Chitosan hydrogel‐coated cotton fabric: Antibacterial,pH‐responsiveness,and physical properties

In this work, chitosan hydrogel has been synthesized and used to impart pH‐sensitivity and antimicrobial finish to cotton fabric. In order to enhance the incorporation rate of hydrogel, anionic, and cationic activation of the textile surface was applied and then compared. The antibacterial activity of the fabric was then studied. The results revealed an enhancement of the antibacterial activities of the modified fabrics against Escherichia coli, Listeria monocytogene, and Staphylococcus aureus bacteria's. The capacity of material to respond to pH change was studied and confirmed using contact angle method. The anionic fabric treated with hydrogel showed a better pH‐responsiveness. Scanning electron microscopic testing results has also confirmed that the deposition of hydrogel was clearly better with the anionic activation. The characteristics of breathability of the fabrics were analyzed. The results show that the moisture management behavior of the finished materials is significantly better than the control one. Although the permeability to air has reduced by 10%, the permeability to water vapor remained practically unchanged. Furthermore, the effects of the antibacterial finishing on the physical properties of the cotton fabrics were also investigated. It was established that the functionalized samples have changed structure parameters, thickness, air permeability, tensile strength, and resistance to wrinkles. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2018 , 135, 46645.     

Structural,electric modulus and complex impedance analysis of ZnO/TiO2 composite ceramics

ZnO/TiO₂ composite ceramics have been prepared by solid‐state reaction technique at 900°C. The X‐ray diffraction results revealed the formation of secondary phases referred to as spinel Zn₂TiO₄ and hexagonal ZnTiO₃. The structural analysis showed that all the composites that have been prepared have a polycrystalline nature and a hexagonal wurtzite structure. The complex modulus (M) and electric impedance of the samples have been investigated by broadband dielectric spectroscopy in a wide range of temperature (40°C‐110°C) and frequency (0.1 Hz to 10 MHz). The modulus plots (M′′, M′) illustrate the presence of non‐Debye type of relaxations attributed to the effects of interfacial and dipolar polarizations. The real and the imaginary parts of the impedance are well fitted to equivalent circuit models. At high temperatures, Z″_max varies from 0.03 × 10⁶ to 4.9 × 10⁶ Ω when the TiO₂ doping concentration increases from 1 to 7 wt%. From the obtained results, the secondary phase ZnTiO₃ plays an important role in the electrical properties.     

Composite electronic materials based on poly(3,4-propylenedioxythiophene) and highly charged poly(aryleneethynylene)-wrapped carbon nanotubes for supercapacitors

Supercapacitor charge storage media were fabricated using the semiconducting polymer poly(3,4-propylenedioxythiophene) (PProDOT) and single-walled carbon nanotubes (SWNTs) that were helically wrapped with ionic, conjugated poly[2,6-{1,5-bis(3-propoxysulfonicacidsodiumsalt)}naphthylene]ethynylene (PNES). These PNES-wrapped SWNTs (PNES-SWNTs) enable efficient dispersion of individualized nanotubes in a wide range of organic solvents. PNES-SWNT film-modified Pt electrodes were prepared by drop casting PNES-SWNT suspensions in MeOH; high stability, first-generation PProDOT/PNES/SWNT composites were realized via electropolymerization of the ProDOT parent monomer (3,4-propylenedioxythiophene) in a 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide/propylene carbonate solution at the PNES-SWNT-modified electrode. The electrochemical properties of PProDOT and PProDOT/PNES/SWNT single electrodes and devices were examined using cyclic voltammetric methods. The hybrid composites were found to enhance key supercapacitor figures of merit (charge capacity and capacitance) by approximately a factor of 2 relative to those determined for benchmark Type I devices that exploited a classic PProDOT-based electrode material. The charge/discharge stability of the supercapacitors was probed by repeated rounds of cyclic voltammetric evaluation at a minimum depth of discharge of 73%; these experiments demonstrated that the hybrid PProDOT/PNES/SWNT composites retained ~90% of their initial charge capacity after 21,000 charge/discharge cycles, contrasting analogous data obtained for PProDOT-based devices, which showed only 84% retention of their initial charge capacity.     

Robust stability of hybrid Roesser models against parametric uncertainty: a general approach

This paper aims at proposing a general framework for the establishement of LMI conditions to analyse the robust stability of a singular hybrid Roesser model subject to parametric uncertainties. The uncertain parameters are involved through implicit Linear Fractional Representations (LFR). Special focus is put on the influence of the number of uncertain parameters and the dimensionality of the model. More precisely it is shown that each dimension can nearly be regarded as an uncertain parameter and the other way around. Therefore, their influence on the conservatism of the obtained condition is very similar.     

A New PSO-based Algorithm for Two-Dimensional Non-Guillotine Non-Oriented Cutting Stock Problem

In this paper, a new algorithm is proposed for the two-dimensional non-guillotine non-oriented cutting stock problem. The considered problem consists of cutting small rectangular pieces of predetermined sizes from large but finite rectangular plates. The objective is to generate cutting patterns that minimize the unused area and fulfill customer orders. The proposed algorithm is a combination of a new particle swarm optimization approach with a heuristic criterion inspired from the literature. The algorithm is tested on twenty-two instances divided into two sets. Corresponding results show the algorithm efficiency in optimizing the trim loss that is comprised between 2.6% and 7.8% for all considered instances.     

Adaptive noise-reducing anisotropic diffusion filter

In image processing and computer vision, the denoising process is an important step before several processing tasks. This paper presents a new adaptive noise-reducing anisotropic diffusion (ANRAD) method to improve the image quality, which can be considered as a modified version of a speckle-reducing anisotropic diffusion (SRAD) filter. The SRAD works very well for monochrome images with speckle noise. However, in the case of images corrupted with other types of noise, it cannot provide optimal image quality due to the inaccurate noise model. The ANRAD method introduces an automatic RGB noise model estimator in a partial differential equation system similar to the SRAD diffusion, which estimates at each iteration an upper bound of the real noise level function by fitting a lower envelope to the standard deviations of pre-segment image variances. Compared to the conventional SRAD filter, the proposed filter has the advantage of being adapted to the color noise produced by today’s CCD digital camera. The simulation results show that the ANRAD filter can reduce the noise while preserving image edges and fine details very well. Also, it is favorably compared to the fast non-local means filter, showing an improvement in the quality of the restored image. A quantitative comparison measure is given by the parameters like the mean structural similarity index and the peak signal-to-noise ratio.     

Effect of Sn2O3 doping on structural,optical and dielectric properties of ZnO ceramics

The synthesis of the undoped ZnO and ZnO–Sn₂O₃ composites prepared by conventional solid-state reaction method has been reported. Besides, the effect of increasing Sn₂O₃ content from 5 to 15 wt% on structural, optical, dielectric and electrical properties of the ZnO–Sn₂O₃ composites has also been investigated. In fact, the X-ray diffraction analysis indicates that the as-prepared ZnO–Sn₂O₃ composites may contain some combined phases such as SnO and Zn₂SnO₄. The atomic force microscopy shows that the surfaces of the composites are rough. The band gap energy seems to depend on the amount of Sn₂O₃ addition, with the maximum obtained at 15 wt% Sn₂O₃. Concerning the optical band gap, it has been found to be in the range of 3.18–3.93 eV. The dielectric loss was found to decrease with the increase in frequency. The results obtained from the ac-conductivity revealed that the values of σ(ω) increases with the Sn₂O₃ adding content. The dc-conductivity of all the composites increases with the increase in temperature. The electrical conductivity was analyzed with the power law, and agrees with the correlation barrier hopping model.     

Sensor fault detection and isolation filter for polytopic LPV systems: A winding machine application

In this paper, a fault diagnosis method is developed for a particular class of nonlinear systems described by a polytopic linear parameter varying (LPV) formulation. The main contribution consists in the synthesis of an accurate fault detection and isolation (FDI) filter and also a sensor fault magnitude estimation with a quality factor. This quality factor of the filter underlines if the fault estimation can be used or not. Stability conditions of the polytopic LPV filter are studied by ensuring poly-quadratic stability with Linear Matrix Inequality (LMI) representation. The effectiveness of this global FDI scheme through LPV modelization, filter design and stability analysis, is illustrated on a real winding machine under multiple sensor faults.