PT) or N-phenylglycine (NPG) and AA were combined in polar solvents such as ethanol. The reactions were conducted at ambient (23°C) or near-ambient (37–60°C) temperatures. Samples (about 3–5 mg) of these products were then trimethylsilylated with a solution consisting of 0.4 mL of bis(trimethylsilyl)trifluoroacetamide (BSTFA) and 0.4 mL of acetonitrile by heating for 30 min at 140°C under N₂. These derivatives were characterized by gas chromatography–mass spectrometry (GC–MS). The GC–MS analyses suggest that 1 mol of the primary amine PT had reacted with 2 mol of AA to yield the expected N-p-tolyliminodipropionic acid. Similarly, the secondary amine NPG added to 1 mol of AA yielded the corresponding mixed iminodiacid, N-phenyliminoacetic–propionic acid. It would appear that the Michael reaction of primary and secondary amines with acrylic monomers may offer a general, facile synthetic route to a variety of tertiary amines. Aryl amino acids of the type synthesized in this study may find use in a number of dental applications, e.g., as surface-active adhesive agents and as polymerization initiators or activators. © 1998 John Wiley & Sons, Inc. J Appl Polm Sci 67:1545–1551, 1998     

Characterization and thermal degradation of poly(d,l‐lactide‐co‐glycolide) composites with nanofillers

Chemical and thermal characterization of poly(d ,l ‐lactide‐co‐glycolide) (PLGA) composites filled with hydroxyapatite (HA) or carbon nanotubes (CNT) were evaluated by infrared spectroscopy, differential scanning calorimetry, thermogravimetry, and dynamic–mechanical–thermal analysis. The morphology and distribution of the nanoparticles were studied by transmission electron microscopy. The composites were prepared by solvent casting using 30% HA or 1, 3, and 5% of pristine and functionalized CNT as nanoparticles and PLGA 75:25 and PLGA 50:50 as copolymer matrix. The Coats–Redfern and E₂ function methodologies were used to calculate the reaction order and the activation energy (E_a) of the thermal degradation process. It was found that the addition of nanoparticles increased the glass transition temperature (T_g) of the composites. Also, higher degradation temperatures and E_a values were obtained for PLGA–HA composites and compared with the neat copolymer, and the opposite behavior was exhibited by PLGA–CNT composites. The thermal and mechanical properties were highly dependent on the morphology and dispersion of the filler. The functionalization process of CNT promoted, to some extent, a better distribution and dispersion of CNT into the matrix, and these composites exhibited a slight enhancement on storage modulus. On the other hand, PLGA–HA composites showed a good dispersion but no improvement on the storage modulus below T_g. POLYM. ENG. SCI., 2013. © 2012 Society of Plastics Engineers     

Optimization of elastic columns using axial grading concept

This paper presents an exact method for obtaining column’s designs with the maximum possible critical buckling load while maintaining the total structural mass at prescribed value equal to that of a known baseline design. The developed optimization model dealt with slender elastic columns that are axially graded in either material or wall thickness. The first type of columns with material grading is constructed from uniform segments that are fabricated from two different materials, making the physical and mechanical properties change piecewisely in the axial direction. Design variables include the volume fraction of the constituent materials as well as the length of each segment composing the column. The other type considers piecewise axial grading of the cross-section wall thickness of columns constructed from uniform homogeneous isotropic segments. The associated design variables include the wall thickness and length of each segment composing the column. The buckling load analysis in either case is performed via an exact method, which ensures the attainment of the global maximum critical load under the imposed equality mass constraint for any number of segments, type of boundary conditions, type of cross section and type of material of construction. Numerical examples and detailed results, which are based on dimensionless analysis, are given and useful design charts have been developed for the cases of simply supported and cantilevered columns. Actually, the given approach can be beneficial to guide structural engineers for choosing the significant design variables in a proper and efficient way without violating economic feasibility requirements.     

Functional versus random test generation for sequential circuits

This article presents a test generation method for sequential circuits based on their synthesis specifications as finite state machines (FSM) and provides comparison with random test generation. The finite state machines are represented by their state transition graph (STG). The test generation method is performed in two phases. The first phase is functional. It generates a test sequence which is one of the shortest input sequences going through all the transitions of the state transition graph machine. This sequence provides a high fault coverage of stuck-at faults on the synthesized circuit compared to a randomly generated test sequence. This fault coverage is very close to the ones of other sequences derived by fault-oriented test generation approaches [9], [10], although these latter sequences are much longer.The trend of the fault coverage curve for different test sequences including progressively the transitions of the test sequence defined in the first phase is similar to the one of the fault coverage curve of a random sequence but for same lengths the first curve gives larger fault coverage. Both curves grow rapidly until a given ratio of faults is detected then continue to grow very slowly exhibiting low efficiency.The second phase of the test generation method is fault-oriented. It uses a fault simulation based approach in order to compute the test sequence for the remaining faults not detected by the first phase. At the end of this phase the test sequence for all the nonredundant faults is derived and, the combinationally redundant faults and the sequentially redundant faults are distinguished.     

EVALUATION OF A COMPOSITE BASED ON HIGH-DENSITY POLYETHYLENE FILLED WITH SURFACE-TREATED HYDROXYAPATITE

Summary  Composites properties are directly related to the degree of interaction between the plastic matrix and the inorganic filler. In the present work, the improvement of the composite’s properties by means of the addition of surface-treated and untreated hydroxyapatite (STHA and HA, respectively) was studied. An ethylene-acrylic acid copolymer was melt blended with high-density polyethylene and HA (HDPE/HA/EA). A surface treatment was performed using an ethylene-acrylic acid (EA) copolymer for STHA₁ and acrylic acid (AA) for STHA₂. High-density polyethylene (HDPE) was also tested. STHA₁ and STHA₂ composites exhibited Young’s modulus values (556 and 558 MPa, respectively) 22 % higher than that of HDPE/HA (455 MPa) and 8 % higher than that of HDPE/HA/EA (520 MPa). Additionally, STHA composites showed both yield stress and strain (σ_STHA1= 23 MPa; ε_STHA1= 9 %; σ_STHA2= 22 MPa; ε_STHA2= 10 %) having a remarkably different behavior from that of the HA composites, which showed no yielding at all. TEM micrographs showed better filler dispersion when surface treatment was applied to HA. Yet, the presence of EA copolymer exhibited a poorer thermal stability. The crystallinity degree as well as the crystallization and melting temperatures showed no significant variation. Regarding in vitro evaluation, composites with HA and EA copolymer proved to have better cell adhesion at early stages. The results of the STHA composites could be attributed to the electrostatic interactions taking place between the ethylene-acrylic acid copolymer and the polar groups of the HA.     

A cataloging framework for software development methods

A framework providing a basis for comparing and evaluating software development methods (SDMs), which are systems of technical procedures and notational conventions for the organized construction of software-based systems, is presented. Using the framework, practitioners and methodologists can describe and rate an SDM's support for 21 properties. The application of the framework to two examples, OMT and R.J.A. Buhr's (1990) architectural design, is discussed. Several suggested uses of the framework include: comparing a group of SDMs with one another; defining a standard in terms of the framework and then using this as a basis for discussion; examining an SDM to discover its coverage and capabilities; and combining the properties of different SDMs to create a new SDM     

Decision Analysis Applied to Tunnel Exploration Planning. I: Principles and Case Study

Exploration planning is a process of decision making under uncertainty. This paper, Part I of two dealing with the exploration problem, briefly reviews the decision analytical procedure for tunnel exploration, and provides practical techniques to do so. Specifically, this paper presents an approach by which the effect of additional exploration can be assessed before actually committing to exploration, through a process of so-called virtual exploration. This is practically done with an easy-to-use software package developed in Visual Basic for Applications in Microsoft Excel, called the Decision Aids for Tunnel Exploration. Part II will describe the uncertainties that enter into the tunnel exploration decision procedure, and will provide practical techniques to asses the effects of these uncertainties on the exploration decision making.     

Gamma-ray emitting test sources for Portal Monitors used for homeland security

The National Institute of Standards and Technology developed a new set of test sources for testing of portal monitors against the ANSI standard N42.35-2004. The design and source specifications are provided in this work.