Role of nano‐size SiO2 additive on the thermal behavior of cyanoacrylate nanocomposite

Nowadays, solvent‐free, one‐part cyanoacrylate adhesive is widely used in medicine and dentistry. According to a literature survey done by the authors, there are few papers concentrated on the role of nano‐sized particles on the thermal behavior of cyanoacrylate glue. Thus the main goal of the current research focused on clarifying the role of nano‐sized SiO₂ on the thermal behavior of cyanoacrylate. Thermal behavior of all materials including cyanoacrylate and its nanocomposites was studied by using Differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) methods. The results of DSC analysis showed that an increase in the amount of nano‐sized SiO₂ results in decreases in the duration of cyanoacrylate curing, energy release during polymerization, and incubation time of polymerization. Furthermore, the results of TGA tests illustrated that the weight loss of cyanoacrylate strongly depends on the contents of both caffeine and SiO₂. In fact, an increase in nano‐sized SiO₂ content increases the degradation temperature of cyanoacrylate. J. VINYL ADDIT. TECHNOL., 2010. © 2010 Society of Plastics Engineers     

Remineralization effects of self-assembling peptide P11-4 associated with three materials on early enamel carious lesions: An in vitro study

The aim of this study was to assess the remineralization of enamel caries lesions using the self-assembling peptide P₁₁-4 associated with different materials. Artificial early enamel lesions were prepared on 154 primary teeth. The samples were randomly divided into eight groups: (1) control, (2) P₁₁-4, (3) fluoridate toothpaste (FT), (4) P₁₁-4 + FT, (5) casein phosphopeptide–amorphous calcium phosphate (CPP–ACP), (6) P₁₁-4 + CPP–ACP, (7) fluoridate bioactive glass toothpaste (BT), and (8) P₁₁-4 + BT. The surface enamel microhardness (EMH) and energy-dispersive X-ray spectroscopy (EDS) of the teeth were then measured at the baseline, after demineralization, and after 28 days of remineralization. The enamel surfaces were assessed by field emission scanning electron microscopy (FESEM) and atomic force microscopy (AFM). The data were analyzed with one-way analysis of variance (ANOVA) (p < .05). EMH after demineralization was significantly lower than the baseline value (p < .001). The interventions led to an enhanced percentage of EMH recovery (%REMH), which was higher in Groups 6 and 7. There was no significant difference between Groups 3 and 4. Groups 1 and 2 had the lowest %REMH. The mean calcium/phosphate weight percentage ratio of P₁₁-4 was significantly lower than the others (p < .001). The FESEM and AFM images revealed mineral deposition on the eroded enamel and reductions in surface roughness in Groups 5 and 7.     

A new mathematical approach to improve residual stress measurement in ring-core method

Journal of Mechanical Science and Technology - III-conditioning at the inverse equation of integral method in ring-core residual stress measurement leads to high stress sensitivity to strain...     

Artifact reduction using reliability reasoning for image generation of FTV

In this paper, we present a new view synthesis method in multiview camera configurations of Free viewpoint TV (FTV) where potential depth errors are considered. The emphasis is on the artifacts eliminating for photorealistic synthesis especially near object boundaries. In contrast to conventional techniques which ignore geometry errors, we first categorize the artifact cases and depth modes. Furthermore, this paper infers the complementarity principle of the artifacts from left and right references. This complementarity guarantees the effectiveness of our reliability-based synthesis. The reliability reasoning is crucial for artifacts reduction. The reliable and unreliable areas from different views can be correctly labeled. Then artifacts caused by unreliable pixels from one reference can be replaced by the reliable pixels from the other reference. As a final result, artifacts of novel view are demonstrated to be significantly reduced on different multiview sequences.     

Biologically‐synthesised ZnO/CuO/Ag nanocomposite using propolis extract and coated on the gauze for wound healing applications

Wound healing has long been recognised as a major clinical challenge for which stablishing more effective wound therapies is necessary. The generation of metallic nanocomposites using biological compounds is emerging as a new promising strategy for this purpose. In this study, four metallic nanoparticles (NPs) with propolis extract (Ext) and one without propolis including ZnO/Ext, ZnO/Ag/Ext, ZnO/CuO/Ext, ZnO/Ag/CuO/Ext and ZnO/W were prepared by microwave method and assessed for their wound healing activity on excision experimental model of wounds in rats. The developed nanocomposites have been characterised by physico‐chemical methods such as X‐ray diffraction, scanning electron microscopy, diffuse reflectance UV–vis spectroscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis and Brunauer–Emmett–Teller analyses. The wounded animals treated with the NPs/Ext in five groups for 18 days. Every 6 days, for measuring wound closure rate, three samples of each group were examined for histopathological analysis. The prepared tissue sections were investigated by haematoxylin and Eosin stainings for the formation of epidermis, dermis and muscular and Masson''s trichrome staining for the formation of collagen fibres. These findings toughly support the probability of using this new ZnO/Ag/Ext materials dressing for a wound care performance with significant effect compared to other NPs.Inspec keywords: nanomedicine, X‐ray diffraction, II‐VI semiconductors, visible spectra, ultraviolet spectra, nanocomposites, biomedical materials, proteins, wounds, nanoparticles, scanning electron microscopy, nanofabrication, skin, zinc compounds, silver, antibacterial activity, Fourier transform infrared spectra, copper compounds, molecular biophysicsOther keywords: propolis, wound healing applications, effective wound, metallic nanocomposites, biological compounds, metallic nanoparticles, microwave method, wound healing activity, physico‐chemical methods, Fourier transform infrared spectroscopy, diffuse reflectance UV‐vis spectroscopy, Brunauer‐Emmett‐Teller analyses, wounded animals, wound closure rate, wound care performance, histopathological analysis, scanning electron microscopy, X‐ray diffraction, thermogravimetric analysis, haematoxylin, Eosin stainings, Masson trichrome, epidermis, muscular trichrome, collagen fibres, time 18.0 d, time 6.0 d, ZnO‐CuO‐Ag     

On the design of new ductile knee bracing

An approximate method is presented that can be used to determine the nonlinear behavior of a new structural bracing system called the ‘Chevron Knee Bracing’ (CKB). In this framing system, an especial form of diagonal brace connected to a knee element instead of a beam-column joint is investigated. The diagonal element provides lateral stiffness during a moderate earthquake. However, the knee element is designed to have three plastic joints or two yielded specimens in flexural and shear yielding mode, respectively, for dissipation of the energy caused by a strong earthquake. This article demonstrates the transformation of a complex problem into a new, practical set of design charts and graphs. To severe purpose, first, an optimal shape and angle for the diagonal-knee element is considered based on the studying of the elastic and inelastic behavior of the system. Then, by use of the main graphs and charts designed accordingly, the dynamic response of this model is properly investigated. Finally, the correctness of the results is ascertained, using example problems. The comparison of the results between the technique presented in this paper and the exact finite element methods and/or experimental results shows very good agreement and very suitable conformity.     

Performance evaluation of modified rotating-jet electrospinning method by investigating the effect of collector size on the nanofibers alignment

Modified rotating-jet electrospinning method (MRJM) is a new electrospinning technique with a novel setup including two metallic concentric hollow cylinders for generating highly aligned fibers. In this report, an experimental study was carried out to evaluate the effectiveness of MRJM for generating highly aligned nanofibers. For this purpose, the effect of voltage in the range of 10–22 kV, inner collector diameter in the range of 20–50 cm, and outer collector diameter in the range of 30–60 cm, on alignment degrees of electrospun fibers were explored and the results for each set of parameters were compared with those obtained for rotating-jet electrospinning method (RJM). The obtained results indicated that the alignment degrees of electrospun fibers in MRJM were significantly higher than those of RJM. The maximum achievable alignment degree in MRJM was around 82 % that was higher than the corresponding maximum value (40 %) of RJM. Although the effect of applied voltage on the degree of alignment in MRJM was observed to be negligible, it was experimentally proved that by manipulating the outer cylinder diameter, the degree of alignment can be increased up to 20 %. To achieve a conceptual understanding of the reason for significant influence of the outer cylinder on the elecrospinning performance, a formula was derived according to the Gauss’s law in the last part of this paper that relates the electric field strength inside the region between the inner cylinder and the spinneret to the radii of inner and outer cylinders.     

Outage Probability Based Robust Distributed Beam-Forming in Multi-User Cooperative Networks with Imperfect CSI

In this paper, a new robust problem is proposed for relay beamforming in relay system with stochastic perturbation on channels of multi user and relay network. The robust problem aims to minimize the transmission power of relay nodes while the imperfect channel information (CSI) injects stochastic channel uncertainties to the parameters of optimization problem. In the power minimization framework, the relays amplification weights and phases are optimized assuming the availability of Gaussian channel distribution. The power sum of all relays is minimized while the outage probability of the instantaneous capacity (or SINR) at each link is above the outage capacity (or SINR) for each user. The robust problem is a nonconvex SDP problem with Rank constraint. Due to the nonconvexity of the original problem, three suboptimal problems are proposed. Simulation and numerical results are presented to compare the performance of the three proposed solutions with the existing worst case robust method.     

Spatial-Temporal Cooperative Spectrum Sensing in Flat Fading Channels for Cognitive Radio Using Extend Kalman Filter

This paper investigates a new channel gain map tracking by Space-Time Extended Kalman Filtering (STEKF) for a flat channel, and a novel spectrum sensing via Time Spatial Weighted Non-negative Lasso (TSWNL) algorithm. STEKF enables CRs to estimate and interpolate channel gain map for the entire geographical area of interest with a limited number of CRs measurements. In order to sense primary users (PU) activities, include the transmission power by each PU, location and number of active PUs, TSWNL algorithm is proposed. Numerical results illustrate that the proposed STEKF channel estimation and TSWNL sensing algorithms outperforms linear methods.