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排序方式: 共有732条查询结果,搜索用时 203 毫秒
11.
Alok Singh Sitaram Dash Mohammed Kamruddin Puthupparampil K. Ajikumar Ashok K. Tyagi Vinjamoor S. Raghunathan Baldev Raj 《Journal of the American Ceramic Society》2002,85(4):927-932
Formation of nanocrystalline calcia from calcite has been studied in situ via transmission electron microscopy. The crystallographic transformation occurred via two mechanisms: the first is by distortion of the cleaved rhombohedron of calcite, formed by {104} planes in hexagonal coordinates, into a cube. This produced a microstructure of oriented, elongated nanocrystals of calcia with planar boundaries. In the second mechanism, the micrometer-sized parent calcite particles broke up into nano-sized grains as the decomposition began, leading to irregularly shaped, randomly oriented nanocrystals of calcia. 相似文献
12.
Reena Rao S. Divakar Belur R. Lokesh 《Journal of the American Oil Chemists' Society》2002,79(6):555-560
The preference of lipase (EC 3.1.1.3) from Rhizomucor miehei in the incorporation of 11 FA, ranging from C10∶0 to C22∶6, into coconut oil TAG during acidolysis was studied by applying
the Plackett-Burman experimental design. Enzymatic acidolysis reactions were carried out in hexane at 37°C for 48 h with coconut
oil (0.1 M) and a mixture of 11 FA at a TAG to FA molar ratio of 1∶1. Lipase was used at the 5 wt% level. The incorporation
of FA into coconut oil TAG was determined by GC. The lipase showed preference for long-chain saturated FA for incorporation
into coconut oil TAG. The FA with 18 carbon atoms showed a high incorporation rate (18∶1>18∶1>18∶3). The lipase showed the
least preference for the incorporation of 12∶0, which occurs in maximal concentration (46%), whereas the most preferred FA,
18∶0, occurs at a very low concentration (<2%) in coconut oil. The overall preference of lipase for the incorporation of different
FA into coconut oil TAG was 18∶0>18∶2, 22∶0>18∶1, 18∶3, 14∶0, 20∶4, 22∶6>16∶0>12∶0≫10∶0. 相似文献
13.
14.
Wireless Personal Communications - Wireless Sensor Networks (WSNs) are used to collect and transmitted the data in various applications from normal to those which requires significant security... 相似文献
15.
Nitin Sharma Shanu Tyagi Satish Kumar Gupta Giriraj Thirupathirao Kulkarni Aseem Bhatnagar Neeraj Kumar 《Drug development and industrial pharmacy》2016,42(11):1763-1771
Objective: This work describes the application of natural plant polysaccharide as pharmaceutical mucoadhesive excipients in delivery systems to reduce the clearance rate through nasal cavity.Methods: Novel natural polysaccharide (Hibiscus rosasinensis)-based mucoadhesive microspheres were prepared by using emulsion crosslinking method for the delivery of rizatriptan benzoate (RB) through nasal route. Mucoadhesive microspheres were characterized for different parameters and nasal clearance of technetium-99m (99mTc)-radiolabeled microspheres was determined by using gamma-scintigraphy.Results: Their Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD) studies showed that the drug was stable during preparation of microspheres. Aerodynamic diameter of microspheres was in the range 13.23?±?1.83–33.57?±?3.69?µm. Change in drug and polysaccharide ratio influenced the mucoadhesion, encapsulation efficiency and in-vitro release property. Scintigraphs taken at regular interval indicate that control solution was cleared rapidly from nasal cavity, whereas microspheres showed slower clearance (p?0.005) with half-life of 160?min.Conclusion: Natural polysaccharide-based microspheres achieved extended residence by minimizing effect of mucociliary clearance with opportunity of sustained delivery for longer duration. 相似文献
16.
Friction and scuffing behaviour of grey cast iron as influenced by the surface roughness under sparse lubrication conditions is studied. The studies are carried out on a three-shoe-on-disc machine under the conditions of parallel sliding. The experiments were conducted at three oil supply rates of 0.10, 0.22 and 0.36 μg/cm2 per contact obtained through a mist oiling system and with specimens of cast iron shoes of different roughness values, Ra, between 0.04 and 2.0 μm against a 0.55% C steel disc. In a step load procedure, the friction torque at the end of each load step and the scuffing load are the major parameters measured. Results of friction and scuffing behaviour as a function of roughness and oil supply rates have been discussed. 相似文献
17.
R. K. Tyagi K. K. Srivastava R. S. Pandey 《Surface Engineering and Applied Electrochemistry》2012,48(1):64-68
The material removal within different machining process can be performed in distinct modalities. One of the modality is based
on the effect of impact phenomenon. In this paper theoretical model of non-traditional machining process based on impact phenomenon
is discussed. The material is removed from the surface due to the impact of ions. The velocity of ions is equal to the velocity
at which the electrostatic ion-cyclotron instability driven by parallel flow velocity shear generated by massive ions takes
place. The main ways for the material removal as consequence of the impact phenomenon are the microcracking, microcutting,
melting and vaporizing of small quantities from the work-piece surface layer. 相似文献
18.
Gaurav Sharma Lokesh Tiwari Dheerendra Kumar Dwivedi 《Transactions of the Indian Institute of Metals》2018,71(1):11-21
In the present study, impulse pressure assisted diffusion bonding of low carbon steel was carried out using silver interlayer. To study the influence of input process parameters namely bonding temperature (T), maximum pulse pressure (P), and number of pulses (N), experiments of diffusion bonding were conducted according to the Taguchi L9 orthogonal array. To reveal the typical bond interface characteristics, selected samples were examined by scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS). The EDS analysis revealed a diffusion affected zone at the interface due to the diffusion of silver and iron across the interface. Lap joints were developed to measure the shear strength of the diffusion bonds. The optimum level of bonding temperature, maximum pulse pressure and number of pulses (875 °C, 10 MPa and 10 pulses) were identified. The ANOVA results indicated that bonding temperature had the highest statistical effect of 66.37% on shear strength followed by number of pulses and maximum pulse pressure. The fracture surface of the lap joints was also examined by FESEM and X-ray diffraction analysis. 相似文献
19.
Anshu Tyagi Florian Döring Hans-Ulrich Krebs Astrid Pundt 《International Journal of Hydrogen Energy》2017,42(35):22575-22582
The influence of a thin polycarbonate de-adhesion layer on the hydrogen concentration is studied on 30 nm vanadium films deposited on glass substrates, using electrochemical hydrogenography in an optical microscopy and scanning tunneling microscopy. It is shown that the optical reflection provides information about the de-adhesion morphology (buckles) while the optical transmission signal gives information about concentration and film thickness changes. Artificially patterned samples allow simultaneous studying adhered and de-adhered film parts, for similar mean concentrations. The optical data clearly show a different hydrogen behavior of the two parts. Data interpretation suggests higher local hydrogen content in the adhered film parts than for the detached films parts. Strong changes in the optical transmission of the adhered film parts can be attributed to strong morphological changes at the film surface. These changes are mainly attributed to grain sliding processes in the vanadium film. 相似文献
20.
Raman K. Mishra Vasanthakumaran Sudarsan Savita Jain Chetan P. Kaushik Rajesh K. Vatsa Avesh K. Tyagi 《Journal of the American Ceramic Society》2014,97(2):427-431
Barium sodium borosilicate glasses containing different amounts of uranium oxides were prepared by conventional melt quench method and investigated for their structural aspects by 29Si and 11B MAS NMR technique combined with steady‐state luminescence and lifetime measurements. Based on MAS NMR studies, it is confirmed that uranium ions act as network modifier up to 15 wt% and beyond which a separate uranium containing phase is formed. From the luminescence studies, it is inferred that uranyl species is in a highly distorted environment. For more than 15 wt% uranium oxide incorporation, weaker U–O–U linkages are formed at the expense stronger U–O–Si/B linkages, as suggested by the excited state lifetime value of the uranyl species as well as red shift in emission peak maximum. For glass samples containing more than 25 wt% uranium oxides, crystalline barium uranium silicate gets phase separated from glass matrix as confirmed by XRD studies. 相似文献