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951.
Different and alternative methods for the preparation of Ni/pillared clays based on impregnation and encapsulation procedures are reported. Several nickel precursors and metal loadings are considered in order to evaluate their influence on the structural, textural and catalytic properties of the resulting solids. The behaviour of the optimum solids as catalysts has been proved in the selective catalytic reduction of nitrogen oxides with propene, and the relevance of the oxidant nature was checked by changing the composition of the oxidant mixture. Of all the factors studied, the nature of the nickel precursors appears as the most important one, owing to the formation of different active nickel species during the synthesis procedure. 相似文献
952.
In this work, the kinetics and mechanism of free-radical polymerisation of glycidyl methacrylate (GMA) using potassium peroxydisulphate
(PDS) as water soluble initiator in the presence of synthesized 1, 4-Bis (tributyl methyl ammonium) benzene dichloride (TBMABDC)
as multi-site phase transfer catalyst (MPTC) was studied. The polymerisation reactions were carried out under inert and unstirred
conditions at constant temperature of 60 ± 1°C in cyclohexane/water biphase media. The role of concentrations of monomer,
initiator, catalyst and volume fraction of aqueous phase, solvent polarity and temperature on the rate of polymerisation (Rp)
was ascertained. The order with respect to monomer and initiator was found to be unity. The order with respect to catalyst
was found to be 0.51. The rate of polymerisation is independent of ionic strength and pH of the medium. However, an increase
in the polarity of solvent has slightly increased the Rp value. Based on the results obtained, a suitable kinetic scheme has
been proposed to account for the experimental observations and its significance discussed. 相似文献
953.
The specific features of SPPA-T3000, a new instrumentation and control system intended for automation of processes in power engineering, are briefly described. Distinctive features of the system architecture, central to which is using the model of web systems, are singled out. 相似文献
954.
The extraction of Te(IV) from aqueous solutions containing various ligands was studied using various inert organic diluents
and other solvents. The extraction was carried out from solutions of various mineral (HCl, HBr, HI, HNO3) and organic (citric, oxalic) acids of various concentrations. The organic phase was an inert diluent (cyclohexane, CCl4, chloroform, benzene, p-xylene, toluene, nitrobenzene) or a solution of 20 vol % Aliquat-336, 20 vol % trioctylamine, or 30 vol % TBP in p-xylene. A correlation between the distribution of Te(IV) and some physicochemical properties of the diluents and the possibility
of extraction separation radioactive Te isotopes and their daughters, i.e., radioactive I isotopes, were examined. In most
cases, the Te(IV) distribution ratio decreases in the order nitrobenzene > CHCl3 > CCl4 > p-xylene > benzene > toluene > cyclohexane.
Published in Russian in Radiokhimiya, 2007, Vol. 49, No. 4, pp. 353–358.
The text was submitted by the authors in English.
An erratum to this article is available at . 相似文献
955.
In this paper, we present a general method to calculate the inverse and direct dynamic models of parallel robots. The models
are expressed in a closed form by a single equation in which all the elements needed are expressed. The solution is given
in terms of the dynamic models of the legs, the dynamics of the platform and some Jacobian matrices. The proposed method is
applied in this paper on two parallel robots with different structures.
Categories (2), (3). 相似文献
956.
A new chromosome encoding method, named fuzzy coding, is proposed for representing real number parameters in a genetic algorithm. Fuzzy coding provides the value of a parameter on the basis of the optimum number of selected fuzzy sets and their effectiveness in terms of degree of membership. Thus, it represents the knowledge associated with each parameter and is an indirect method of encoding compared with alternatives, where the parameters are directly represented in the encoding. Fuzzy coding is described and compared with conventional binary coding, gray coding, and floating-point coding. Two test examples, along with neural identification of a nonlinear pH process from experimental data, are studied. It is shown that fuzzy coding is better than the conventional methods and is effective for parameter optimization in problems where the search space is complicated. 相似文献
957.
Finite sample properties of estimators of spatial autoregressive models with autoregressive disturbances 总被引:1,自引:0,他引:1
The article investigates the finite sample properties of estimators for spatial autoregressive models where the disturbance
terms may follow a spatial autoregressive process. In particular we investigate the finite sample behavior of the feasible
generalized spatial two-stage least squares (FGS2SLS) estimator introduced by Kelejian and Prucha (1998), the maximum likelihood
(ML) estimator, as well as that of several other estimators. We find that the FGS2SLS estimator is virtually as efficient
as the ML estimator. This is important because the ML estimator is computationally burdensome, and may even be forbidding
in large samples, while the FGS2SLS estimator remains computationally feasible in large samples.
Received: 20 January 2001 / Accepted: 31 August 2001 相似文献
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