High-yield synthesis of single-crystalline 3C-SiC nanowires by a facile autoclave route

Single-crystalline 3C-SiC nanowires have been synthesized in large scale through a one-step autoclave route by the reaction of SiCl₄, (C₅H₅)₂Fe and metallic Na at 500 °C. Electron microscopy investigations show that the nanowires have typical diameters of 15-50 nm, lengths up to several tens of micrometers and grow along the [111] direction. The possible growth mechanism of the nanowires is discussed.     

静压下ZnS：Te中Te等电子陷阱的发光

研究了4块ZnS：Te薄膜样品(Te组分从0．5％到3．1％)的光致发光谱在常压下的温度特性．对于Te组分较小的2块样品观察到2个发光峰，分别来自Te1和Te2等电子陷阱；而对Te组分较大的2块样品则只观察到1个来自Te2等电子陷阱的发光．我们还研究了这些发光峰在低温1．5K下的流体静压压力行为．观察到与Te1有关的发光峰压力系数比ZnS带边的要大很多，而与Te2有关的发光峰压力系数则比带边小．根据Koster-Slater模型，价带态密度半宽随压力的增加是Te1中心有较大压力系数的主要原因，而Te1和Te2中心的不同压力行为则是由于压力对两者缺陷势增强的不同效果引起的．     

利用煤化工艺设备对洗油深加工

利用工业萘生产装置 ,在工业萘生产的空余时间 ,对洗油进行深加工 ,制取工业萘及甲基萘等产品 ,实现一套装置的多种使用 ,提高企业经济效益     

溶胶-凝胶生物玻璃多孔材料显微结构和生物活性的扫描电镜及红外光谱分析

本文利用溶胶．凝胶法制备了CaO-P2O5-SiO，系统生物活性玻璃，并以其为原料制备了用于骨修复及骨组织工程支架的块状生物活性材料。利用体外实验方法(invitro)结合x射线衍射(XRD)、扫描电子显微镜(SEM)和傅立叶变换红外光谱分析(FTIR)技术对不同烧结工艺制备的材料结构、晶相和生物活性的影响进行了分析研究。研究表明，经800℃和1100℃烧结5min的两种材料均有硅磷酸钙Ca5(PO4)2SjO4微晶相析出。烧结温度越高，析出微晶相的体积比例越大，材料的生物活性则越低。在模拟生理溶液中碳酸羟基磷灰石(HCA)只在烧结体中的玻璃颗粒表面形成，而在其硅磷酸钙Ca5(PO4)2SiO4微晶相表面未发现HCA形成。     

东方红浆砌石重力坝扬压力安全评价

东方红水库大坝是一座运行近40a的浆砌石重力坝，坝体裂缝、坝体渗漏及坝体碳化严重，扬压力有逐年增高的趋势。本文利用坝基扬压力测压管水位观测资料建立了测压管水位的统计模型，并结合现场渗漏实测流量资料建立了渗流反分析模型，详细分析了坝基的渗流性态和扬压力状态，并对其渗流性态做出安全评价。     

稀土混合物水溶液中囊泡的形成

依据柠檬酸的螯合作用和乙二醇的空间位阻效应，获得了稀土混合物囊泡。并利用ＩＣＰ、ＴＥＭ、ＦＳ等仪器对囊泡的性能进行了研究，最后对囊泡的形成机理进行了讨论。     

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本文通过对在用钻机井架的现场实际测试,建立数据库、测评模型,对实测的数据用计算机技术进行分析,提出了初始弯曲应力;数据正态分布检验——x～2检验;建立回归方程;在给定置信度下测评当前承载能力的技术概念。解决了在用钻机A型井架的安全性评估问题,是一种较为合理、可靠、科学的测评技术和方法。     

Spatial memory deficits following stimulation of hippocampal 5-HT1B receptors in the rat

The authors review the principles of reconstructive surgery for lower limb salvage after severe lower limb trauma to determine factors that have been used as decision-making criteria for limb salvage or amputation in severe lower extremity injuries and the methods of reconstruction and their outcome. The use of scoring systems and their value in acute decision making (primary amputation or limb salvage) are described. Soft-tissue reconstructive techniques, with emphasis on the use of flaps and the importance of selecting the best technique and time for the reconstruction are reviewed. Skeletal reconstructive techniques are described, including available options and currently held views on indications and use of the best contemporary methods. It is essential for the physician to make a good initial decision on the need for primary amputation or limb salvage. A multidisciplinary approach is fundamental to successful salvage.     

Simple ASK transmitter using a 790 nm self-pulsating laser diodefor local area networks

A simple amplitude shift keying (ASK) optical link is demonstrated by using a low-cost self-pulsating laser diode and an envelope detector for a low-cost broadband local area network. A link sensitivity of -22 dBm was achieved at 200 Mbit/s. Because the self-pulsation frequency can be tuned by the bias current, frequency division multiplexing can be simply implemented for multiuser applications     

粉煤灰对碾压混凝土抗裂的影响分析

粉煤灰在混凝土中的作用举足轻重，该文主要从水泥脆性系数、弹性模量、温度、混凝土干缩及徐变等角度，分析了粉煤灰对碾压混凝土的抗裂影响。