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71.
Sara Amouzad Mehdi Khosravi Niaz Monadi Behzad Haghighi Suleyman I. Allakhverdiev Mohammad Mahdi Najafpour 《International Journal of Hydrogen Energy》2021,46(37):19433-19445
In this study, the effect of potassium hydroxide concentration in anodization bath, anodization time, and calcination temperature on the photo-electrochemical behavior of metallic titanium/mixed phase titanium oxide is investigated. Further, the phase structure of a titanium oxide photocatalyst prepared on a titanium electrode through a high-voltage anodization method is examined. The study exploits photo-electrochemical, Fourier transform infrared spectroscopy attenuated total reflectance (FTIR–ATR), X-ray diffraction, and Raman spectroscopic methods to obtain better insights into the mechanism of mixed-phase titanium oxide formation. In this regard, the photo-electrochemical properties of the photocatalysts prepared in single excitation energy, violet light (410 nm), were investigated. The anodization time and the potassium hydroxide concentration in the anodization bath have significant effects on the photo-electrochemical properties of the photocatalysts. The experiments show that the effect of potassium hydroxide concentration is a function of the anodization potential applied, demonstrating different patterns as the anodization potential changes. Furthermore, FTIR-ATR, X-ray diffraction, and Raman spectroscopic studies reveal that the extended anodization times decrease the population of OH-containing groups, leading to lower photo-electrochemical performance. On the other hand, the formation of anatase phases becomes more favorable only in the extended anodization times before application of the calcination process. Additionally, the calcination temperature has a significant impact on the anatase to rutile ratio. Finally, increasing potassium hydroxide concentration leads to the formation of an amorphous titanium oxide layer. It can be concluded that the obtained information might have a significant impact on the preparation of titanium oxide and other metal oxide photocatalysts through the high voltage anodization process. 相似文献
72.
Mahdi Norouzi Malihe Tahernejad Seyed Ghorban Hosseini Saeed Tavangar 《化学工程与技术》2020,43(11):2215-2223
The sphericity and size of ammonium perchlorate (AP) particles significantly influence the properties of composite propellants. As the AP particles become more spherical, the accumulation coefficient increases, the viscosity during casting decreases, and the particle loading and burning rate increase. Hence, the production of micronized AP particles with an average size between 1 and 20 μm is important to increase the loading percentage of AP in the composite propellant. Here, the Taguchi experimental design was used to optimize the solvent-antisolvent crystallization (SAC) process for the preparation of micronized AP particles with higher sphericity. SAC parameters such as the type of antisolvent, the solvent-to-antisolvent ratio, the antisolvent temperature, the stirring speed, and the retention time were investigated at four levels. The type of antisolvent and the solvent-to-antisolvent ratio were found to mainly contribute to improving the sphericity and size of the AP particles, respectively. 相似文献
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Mahdi Mohammadi Ghaleni Elham Tavakoli Mona Bavarian Siamak Nejati 《American Institute of Chemical Engineers》2020,66(11):e17019
Membranes with asymmetric wettability-Janus membranes-have recently received considerable attention for a variety of critical applications. Here, we report on a simple approach to introduce asymmetric wettability into hydrophilic porous domains. Our approach is based on the physicochemical-selective deposition of polytetrafluoroethylene (PTFE) on hydrophilic polymeric substrates. To achieve selective deposition of PTFE, we inhibit the polymerization reaction within the porous domain. We prefill the substrates with glycerol, containing a known amount of free radical inhibitor, and utilize initiated chemical vapor deposition (iCVD) for the polymerization of PTFE. We show that the glycerol/inhibitor mixture hinders the deposition of PTFE within the membrane pores. As a result, the surface of the substrates remains open and porous. The fabricated Janus membranes show stable wetting-resistant properties, evaluated through sessile drop contact angle measurements and direct contact membrane distillation (DCMD). 相似文献
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Water Resources Management - The present study develops a novel form of optimization framework to assess environmental flow in the reservoirs in which upstream and downstream river ecosystems and... 相似文献
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Combination of multiple diverse classifiers using belief functions for handling data with imperfect labels 总被引:1,自引:0,他引:1
Mahdi Tabassian Reza Ghaderi Reza Ebrahimpour 《Expert systems with applications》2012,39(2):1698-1707
This paper addresses the supervised learning in which the class memberships of training data are subject to ambiguity. This problem is tackled in the ensemble learning and the Dempster-Shafer theory of evidence frameworks. The initial labels of the training data are ignored and by utilizing the main classes’ prototypes, each training pattern is reassigned to one class or a subset of the main classes based on the level of ambiguity concerning its class label. Multilayer perceptron neural network is employed to learn the characteristics of the data with new labels and for a given test pattern its outputs are considered as basic belief assignment. Experiments with artificial and real data demonstrate that taking into account the ambiguity in labels of the learning data can provide better classification results than single and ensemble classifiers that solve the classification problem using data with initial imperfect labels. 相似文献
79.
Ali Hemmatifar Mohammad Said Saidi Arman Sadeghi Mahdi Sani 《Microfluidics and nanofluidics》2013,14(1-2):265-276
Dielectrophoresis (DEP) is an electrokinetic phenomenon which is used for manipulating micro- and nanoparticles in micron-sized devices with high sensitivity. In recent years, electrode-based DEP by patterning narrow oblique electrodes in microchannels has been used for particle manipulation. In this theoretic study, a microchannel with triangular electrodes is presented and a detailed comparison with oblique electrodes is made. For each shape, the behavior of particles is compared for three different configurations of applied voltages. Electric field, resultant DEP force, and particle trajectories for configurations are computed by means of Rayan native code. The separation efficiency of the two systems is assessed and compared afterward. The results demonstrate higher lateral DEP force, responsible for particle separation, distributed wider across the channel width for triangular shape electrodes in comparison with the oblique ones. The proposed electrode shape also shows the ability of particle separation by attracting negative DEP particles to or propelling them from the flow centerline, according to the configuration of applied voltages. A major deficiency of the oblique electrodes, which is the streamwise variation of the lateral DEP force direction near the electrodes, is also eliminated in the proposed electrode shape. In addition, with a proper voltages configuration, the triangular electrodes require lower voltages for particle focusing in comparison with the oblique ones. 相似文献
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