镁钴铝类水滑石催化合成安息香甲醚

采用共沉淀法制备了镁钴铝类水滑石化合物(MgCoAl-HTLcs),并用 X 射线衍射、扫描电子显微镜、NH_3程序升温脱附等方法对 MgCoAl-HTLcs 进行了表征,并以 MgCoAl-HTLcs 为催化剂催化苯甲醛与甲醇反应合成安息香甲醚,研究了n(Mg):n(Co):n(Al)、催化剂用量、原料配比、反应温度、反应时间对合成反应的影响。表征结果显示,MgCoAl-HTLcs 的晶相完整,表面主要为弱酸、弱碱性。催化合成安息香甲醚的适宜条件为:MgCoAl-HTLcs 催化剂用量0.10 g(约为原料总质量的0.23%),n(Mg):n(Co):n(Al)=0.4:1.6:1.0,V(苯甲醛):V(甲醇)=3:50,反应温度50℃,反应时间150 min。在此条件下,苯甲醛的平衡转化率达77.49%,安息香甲醚选择性接近100%。为洁净合成安息香甲醚开辟了一条新的途径。     

Optimal and self‐tuning fusion Kalman filters for discrete‐time stochastic singular systems

Based on the optimal fusion estimation algorithm weighted by scalars in the linear minimum variance sense, a distributed optimal fusion Kalman filter weighted by scalars is presented for discrete‐time stochastic singular systems with multiple sensors and correlated noises. A cross‐covariance matrix of filtering errors between any two sensors is derived. When the noise statistical information is unknown, a distributed identification approach is presented based on correlation functions and the weighted average method. Further, a distributed self‐tuning fusion filter is given, which includes two stage fusions where the first‐stage fusion is used to identify the noise covariance and the second‐stage fusion is used to obtain the fusion state filter. A simulation verifies the effectiveness of the proposed algorithm. Copyright © 2008 John Wiley & Sons, Ltd.     

从关联分析法看如何改善沥青抗老化性能

用灰色关联分析法研究了沥青抗老化性能与沥青化学组成之间的关联程度，结果表明，影响再生沥青性质的主要因素是沥青中的芳烃和胶质的含量。通过添加芳香组分能改善沥青四组分之间的配伍性，从而可以改善再生沥青的抗老化性能。并通过对再生剂进行富芳处理，验证了上述结论。     

A novel distributed approach to robust fault detection and identification

In this paper, we propose a novel distributed robust fault detection and identification (RFDI) scheme for a class of nonlinear systems. Firstly, a detection and identification estimator—robust fault tracking approximator (RFTA) is designed for online health monitoring. A novel feature of the RFTA is that it can simultaneously detect and accurately identify the shape and magnitude of the fault and disturbance. Moreover, it takes less online training time compared with the traditional neural network based fault diagnosis schemes. For some distributed systems, a network of distributed estimators is constructed where the RFTA is embedded into each estimator. Then we use consensus filter to filter the outputs of each estimator. One of the most important merits of the consensus filter is that its outputs can dramatically improve the accuracy of fault detection and identification. Next, the stability of the distributed RFDI scheme is rigorously investigated. Finally, two numerical examples are given to illustrate the feasibility and effectiveness of the proposed approach.     

PVC树脂聚合用有机过氧化物引发剂

介绍了目前国内外引发剂的使用及开发方向,并对引发剂的选择及其对树脂质量的影响进行了讨论。     

一种采用单台微机控制的标签粘贴机

标签粘贴机是一种可自动进行标签打印和粘贴的设备装置,在工业自动化生产中有着广泛的应用.介绍了一种采用单台微机进行控制的全自动标签粘贴机的工作原理及各部分组成,以及使用过程中对其进行设置和调整的方法.该标签粘贴机已实际应用于华飞彩色显示系统有限公司29英寸彩色显像管生产线的屏网组装工序,取得了良好的效果.     

一种动态开关电容运算放大器共模负反馈电路

本文主要介绍了一种应用于Cascode结构运放中的开关电容共模负反馈电路，它具有稳定性好、对运放频率特性影响小、不消耗额外功率等优点。对电路运用Hspice进行了模拟，并给出了模拟结果。     

cdma1x无线子系统导频信道功率分配分析

分析了目前联通CDMA网络建设中的主要问题之一——导频功率分配问题。主要介绍了cdma 1x系统的信道类型，以及前向链路信道功率分配原则，并且对导频信道功率与无线网络覆盖和容量之间的关系进行了初步探讨。     

IPv6和基于IPv6的网络设计

对IPv6协议的主要内容进行了简要介绍,并针对IPv6的特点对基于IPv6的网络设计进行了探讨。     

透析3G在中国面临的重重困局(1)--牌照与标准选择

探讨了中国3G牌照何时发放、发放数量、牌照与标准是否捆绑、3G产业链如何搭建、频率如何分配、市场容量和终端等问题，并对此提出了建设性的意见。