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131.
132.
A series of new o‐phenylenediamine (OPD)/o‐phenetidine (PHT) copolymers with partly phenazine‐like structures has been successfully synthesized at three polymerization temperatures by chemically oxidative polymerization in four different polymerization media. The molecular structures and properties of the resulting OPD/PHT polymers were investigated by IR, UV–vis and high‐resolution 1H NMR spectroscopies, and DSC, in order to ascertain the effect of reaction temperature, comonomer ratio and acid medium. The copolymerization mechanism of OPD with PHT monomers has been proposed. It is found that the statistical OPD/PHT copolymer obtained at a temperature of 118 °C has a higher degree of polymerization than that obtained at 12–17 °C. The OPD content in the copolymers calculated from NMR spectroscopic analysis is higher than that in the feed OPD content, whereas the OPD content calculated from element analysis is slightly lower than the feed OPD content. It can be predicted that denitrogenation takes place in the OPD units during the polymerization process at OPD/PHT molar ratios of 90/10 and 100/0. These OPD/PHT copolymers exhibit a much better solubility than the OPD homopolymer, hence suggesting an incorporation of PHT units into the phenazine structure of the homopolymer. The thermal behavior of the copolymers was also studied. Copyright © 2004 Society of Chemical Industry 相似文献
133.
The solubilities of ethyl palmitate, ethyl oleate, ethyl eicosapentaenoate (EPA) and ethyl docosahexaenoate (DHA) in supercritical
carbon dioxide were determined by a continuous flow method. The solubilities of fatty acid ethyl esters increased with pressure
and decreased as the temperature was increased. An empirical equation, similar to Chrastil's equation, was used to describe
the relationship between solute solubility and the density of carbon dioxide. The empirical equation was further used to qualitatively
estimate the separation efficiency of isolating EPA and DHA ethyl esters from fatty acid esters. The operating conditions
yielding high solubility gave fast extraction rate but resulted in low separation efficiency. Experiments were conducted to
separate ethyl EPA and ethyl DHA from a model mixture containing four fatty acid ethyl esters and from esterified squid visceral
oil. The experimental data compared closely with the calculated values. 相似文献
134.
The in vitro effect of citric acid application on periodontally involved root surfaces was investigated using scanning electron microscopy. Teeth were selected following specific criteria. The specimens were prepared for observation, and the features of the root surface were studied. The results demonstrated that a 3-minute application of citric acid (pH = 1.0) to the root surface after scaling and root planing demineralized the outer root surface, opened the dentinal tubules, and exposed collagen fibers. Scaling and root planing alone left the surface with a smear layer, scattered islands of cementum, and no collagen fibers or exposed dentinal tubules. 相似文献
135.
136.
Four monoalkyl esters of isoalkylphosphonic acids have been studied for the chromatographic separation ofrare earths (RE).The relationship between distribution ratios and acid concentration of the eluants forsamarium and ytterbium has been explored.The characteristics of these extractants loaded onto macroreticularpoly (methyl methacrylate) resin beads for the separation of lanthanum,cerium,praseodymium and neodymiumhave been compared.Among the extractants studied,mono(1-methylheptyl) ester of isooctylphosphonic acidwas found to be the best for RE separation.The acidity for separation is lower than any known P-containingextractants for the same purpose.For instance,with 1.73 mol·L~(-1) nitric acid as eluent,thulium,ytterbium andlutetium can be separated quantitatively.The extractant-loaded resins possess high column efficiency with goodkinetic characteristics.The extraction mechanism was also explored. 相似文献
137.
Effect of the absence of lipoxygenase isoenzymes on the storage characteristics of rice grains 总被引:1,自引:0,他引:1
Three varieties of paddy rice with and three varieties without lipoxygenase (LOX) isoenzymes were stored at room temperature, in dark conditions for 42 months. Insect damage and viability were investigated during that time. Varieties without LOX-1,2 and their offspring were screened with a rapid method of estimating LOX isoenzymes, and subjected to an accelerated-ageing experiment. The results indicated that in varieties without LOX-1,2, after long storage, rice quality was normal, but for varieties with LOX-1,2, rice quality deteriorated. With increase of storage time, the germination rate of the seed of most varieties decreased greatly except for varieties without LOX-1,2 where there was almost no change in the germination rate. In varieties without LOX-1,2 and their offspring, after an accelerated ageing experiment the germination rate of some varieties changed slowly, but with others, the germination rate changed quickly. This indicated that a definitive factor, which influenced the life of seeds, may be the loss of LOX-1,2. During storage, there was also a significant difference in the degree of insect damage. In varieties without LOX-3 insect damage was lower, but in varieties with LOX-3 insect damage was higher. Therefore, the absence of LOX-3 may be very important in insect resistance in rice grain. 相似文献
138.
本文对氨基酸营养条件下植物体内硝酸盐含量变化及其机理,土施植物激素前体色氨酸和蛋氨酸对高等植物生长和化学组成的影响。氨基酸和氨基酸肥料对植物产量和品质的影响作了综述。 相似文献
139.
一只毛绒狗的故事
“大红狗”是正流行在日本京都白领女性圈子里的一款玩具。它选用毛巾布料,因此手感良好,据宣传称它的红色能够刺激脑细胞,使人充满活力,所以兼具一定的医疗保健作用。很多白领女性都喜欢将它摆放在办公室的写字台上,而现在东京都三鹰市内各大商店正以2100日元(含税)的价格热销中。 相似文献
140.
稠油热采注汽管道由于长期在高温、高压下运行,极易发生各种损伤,如腐蚀、裂纹、材料退化等,极易造成管道承压能力降低,发生失效事故。如何检测出潜在危险性缺陷,判断注汽管道能否继续使用,是保证注汽管道安全运行的关键问题。探讨了高温压力管道在线检测技术发展现状及其应用范围。 相似文献