矿山企业网络信息系统中Intranet技术的实现

分析了Intranet技术在建设矿山企业网络信息系统中所具有的独特优势,并介绍了Intranet的信息交换技术在矿山企业网络信息系统中应用的一种具体实现方法,以期能为正在筹建的矿山企业网络信息系统采用Intranet技术提供借鉴。     

Structural scheme and theory behind feedback compensation of new parallel machine tools

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A novel intelligent verification platform based on a structured analysis model

An intelligent verification platform based on a structured analysis model is presented.Using an abstract model mechanism with specific signal interfaces for user callback,the unified structured analysis data,shared by the electronic system level design,functional verification,and performance evaluation,enables efficient management review,auto-generation of code,and modeling in the transaction level.We introduce the class tree,flow parameter diagram,structured flow chart,and event-driven finite state machine as structured analysis models.As a sand table to carry maps from different perspectives and levels via an engine,this highly reusable platform provides the mapping topology to search for unintended consequences and the graph theory for comprehensive coverage and smart test cases.Experimental results show that the engine generates efficient test sequences,with a sharp increase in coverage for the same vector count compared with a random test.     

飞行器与机器人的区域目标搜索最优控制

描述了飞行器导航或移动机器人的区域搜索控制问题.为了使该问题得到优化解决,首先建立了基于区域搜索控制问题的模型,将最优控制原理运用于此模型上,得到其伴随方程和控制方程,后基于此分析了该问题,且讨论了此方法的可行性.然后,通过解出问题的规范方程,使飞行器导航或移动机器人的区域搜索控制问题最终得以解决,进而推导得到了飞行器导航或移动机器人的区域目标搜索最优控制以及最优轨线.最后,通过计算仿真结果表明,该方法是有效的,故为飞行器导航与移动机器人的区域目标搜索最优控制提供了依据.     

原位插层聚合法制备聚苯乙烯/海泡石纳米复合材料

采用十八烷基三甲基氯化铵(OTAC)作为有机插层剂对海泡石进行了有机化处理,该有机化的海泡石粒子在苯乙烯单体中很容易地均匀分散并形成稳定的胶体溶液.通过对分散有海泡石的苯乙烯进行原位插层聚合制备了聚苯乙烯/海泡石纳米复合材料.并用X射线衍射(XRD)、傅里叶变换红外光谱(FT-IR)、扫描电镜(SEM)和透射电镜(TEM)对聚苯乙烯/海泡石复合材料的结构进行了表征.研究表明聚苯乙烯的大分子链插入到海泡石片层间,形成了部分插层、部分剥离型纳米复合材料.     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

电子台秤自动检定装置的新型检定砝码的设计

为了解决利用反向架方式来设计的最大称量为(30～150)kg的电子台秤自动检定装置的砝码的问题,深入分析了电子台秤自动检定装置所需砝码的要求,采用了机械腾空不接触的设计,设计了一套1g～10kg的M1等级的砝码用于电子台秤自动检定装置中,满足检定所需要求,且满足量值传递要求.     

Ultraviolet-visible and surface-enhanced Raman scattering spectroscopy studies on self-assembled films of ruthenium phthalocyanine on organic monolayer-modified silver substrates

A self-assembled film of ruthenium phthalocyanine (RuPc) fabricated on a silver substrate pre-modified with a monolayer of 4-mercaptopyridine (PySH) or 1,4-bis[2-(4-pyridyl)ethenyl]-benzene (BPENB) was studied by ultraviolet-visible (UV-Vis) and surface enhanced Raman scattering (SERS) spectroscopy. PySH or BPENB was used as a ligand to link RuPc since they not only modify the silver substrate, but also deliver a pyridyl group pointing out from the silver surface. Therefore, we can explore the relationship between the structure and orientation of metallophthalocyanine and the substrate modified by the two kinds of organic-monolayers with the different conjugates and molecular lengths. UV-Vis bands due to the organic-monolayer (PySH or BPENB) modified silver films shift to longer wavelengths and a new band arising from the metallophthlocyanine appears, suggesting the binding of RuPc to PySH/BPENB, as well as the interaction between the marcocycle of RuPc and the ring of PySH/BPENB. Vibrational bands arising from both the RuPc and PySH/BPENB moieties appear clearly in the SERS spectra of the RuPc-PySH/BPENB composite films, indicating that RuPc is successfully assembled on the top of PySH/BPENB film. The shifts and relative intensity changes of bands due to PySH or BPENB in the SERS spectra imply the binding of the metallophthalocyanine to the pyridyl group in the composite films. Furthermore, the comparison of the SERS spectra revealed that the orientations of PySH and BPENB in the two kinds of composite films are different; the BPENB moiety in the RuPc-BPENB composite film is more perpendicular to the silver surface compared with the PySH moiety in the RuPc-PySH composite film.     

Self-assembly synthesis of cactuslike Cu2O 3D nanoarchitectures via a low-temperature solution approach

Cu₂O nanocactuses were synthesized via a simple, low-temperature, and no time-consuming wet chemical route. The synthesized products were systematically studied by X-ray powder diffraction, scanning electron microscopy, and transmission electron microscopy. The results showed that the formation of Cu₂O nanocactuses was strongly depended on the addition of CTAB and NaOH. The structural evolution of the cactuslike Cu₂O was found to follow dissolution and recrystallization processes. It is noteworthy that the stepwise synthetic procedure was crucial to the growth of the final nanoarchitectures. UV–vis spectrum was also used to estimate the absorption and photodegradation ability of the nanocactuses.