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941.
Crystallization of hydrogenated sunflower-cottonseed oil 总被引:1,自引:0,他引:1
G. Rivarola J. A. Segura M. C. Añón A. Calvelo 《Journal of the American Oil Chemists' Society》1987,64(11):1537-1543
Crystal structures formed during solidification of hydrogenated cottonseed oil, sunflowerseed oil and their blends were analyzed
by using an X-ray diffraction technique, differential scanning calorimetry (DSC) and polarized light microscopy. Temperatures
and times of crystallization under conditions which tend to produce β′ type structures were determined in terms of refrigeration
parameters. Microscopy with polarized light also helped clarify some aspects of the tridimensional network of crystals that
contribute to the consistency of products made from hydrogenated oils. 相似文献
942.
943.
A series of new polyamides 3a–d containing aryl-azo, ether and sulfone groups in the main chain were synthesized from bis[4-(4-aminophenoxy)phenyl sulfone]
1 and several azo aromatic diacyl chlorides 2a–d by the low temperature solution polycondensation technique. FTIR spectroscopy, nuclear magnetic resonance (NMR) and elemental
analyses confirmed the structure of these polymers. Owing to the aryl and amide groups in the main chain, these polymers exhibit
photochromic properties as well as excellent thermal stabilities. The transition temperatures (T
g) are between 242 and 265 °C, and the char yields at 800 °C in nitrogen atmosphere were above 39%. Based on incorporation
of flexible ether linkages and polar sulfone groups, the polyamides show desirable solubility in organic solvents such as
DMAc, N,N-dimethylformamide (DMF), N-methyl-2-pyrroidinone (NMP) and dimethylsulfoxide (DMSO). And it is exemplified that
polyamide containing 2 and 2′ substitutes performed better solubility.
Funded by the National Natural Science Foundation of China (No. 50572081) 相似文献
944.
The tribological properties of perfluoro and non-perfluoro alkylsilane molecular films were investigated and compared detailedly.
Their surface properties were characterized by X-ray photoelectron spectroscopy (XPS), atomic force microscopy (AFM) and contact
angle (CA) measurement. A ball-on-disk tribometer was used to study the frictional properties of these alkylsilane monolayers.
The experimental results reveal that the alkylsilane molecular films are good candidates to decrease friction and they have
good capability to endure rigorous shear forces. Perfluoro alkylsilane molecular films are bonded better with the Si substrate
than the simple hydrocarbon ones. The effects of sliding velocity and normal load on friction coefficient are evident and
the friction coefficient increases with the increase of the sliding velocity. However, friction coefficient decreases with
the increase of normal load initially and then increases, indicating there exists a critical normal load for the load effect.
Funded by the National Natural Science Foundation of China (No.50730007 and 50805086), the Foundation of Tsighua Basic Research,
and the National Key Basic Research Program of China(No. 2007CB607604) 相似文献
945.
A micro-envioment for nerve cells and tissue growth were designed and constructed via surface modification of poly(L-lactide-co-glycolide)(PLGA)
with chitosan and hydroxyapatite(HA). The poly(L-lactide-co-glycolide)/chitosan/hydroxyapatite (PLGA/chitosan/HA) conduits
were manufactured by a combined solvent casting and particulate leaching technique. The conduits were highly porous with an
interconnected pore structure and 76.5% porosity. Micropores with 50–100 micrometer diameter were formed in the conduits.
In vivo application of PLGA/chitosan/HA conduits for reconstruction of 10 mm sciatic nerve defect was assessed by the walking
track analysis, the quantifying of the wet weight of tibialis anterior muscle and the histological assessment. The conduits
in host rats in vivo can not only be an effective in promoting regenerating of nerves but can also lead to favorable nerve
functional recovery.
Funded by the National Natural Science Foundation of China(No.50774096) 相似文献
946.
郑立霞 《武汉理工大学学报(材料科学英文版)》2009,24(3):415-417
The deformation resistance effect of polyacrylonitrile (PAN)-based carbon fibers was investigated, and the variatipn law of
electrical resistivity under tensile stress was analyzed. The results show that the gauge factor (fractional change in resistance
per unit strain) of PAN-based carbon fibers is 1.38, which is lower than that of the commonly-used resistance strain gauge.
These may due to that the electrical resistivity of carbon fibers decreases under tensile stress. In addition when the carbon
fibers are stretched, the change of its resistance is caused by fiber physical dimension and the change of electric resistivity,
and mainly caused by the change of physical dimension. The mechanical properties of carbon fiber monofilament were also measured.
Funded by the National Natural Science Foundation of China (No. 10672128 and 50878170) 相似文献
947.
王智宇 《武汉理工大学学报(材料科学英文版)》2009,24(5):698-701
A simple sonochemical route for the surface coating of titanium dioxide on cadmium sulfide nanocrystal was reported. After
2 h ultrasonic irradiation treatment, the mixture of CdS nanocrystals and tetrabutyl titanate in an aqueous medium yielded
CdS/TiO2 nanocrystals composites with core/shell structure. The thickness of TiO2 layer with smooth interface could be easily controlled via changing the concentration of the precursors and the time of irradiation.
The core/shell nanocrysrals were characterized by X-ray diffraction, transmission electron microscope and UV-vis spectrometry
techniques. The prepared semiconductor composites with particular band structure present appealing properties especially in
photochemical activity. 相似文献
948.
任平 《武汉理工大学学报(材料科学英文版)》2009,24(6):927-930
Spinel zinc ferrites ZnFe2O4, prepared by co-precipitation method using the zinc nitrate Zn(NO3)2·6H2O and ferric nitrate Fe(NO3)3·2H2O as the raw materials, were characterized by the thermo gravimetric analysis (TG) and differential scanning calorimeter (DSC), X-ray diffraction (XRD) and scanning electron microscope (SEM). The influence of synthesis conditions, such as Zn/Fe molar ratio, pH value, the sintering temperature and time, on the microstructures was detailedly investigated. The relationships between the microstructures and the synthesis conditions were discussed. The results show that the pure spinel zinc ferrites ZnFe2O4 are formed when the Zn/Fe molar ratio is 1.05:2 at pH=8.5 or Zn/Fe molar ratio is 1:2 at Ph=9-10, and the precursors are sintered at 1100 °C for 4 h. Especially no other phases are observed when the Zn/Fe molar ratio is 1:2 at pH=10 and the precursor is sintered above 700 for 4 °C h. The higher sintering temperature and longer sintering time contribute to grain growth. 相似文献
949.
何庆复 《武汉理工大学学报(材料科学英文版)》2009,24(3):428-431
Behaviour of hardening and serration yield of a Fe-Ni-Cr alloy under isothermal cycling (ISC) and out-phase TMF was studied
on the basis of varied hysteresis loops. Cycling hardening and serrated yielding for ISC depend on the temperature and the
total strain range, stronger hardening with serrated yielding at higher strain range under ISC at 600 °C, but no hardening
and serrated yielding occurred under ISC at 800 °C. Stronger hardening with stress serration occurred at the thermal path
going to the lowest temperature, no stress serration occurred at the highest temperature under the out-phase. The hardening
also depends on the total strain range, higher total strain range with lower cycling temperature resulted in a stronger hardening
and remarkable serration yielding behavior. Weaker hardening without serrated yielding occurred at near 800 °C may due to
an obvious cycling stress drop under out-phase TMF. Change in the shape of the hysteresis loops also expresses the degree
of the damage of the tested alloy under out-phase and ISC. 相似文献
950.
章桥新 《武汉理工大学学报(材料科学英文版)》2009,24(6):871-874
Silver powder was fabricated by spray pyrolysis, using 2%–20% AgNO3 solution, 336–500 mL/h flux of AgNO3 solution, 0.28–0.32 MPa flux of carrier gas and in the 620–820 °C temperature range. The effects of furnace set temperature,
concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated.
The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain
size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder
about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 °C furnace set temperature. 相似文献