氧化淀粉变性基团的分析方法

介绍了淀粉工业中氧化淀粉变性基团羧基和羰基的测定方法     

Étude expérimentale du mélange réactif au sein d'un réacteur torique ondulé (RTO)

Reactive mixing in a wavy torus reactor (WTR) has been examined experimentally. Its performances are compared to these of two other reactors: a plane torus reactor (PTR) and a baffled stirred tank reactor (BSTR). hydrodynamics of mixing has been studied using a plug flow model with axial dispersion for the WTR and PTR. The effect of axial dispersion on the kinetic of a chemical reaction was then analysed for the WTR, PTR and BSTR. Mixing times were slightly longer for the WTR due to a weaker axial dispersion. We also noticed an improvement of the convertion rate for low dissipated power.     

Al ionic radius influence on molecular dynamics simulations ofγ-Al2O3

Molecular dynamics (MD) simulations of-Al₂O₃, using a pairwise additive interaction potential of Pauling's type with four different radii for aluminum atoms, were analysed in order to determine the influence of the radius on the modification of coordination numbers of A1 relative to the ideal structure, at two different temperatures of 300 and 1500 K. It is found that the best choice is the radius of penta-coordinated aluminum, reproducing structural and vibrational properties of the compound in excellent agreement with experimentally observed properties.     

塔里木河干流人工与天然绿洲转化及适宜比例研究

利用1990,2000,2010年3期Landsat TM/ETM遥感影像,基于RS/GIS技术,分别提取土地利用/覆被类型信息,分析1990~2010年塔里木河流域人工绿洲和天然绿洲的变化规律及其比例,探讨该区人工绿洲和天然绿洲的适宜配比。研究结果表明:(1)1990~2010年,研究区域人工绿洲呈不断扩张,天然绿洲面积不断缩小,人工绿洲替代天然绿洲的趋势。(2)1990~2010年,人工与天然绿洲总面积几乎无差异,面积变化主要是人工绿洲与天然绿洲之间的相互转换。具体表现为:天然草地、林地等向人工绿洲中的耕地、建筑用地转化;同时植被长势衰退:高覆盖草地向中、低覆盖草地转化,中覆盖草地向低覆盖草地转化,灌木林地逐渐退化为草地,低覆盖草地向沙漠转化。(3)人工与天然绿洲面积比例在近20 a呈增加的趋势,在1990,2000,2010年,人工与天然绿洲面积比值分别是1∶9,2∶8,3∶7。     

湿法制造热塑性片材的工艺技术研究Ⅰ.热塑性片材概论

本文介绍了玻璃纤维毡增强热塑性片材（GMT）的特点，分类及制造工艺；阐述了湿法即介质悬浮法制造热塑性片材的工艺流程及专用设备。     

Random Forests with ensemble of feature spaces

Random Forests receive much attention from researchers because of their excellent performance. As Breiman suggested, the performance of Random Forests depends on the strength of the weak learners in the forests and the diversity among them. However, in the literature, many researchers only considered pre-processing of the data or post-processing of the Random Forests models. In this paper, we propose a new method to increase the diversity of each tree in the forests and thereby improve the overall accuracy. During the training process of each individual tree in the forest, different rotation spaces are concatenated into a higher space at the root node. Then the best split is exhaustively searched within this higher space. The location where the best split lies decides which rotation method to be used for all subsequent nodes. The performance of the proposed method here is evaluated on 42 benchmark data sets from various research fields and compared with the standard Random Forests. The results show that the proposed method improves the performance of the Random Forests in most cases.     

Large-scale SRAM-based IP lookup architectures using compact trie search structures

SRAM-based pipelined architectures for high-speed IP lookup using Field Programmable Gate Arrays (FPGAs) has recently attracted a great deal of attention from researchers. Due to the limited amount of on-chip memory and the number of I/O pins of FPGAs, compact data structures providing high memory efficiency are in great demand.     

润滑油调和数学模型的建立与应用

分析了南阳石蜡精细化工厂的基础油用阿伦尼乌斯公式计算的粘度数值与实测粘度数值的关系,对其系数进行校正,成功得出了精确度较高的润滑油调和数学模型,并经现场应用,证明可用于生产中.     

Silica Nanoboxes as New Nano-structured Materials: Their Secondary Synthesis from Alumina-Rich Zeolites

Novel silica nanoboxes were prepared by controlled dealumination of Na-X and Ca-A type zeolites using ammonium hexafluorosilicate (AHFS). The silica-richer the parent zeolite, the smaller the average pore size produced and the narrower the pore size distribution obtained. This was due to the specific reactivity of the extracting agent with the zeolite framework aluminum atoms. High temperature calcination of the dealuminated X-zeolite (ammonium form) resulted in mesoporous materials exhibiting an ink-bottle shape, a quite high surface area (330 m²/g, no micropores), an average pore diameter of 4.5 nm with a quite narrow pore size distribution (± 1.0 nm) and finally, a pore opening diameter of 3.9 nm. The latter was determined by using the nitrogen sorption isotherms (BET technique) and related pore volume data. The sorption behavior also suggested the interconnecting character of the newly created nanoboxes. The periodicity of these nanoboxes throughout the mesoporous material was clearly shown by X-ray powder diffraction at very small angles. These materials, herein called monomodal nanoboxes because of the absence of micropores in the structure, were also thermally stable. Incorporation of orthosilicate into the obtained silica nanoboxes, in accordance with the recently developed technique for pore size engineering in zeolites, led to materials with smaller pore openings but having almost the same textural properties. Solid superacidic materials were prepared by incorporating a liquid superacid (triflic acid or trifluoromethanesulfonic acid) into the silica nanoboxes using the wet impregnation technique. The maximum triflic acid loading which did not significantly affect the mesoporous framework of the materials was 24 wt%. As a reference, the maximum loading of less acidic sulfuric acid was slightly lower. All this showed the high chemical stability of the silica nanoboxes for supporting very acidic species. Temperature-programmed desorption using a combined DTA/TGA system allowed the identification of the bound phases and some liquid phase of the loaded triflic acid.     

Development of high-performance liquid chromatography criteria for determination of grades of commercial olive oils. Part I. The normal ranges for the triacylglycerols

Criteria for authentic olive oils were developed from isocratic high-performance liquid chromatography analyses of 99 olive oils from the major Mediterranean producers in the 1983–1986 crop years. Authentic olive oils include extra virgin, virgin and pure or refined oils, but exclude all reesterified and adulterated oils. The extra virgin through pure grades will have a combined area for the LOO (C_18:2C_18:1C_18:1), LOP (C_18:2C_18:1C_16:0), OOO (C_18:1C_18:1C_18:1), POO (C_16:0C_18:1C_18:1), POP (C_16:0C_18:1C_18:1), and SOO (C_18:0C_18:1C_18:1) peaks between 82.0 and 92.6% of the total area (L, linoleic; O, oleic; P, palmitic; S, stearic). Authentic oils will have ratios of LOO/LOP and OOO/POO that coincide with a line defined by OOO/POO=0.7844(LOO/LOP)+0.0968; correlation coefficient is 0.885. Authentic oils will not have a trilinolein (LLL) peak over 0.5% in area. Neither triolein (OOO) nor any other single peak suffices to characterize an olive oil sample as one of the authentic grades.