Effect of extraction conditions on yield and degree of esterification of durian rind pectin: An experimental design

The effect of time (1 and 4 h), pH (2.0 and 2.5) and temperature (80 and 90 °C) on yield and degree of esterification (DE) of durian rind pectin was investigated. The yield and DE of the extracted pectin ranged from 2.1 to 10.3% (w/w, based on dry weight of durian rind) and 45.6–64.8% respectively. Yield was significantly affected by time, temperature and pH, and interactions between temperature and pH, and heating time and pH. DE was significantly affected by heating time and pH, and interactive effects of temperature and pH, and heating time and pH. The extraction yield was not related to DE. By considering pectin yield and DE, the acid extraction of durian rind pectin at 80 °C, for 4 h and at pH 2.5 could be suitable.     

Optimisation of rancidity stability in long‐chain PUFA concentrates obtained from a rainbow trout (Oncorhynchus mykiss) by‐product

This research was focused on the production of polyunsaturated fatty acid concentrates from a farmed rainbow trout (Oncorhynchus mykiss) by‐product (i.e. belly muscle). The effect of different process variables (urea/fatty acids (FA) contents ratio, crystallisation time and temperature and stirring speed of the urea/FA mixture) on the lipid oxidation development during the urea complexation process was investigated. For this purpose, an experimental design (26 runs) following the response‐surface methodology was developed. As a result, peroxide value and TOTOX index showed to be dependent on the crystallisation time and temperature and the urea/FA ratio, while no influence of the crystallisation stirring speed was detected on both indices; additionally, polyene index was affected by the urea/FA ratio and its interaction with the crystallisation time. An optimised desirability score near 1.0 was attained provided values of 2.8 °C, 3.05 h and 3.57 were applied for crystallisation temperature, crystallisation time and urea/FA ratio, respectively.     

广告英语中的修辞用法(英文)

广告英语是英语文体学研究的一个重要分支。修辞在广告文体中起着重要作用。从比喻、拟人、双关等六个方面论述了广告英语的修辞特点。     

Spectroscopic characterization of 1,5-diphenyl-3,7-dihydroxy-1,5-diazacyclooctane — (8C ring compound) formed in N,N-diglycidylanaline/aniline curing systems

Summary A NMR and infrared analysis of the cyclic product formed by the reaction of N,N-diglycidylaniline with aniline confirms the structure of an eight-membered ring (I). The conformational structure of this compound is discussed.     

RDX含量对NC－DBP－RDX体系流变性和弹性效应的影响

运用Ｉｎｓｔｒｏｎ３２１１型毛细管流变仪研究了ＲＤＸ含量在０～４６．９％范围内，在不同温度下对ＮＣ－ＤＢＰ－ＲＤＸ体系流变性的影响，得到了各种流变规律；同时利用公差显微镜研究了ＲＤＸ含量在８０℃下对该体系弹性效应的影响规律。     

Structural Diversity and Defensive Properties of Norditerpenoid Alkaloids

We have tested the insect antifeedant and toxic activity of 43 norditerpenoid alkaloids on Spodoptera littoralis and Leptinotarsa decemlineata including eserine (physostigmine), anabasine, and atropine. Antifeedant effects of the test compounds were structure- and species-dependent. The most active antifeedants to L. decemlineata were 1,14-diacetylcardiopetaline (9) and 18-hydroxy- 14-O-methylgadesine (33), followed by 8-O-methylconsolarine (12), 14-O-acetyldelectinine (27), karakoline (7), cardiopetaline (8), 18-O-demethylpubescenine (13), 14-O-acetyldeltatsine (18), takaosamine (21), ajadine (24), and 8-O-methylcolumbianine (6) (EC50 < 1 microg/cm2). This insect showed a moderate response to atropine. S. littoralis had the strongest antifeedant response to 24, 18, 14-O-acetyldelcosine (19), and delphatine (29) (EC50 < 3 microg/cm2). None of the model substances affected the feeding behavior of this insect. The most toxic compound to L. decemlineata was aconitine (1), followed by cardiopetalidine (10) (% mortality > 60), 14-deacetylpubescenine (14), 18-O-benzoyl-18-O-demethyl-14-O-deacetylpubescenine (17), 14-O-acetyldelcosine (19), 14-deacetylajadine (25) and methyllycaconitine (30) (% mortality > 45). Orally injected S. littoralis larvae were negatively affected by 1, cardiopetaline (8), 10, 1,14-O-acetylcardiopetalidina (11), 12, 14, 1,18-O-diacetyl-19-oxo-gigactonine (41), olivimine (43), and eserine in varying degrees. Their antifeedant or insecticidal potencies did not parallel their reported nAChR binding activity, but did correlate with the agonist/antagonist insecticidal/antifeedant model proposed for nicotininc insecticides. A few compounds [14, tuguaconitine (38), 14-demethyldelboxine (40), 19, dehydrodelsoline (36), 18-O-demethylpubescenine (13), 41, 9, and delcosine (23)] had selective cytotoxic effects to ward insect-derived Sf9 cells. None were cytotoxic to mammalian CHO cells and none increased Trypanosoma cruzi mortality. The selective cytotoxic effects of some structures indicate that they can act on biological targets other than neuroreceptors.     

iMLP: Applying Multi-Layer Perceptrons to Interval-Valued Data

Interval-valued data offer a valuable way of representing the available information in complex problems where uncertainty, inaccuracy or variability must be taken into account. In addition, the combination of Interval Analysis with soft-computing methods, such as neural networks, have shown their potential to satisfy the requirements of the decision support systems when tackling complex situations. This paper proposes and analyzes a new model of Multilayer Perceptron based on interval arithmetic that facilitates handling input and output interval data, but where weights and biases are single-valued and not interval-valued. Two applications are considered. The first one shows an interval-valued function approximation model and the second one evaluates the prediction intervals of crisp models fed with interval-valued input data. The approximation capabilities of the proposed model are illustrated by means of its application to the forecasting of daily electricity price intervals. Finally, further research issues are discussed. Research funded by Universidad Pontificia Comillas.     

The “root” experiment of the “cervantes” spanish soyuz mission: Cell proliferation and nucleolar activity alterations in arabidopsis roots germinated in real or simulated microgravity

In an experiment conducted in the “Cervantes” Spanish Soyuz Mission, a 10-day flight to the International Space Station, Arabidopsis seeds were germinated, seedlings grew for 4 days at 22ºC, and they were fixed in flight with paraformaldehyde. A ground 1 g control experiment was replicated, and an additional experiment in simulated microgravity, using a Random Positioning Machine, was performed in the same conditions. Structural, morphometric and immunocytochemical data were compared. Glutaraldehyde-fixed seedlings similarly grown in the Space Shuttle (STS-84 Mission) were also used for ultrastructural and morphometric studies. Seedlings grown for 4 days in real or simulated weightlessness showed a longer size than the ground 1 g control. Root meristematic cells showed an enhanced proliferating rate, but ribosome biogenesis was reduced, as inferred from the nucleolar size and from the levels of the nucleolar protein nucleolin. This could be the consequence of the acceleration of the cell cycle, with shortening of its phases. Weightlessness induces stress in the plant, influencing cellular processes decisive for development and morphogenesis. This stress may endanger the plant and would require the action of compensating specialized defence mechanisms.     

Mapping Simple Polygons: How Robots Benefit from Looking Back

We consider the problem of mapping an initially unknown polygon of size n with a simple robot that moves inside the polygon along straight lines between the vertices. The robot sees distant vertices in counter-clockwise order and is able to recognize the vertex among them which it came from in its last move, i.e. the robot can look back. Other than that the robot has no means of distinguishing distant vertices. We assume that an upper bound on n is known to the robot beforehand and show that it can always uniquely reconstruct the visibility graph of the polygon. Additionally, we show that multiple identical and deterministic robots can always solve the weak rendezvous problem in which the robots need to position themselves such that all of them are mutually visible to each other. Our results are tight in the sense that the strong rendezvous problem, where robots need to gather at a vertex, cannot be solved in general, and, without knowing a bound beforehand, not even n can be determined. In terms of mobile agents exploring a graph, our result implies that they can reconstruct any graph that is the visibility graph of a simple polygon. This is in contrast to the known result that the reconstruction of arbitrary graphs is impossible in general, even if n is known.