磁控溅射CuCrMo薄膜耐126kV 20kA电弧烧蚀性能

提升真空断路器CuCr触头的抗电弧烧蚀能力是决定其能否应用于高压真空灭弧室的核心关键,尚未见有效触头材料或表面涂层改性技术使CuCr触头应用于126kV以上真空灭弧室的报道。基于CuCrMo薄膜的优异电气性能,对沉积CuCrMo薄膜的真空灭弧室触头进行126kV下的抗电弧烧蚀研究,并进行开断寿命的工程验证。采用磁控溅射技术在CuCr50真空触头片表面沉积5μm厚的CuCrMo薄膜,对其进行126kV 20kA电流下23次的电寿命试验。利用XRD、SEM和3D共聚焦显微镜研究电弧烧蚀后表面形貌。研究结果表明：沉积CuCrMo薄膜的触头片,在纵向磁场和126kV 20kA条件下可有效分散电弧,较未镀膜触头片有更小电弧电流密度;经过23次电寿命试验后,表面烧蚀程度比未镀膜的触头片轻,表面粗糙度降低,提高了触头的开断寿命。为表面改性真空断路器CuCr触头在高电压大电流真空灭弧室的应用提供了有效工程依据。     

Investigation of microstructure and mechanical properties of multi-layer Cr/Cr2O3 coatings

Single and multi-layer Cr/Cr₂O₃ coatings were deposited by reactive magnetron sputtering with the total thickness of 7 μm on steel substrates. X-ray diffraction analysis showed that single and multi-layer Cr/Cr₂O₃ coatings have different preferred crystal orientations. Columnar microstructure was detected by transmission electron microscopy both in metal chromium and ceramic chromium oxide layers. Grain size increased with the coating thickness. The value of single and multi-layer coating's fracture toughness is between 4 and 6 MPa·m^1/2 measured with the Berkovich tip indentation, and it is between 2.8 and 3.9 MPa·m^1/2 when measured with the Vickers indenter. The adhesion is about 192.1 and 246.7 J/m² for single and multi-layer coatings, respectively.     

A prediction method for fatigue life of large moving components as function of scale factor: A case of motor‐generator rotor

With the development of science and technology, more and more large moving components have been used in industry, and their service lives have become an important issue. After analysis of the previous results, considering the scale factor, a prediction method for fatigue life of large moving components based on the Basquin relation was proposed at first, and then the magnet pole part of motor‐generator rotor was chosen to make simulation parts with different scale factors mainly in terms of their S‐N curves and fractographies. It was found that with the change of specimen scale factor, the stress concentration factor at transition arc is almost unchanged as well as the fatigue strength exponent, and the fatigue strength coefficient changes linearly. Based on those results, a life prediction method was validated, and the results show that this method is a simple but more precise relation. After fatigue fracture surface and crack growth angle observations and quantitative analyses, the fatigue damage mechanisms associated with the relation among fatigue strength exponent and coefficient and scale factors were explained well. Those studies will provide a new clue to the prediction of the service life for those large moving components.     

武器维修器材包装系列研究(1):研究情况概述

介绍武器维修器材包装系列研究的主要技术成果。该成果运用系统工程原理,从整个器材流通过程出发,通过全面、深入的研究,使器材包装融生产、运输、储存、管理、供应、使用为一体,为器材包装的通用化、系列化、标准化奠定了基础。     

储油缸塑件圆周抽芯注射模设计

分析了储油缸的塑件工艺特点,主要分析了点浇口注射模成型且带侧向抽芯机构制品的工艺特点．介绍了带转盘的注射模结构,为保证外观质量,综合地处理好产品外观要求与浇口位置及脱模方式之间的问题,简化模具结构,减低制造成本,提高了生产效率。     

Microwave Absorption of Crystalline Fe/MnO@C Nanocapsules Embedded in Amorphous Carbon

Crystalline Fe/MnO@C core–shell nanocapsules inlaid in porous amorphous carbon matrix(FMCA)was synthesized successfully with a novel confinement strategy.The heterogeneous Fe/MnO nanocrystals are with approximate single-domain size which gives rise to natural resonance in 2–18 GHz.The addition of MnO2 confines degree of graphitization catalyzed by iron and contributes to the formation of amorphous carbon.The heterogeneous materials composed of crystalline–amorphous structures disperse evenly and its density is significantly reduced on account of porous properties.Meanwhile,adjustable dielectric loss is achieved by interrupting Fe core aggregation and stacking graphene conductive network.The dielectric loss synergistically with magnetic loss endows the FMCA enhanced absorption.The optimal reflection loss(RL)is up to−45 dB,and the effective bandwidth(RL<−10 dB)is 5.0 GHz with 2.0 mm thickness.The proposed confinement strategy not only lays the foundation for designing high-performance microwave absorber,but also offers a general duty synthesis method for heterogeneous crystalline–amorphous composites with tunable composition in other fields.     

青岛和大连海区海带(Laminaria japonica)外生细菌的16S rRNA基因序列分析

从采集自青岛和大连的大型褐藻海带(Laminaria japonica)表面分离到22株革兰氏阴性海洋细菌。根据16SrRNA基因序列分析结果,将其分别鉴定为假交替单胞菌(Pseudoalteromonas,Cobetia)菌,嗜冷单胞菌(Psychromonas),交替单胞菌(Alteromonas),产碱杆菌(Alcaligens)和海杆菌(Marinobacter)。其中假交替单胞菌在两地样品中占据绝对优势,但每个产地的假交替单胞菌不能单独聚类在一起,不同海区的海带表面存在遗传关系非常接近的菌株。假交替单胞菌之外的其他菌株于两地样品之间存在种或属水平上的差异。本文结果提示外生细菌的种类既与环境相关,又受宿主的状况影响。对8株受试菌株的拮抗实验结果显示了外生细菌在寻找新型抗生素方面的潜力。     

高吸油性树脂的合成及性能研究

采用悬浮聚合法合成了低交联度的聚甲基丙烯酸酯高吸油性树脂，研究了交联剂用量、单体配比、反应温度和时间等对树脂性能和反应的影响，确定了合适的聚合工艺条件。     

Synthesis, characterization and osteoconductivity properties of bone fillers based on alendronate-loaded poly(ε-caprolactone)/hydroxyapatite microspheres

A superior drug controlled release system capable of achieving efficient osteogenesis is in imperative demand because of limited bone substitute tissue for the treatment of bone defect. In the present study, we investigated the potential of using poly(ε-caprolactone)–hydroxyapatite (PCL–HA) composite microspheres as an injectable bone repair vehicle by controlled release of alendronate (AL), a medicine that belongs to the bisphosphonates family. The PCL/HA–AL microspheres were prepared with solid/oil/water emulsion technique, which included two processes: (1) AL was loaded on the hydroxyapatite nanoparticles; (2) the HA–AL complex was built in the PCL matrix. The spherical PCL/HA–AL microspheres were characterized with its significantly improved encapsulation efficiency of hydrophilic AL and better sustained release. Human bone mesenchymal stem cells (hMSCs) were cultured on the surface of these microspheres and exhibited high proliferative profile. Specifically, in osteogenic medium, hMSCs on the surface of PCL/HA–AL microspheres displayed superior osteogenic differentiation which was verified by alkaline phosphatase activity assay. In conclusion, by presenting strong osteogenic commitment of hMSCs in vitro, the PCL/HA–AL microspheres have the potential to be used as an injectable vehicle for local therapy of bone defect.