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排序方式: 共有1177条查询结果,搜索用时 0 毫秒
61.
Sondes Mechri Khelifa Bouacem Taha-Bilel Chalbi Marwa Khaled Fawzi Allala Amel Bouanane-Darenfed Hocine Hacene Bassem Jaouadi 《Journal of surfactants and detergents》2022,25(4):487-504
The ability of microorganisms to grow at high temperature, alkaline pH, and high salinity makes them an attractive target for enzyme-production with several industrial applications. One strain TN-X30 has been selected as protease producer and identified as Streptomyces mutabilis after a phenotypic and molecular study. Its production of protease was improved using Taguchi L27 design. The strategy was carried out to identify the optimum levels and the interaction of the screened factors. Following this step, maximum protease activity (10,895 U/ml) was achieved after 6-days of incubation. The TN-X30 protease activity had an optimum of pH and temperature of 10 and 65°C, respectively. Thermodynamic parameters at 60°C were enthalpy 14.26 kJ/mol, entropy −220 J/mol/K, and Gibbs free energy 90.53 kJ/mol. TN-X30 protease production displayed a 16-fold increase reaching 175,000 U/ml in a 100-L fermentor. Furthermore, the lyophilization in presence of sorbitol enhanced the stability of the TN-X30 protease which remained active at 75% after 24-months of storage. The lyophilized TN-X30 protease exhibited exceptional stability indexes in presence of some known commercialized detergent components as NEODOL® 25-7, Dehydol® LT 7, Na2 CMC, Galaxy LAS, Galaxy LES 70, Galaxy 110, Galaxy CAPB Plus, and Sulfacid K. The lyophilized enzyme also displayed high stability with respect to both solid and liquid detergents. Finally, TN-X30 protease exhibited remarkable destaining of blood, egg, and chocolate stained cloth pieces. These findings may promote TN-X30 protease for use as bioadditive in detergent formulation, thereby reducing environmental chemical threat. 相似文献
62.
K. F. Khaled 《Journal of Applied Electrochemistry》2009,39(3):429-438
Electrochemical frequency modulation, EFM is a new technique for corrosion rate measurements. With the EFM technique, the
corrosion rate and corrosion kinetic parameters can be obtained instantaneously without prior knowledge of Tafel slopes, which
makes this method an ideal technique for application as a corrosion monitoring tool. Results obtained with the EFM technique
were shown to be in agreement with chemical (weight loss) and electrochemical methods (Tafel extrapolation and electrochemical
impedance spectroscopy, EIS) for corrosion rate measurements. New synthesized hydrazine carbodithioic acid derivatives namely,
N′-furan-2-yl-methylene-hydrazine carbodithioic acid (A), N′-(4-dimethylamino-benzylidene)-hydrazine carbodithioic acid (B) and N′-(3-nitro-benzylidene)-hydrazine carbodithioic acid (C) were examined as corrosion inhibitors for carbon steel in 1 M perchloric
acid solution. The results obtained from both chemical and electrochemical measurements show that these compounds suppressed
both anodic and cathodic processes of carbon steel corrosion in 1 M HClO4 by adsorption on the electrode surface. The adsorption mode follows the Langmuir adsorption isotherm. The efficiency of the
inhibitors increases in the order C > B > A. 相似文献
63.
An investigation of pore cracking in titanium welds 总被引:1,自引:0,他引:1
T. Khaled 《Journal of Materials Engineering and Performance》1994,3(1):21-36
Two welded Ti-6A1-4V pressure vessels leaked prematurely in service. The leaks were caused by cracks emanating from weld porosity.
The cracks originated during fabrication, with subsequent growth in service leading to the formation of the leak paths. Pore
cracking is thought to be caused by a mechanism that involves both sustained-load and cyclic contributions, with the former
being the more prominent. It is shown that the tendency for cracking is influenced by pore position and that pore size is
not a deciding factor in that regard. The factors that govern pore cracking are discussed, and the possible role of interstitial
embrittlement is assessed. 相似文献
64.
Nanospherical titanium oxide with anatase structure was obtained at low temperature and normal pressure using a simple method of preparation. The dilute titanium (III) chloride solution was stirred at room temperature for several hours, and then ammonium hydroxide with hydrogen peroxide was added. A yellow gel TiO2·xH2O was obtained with nanodot shape and amorphous structure. Heated at 300 °C, it crystallized to pure anatase structure with nanospherical shape. The anatase particles prepared show good adsorption and photodegradation of Congo red solution under the sunlight. Materials were characterized by powder X-ray diffraction, thermal analysis, transmission electron microscope and UV spectroscopy. 相似文献
65.
66.
Synthesis and characterization of (poly (N-vinyl formamide)—pregelled starch—graft copolymer 总被引:1,自引:0,他引:1
Khaled M. Mostafa Abdul Rahim Samarkandy Azza A. El-Sanabary 《Journal of Polymer Research》2010,17(6):789-800
Bromate / cyclohexanone redox system was investigated as a novel initiator for graft copolymerization of N-vinyl formamide
onto pregelled starch. A number of variables in the grafting reaction were investigated including N-vinyl formamide, cyclohexanone,
bromate ion, sulphuric acid and pregelled starch concentrations, material to liquor ratio along with polymerization time and
temperature. The graft copolymers were evaluated in terms of graft yield, graft reaction efficiency and homopolymer formation
(%). The optimum conditions for grafting of N-vinyl formamide onto pregelled starch are: N-vinyl formamide 50% based on weight
of substrate, cyclohexanone 15 mmol / l, bromate ion, 30 mmol / l, liquor ratio 10, pH 6, time 120 min., and temperature 40°C.
On the other hand, characterizations of the resultant copolymers with respect to swelling capacity, solubility %, metal ion
up-take and suitability as a sizing agent for cotton textiles were investigated. The results obtained reflect that, the resultant
copolymer shows better results for the aforementioned properties in comparison with that obtained from native pregelled starch
as a starting substrate. 相似文献
67.
Fadi Al-Badour Nesar Merah Abdelrahman Shuaib Abdelaziz Bazoune 《Journal of Materials Processing Technology》2013,213(8):1433-1439
A 3-dimensional localized finite element model (FEM) is developed to predict likely conditions that result in defect generation during friction stir welding (FSW). The workpiece is modeled using Eulerian formulation, while the tool is modeled using Lagrangian. Coulomb's frictional contact model is adopted to define the tool workpiece interaction, while the welding speed is defined by material inflow and outflow velocities. The numerical results show that the coefficient of friction has a major effect on void formation; the lower the friction coefficient is applied, the larger the void is formed. Furthermore, welding using force control (FC) at lower welding speed results in smaller void size and wider plastic zone, leading to higher quality weld. 相似文献
68.
Rajivgandhi Govindan Nadar Chenthis Kanisha Chelliah Vijayakumar Sekar Alharbi Naiyf S. Kadaikunnan Shine Khaled Jamal M. Alanzi Khalid F. Li Wen-Jun 《Journal of Inorganic and Organometallic Polymers and Materials》2021,31(10):3921-3933
Journal of Inorganic and Organometallic Polymers and Materials - The silver oxide nanoparticle was successfully synthesized using floral waste by simple one pot, cost effective method. The complete... 相似文献
69.
Khaled Sennah Marwan Saliba Nidal Jaalouk 《Journal of Constructional Steel Research》2009,65(5):1034-1042
The Canadian Standard for Antenna Towers and Antenna Supporting Structures, CSA-S37-01, specifies expressions for the compressive resistance of solid rounds based on the Structural Stability Research Council (SSRC) Column Curves for non-solid-round members and the results from experimental investigations on the compressive resistance of solid rounds carried out back to 1965. Similar Standard in USA (TIA/EIA-222-G.0) specifies design criteria for such members as derived from the superseded AISC-LRFD-94 Standard, which is independent of the shape of the member cross-section. The European Standard, Eurocode 3, provides column curves for the compressive resistance of various structural steel members, and assumes the applicability of one of them to solid rounds. As such, it is necessary to conduct an experimental study on solid round stress-relieved steel members to refine the available design equations for such members. This paper provides a summary of the literature review on solid rounds as well as a recent test program conducted on stress-relieved steel solid rounds. Correlation between the results from these tests and the current practice for the design of solid rounds is investigated. The paper concludes with a proposed compressive resistance equation for economical design of such members. 相似文献
70.
Elsayed KA DeYoung RJ Petway LB Edwards WC Barnes JC Elsayed-Ali HE 《Applied optics》2003,42(33):6650-6660
An all solid-state Ti:sapphire laser differential absorption lidar transmitter was developed. This all-solid-state laser provides a compact, robust, and highly reliable laser transmitter for potential application in differential absorption lidar measurements of atmospheric ozone. Two compact, high-energy-pulsed, and injection-seeded Ti:sapphire lasers operating at a pulse repetition frequency of 30 Hz and wavelengths of 867 and 900 nm, with M2 of 1.3, have been experimentally demonstrated and their properties compared with model results. The output pulse energy was 115 mJ at 867 nm and 105 mJ at 900 nm, with a slope efficiency of 40% and 32%, respectively. At these energies, the beam quality was good enough so that we were able to achieve 30 mJ of ultraviolet laser output at 289 and 300 nm after frequency tripling with two lithium triborate nonlinear crystals. 相似文献