用SY87721实现城域网波分复用系统的多业务接入

为了使城域网的DWDM（密集波分复用）系统可以接入多种信号速率和格式，以满足用户的要求，首先介绍了一种波长转换板的设计方法，使用SY87721自适应提取28Mbit／s～2.7Gbit/s之间任意速率信号的时钟，其次介绍了SY87721提取时钟的工作原理、与单片机和CPLD（复杂可编程逻辑器件）的接口方式、对寄存器的配置和读出方式。最后介绍了使用参考时钟测量接入信号频率的方法，这会在系统维护时带来较大的方便。     

An efficient purification method for detonation nanodiamonds

This article reports the purification process of detonation soot to obtain pure nanodiamond powder. Nanodiamonds are synthesized by detonation using a high explosive mixture composed of trinitrotoluene and hexogen. The detonation of the charge leads to a powder containing nanodiamonds as well as metallic impurities and sp² carbon species. Further, to remove metallic particles, an unusual acidic treatment (hydrofluoric/nitric acids; i.e. fluorinated aqua regia) was set up. To eliminate sp² carbon species such as graphite and amorphous carbon, a thermal oxidation treatment was performed at 420 °C under air in a furnace during several hours. Transmission Electronic Microscopy, Raman spectroscopy, X-ray diffraction and Thermo-Gravimetric Analysis showed that this purification process is very efficient. From TGA measurements, a model of the carbon grain combustion was developed by considering graphitic shells surrounding the nanodiamond particles, and was used to demonstrate that the selective oxidation of graphite was experimentally realistic. Moreover, another model was set up from specific area measurements to evaluate the thickness of the functional groups surrounding the nanodiamonds after the oxidation of sp² carbonaceous species. The treatment described herein was achieved on several tens of grams of product and could be easily adapted to the industrial scale.     

Further observation of leucocyte migration through the endothelium of venules in the posterior latissimus dorsi muscle of the quail-chick spinal cord chimeras

The migration of leucocytes through the walls of venules was examined in detail in the posterior latissimus dorsi muscle of quail-chick spinal cord chimeras, in which flaccid paralysis of the wings was observed. Examinations were made from the 70th to 80th day after hatching. Muscle fibers were degenerated and intramuscular nerve bundles destroyed. Massive leucocytes (almost lymphocytes) were found around the venules, depending on the passage of wandering leucocytes through the endothelium. Lymphocytes penetrated and were encased in the cytoplasm of the venular endothelial cell, and did not pass through the interendothelial junction. These findings suggest that, in the venules of the atrophied chimeric muscle, wandering leucocytes in the blood may pass through the endothelial cell body and migrate into the inflamed extravascular space.     

Tests of electric and electromagnetic methods in the travale geothermal field

Within the framework of an EEC project involving ten European laboratories, research on the application of several electric and electromagnetic methods to a geothermal field (Travale, Tuscany), has been undertaken by the B.R.G.M. The objective was to refine the conceptual model of the Travale field and, therefore, to describe the morphology of the basement (down to 2 km depth) and of the Rhaetian reservoir covered by impermeable series.The method best suited to this type of prospection appeared to be electrical dipole — dipole profiling, combined with a 2-D interpretation. Contrasts at more than 2 km depth (500 m long dipoles) could be seen and compared to the depths measured in the boreholes. The EM Melos method (Syscal equipment) should be improved (lower frequencies) to increase the depth penetration. It is, however, a good complementary method for the surface layers. An attempt at a computational interpretation of the self potential profiles gave promising results. To make full advantage of the bipole — dipole measurements efforts should be devoted to their computational interpretation.     

Development of high-performance liquid chromatography criteria for determination of grades of commercial olive oils. Part I. The normal ranges for the triacylglycerols

Criteria for authentic olive oils were developed from isocratic high-performance liquid chromatography analyses of 99 olive oils from the major Mediterranean producers in the 1983–1986 crop years. Authentic olive oils include extra virgin, virgin and pure or refined oils, but exclude all reesterified and adulterated oils. The extra virgin through pure grades will have a combined area for the LOO (C_18:2C_18:1C_18:1), LOP (C_18:2C_18:1C_16:0), OOO (C_18:1C_18:1C_18:1), POO (C_16:0C_18:1C_18:1), POP (C_16:0C_18:1C_18:1), and SOO (C_18:0C_18:1C_18:1) peaks between 82.0 and 92.6% of the total area (L, linoleic; O, oleic; P, palmitic; S, stearic). Authentic oils will have ratios of LOO/LOP and OOO/POO that coincide with a line defined by OOO/POO=0.7844(LOO/LOP)+0.0968; correlation coefficient is 0.885. Authentic oils will not have a trilinolein (LLL) peak over 0.5% in area. Neither triolein (OOO) nor any other single peak suffices to characterize an olive oil sample as one of the authentic grades.     

Polymer electrolytes

Summary The room temperature conductivity of lithium salts dissolved in polyethylene oxide, proposed as polymer electrolytes, is shown to decrease drastically upon storage. The crystallization process, which is responsible for that ageing, can be blocked, if two further components are added : an elastomer copolymer butadiene-acrylonitrile and a macromer of polyoxyethylene. In addition, a crosslinking process must be carried out.     

Characterisation of inelastic power-law fluids using falling sphere data

Two simple methods are presented for the characterization of inelastic power law fluids from falling sphere data. The methods involve the application of shear rate or shear stress correction factors which have been derived theoretically using Slattery's solution for creeping flow about spheres. Flow curves obtained using these methods are in excellent agreement with those measured on a Weissenberg rheogoniometer for 0.83 ≤ n ≤ 1.0. The experimentally determined drag coefficients are found to be in good agreement with the predictions of Slattery's creeping flow first approximation solution. The wall correction factors of Faxen and Francis appear to be valid for inelastic non-Newtonian fluids up to a diameter ratio of at least 0.08.