More Relaxed Non‐Quadratic Stabilization Conditions Using Ts Open Loop System and Control Law Properties

This paper proposes more relaxed stabilization conditions based on a non‐quadratic Lyapunov function (NQLF) and parallel distributed compensator (PDC) controller. The conditions are derived in terms of linear matrix inequalities (LMIs) by introducing three slack matrices based on the properties of TS membership functions, an open loop system and a PDC controller. These slack matrices are utilized to decouple the LMI variables from the TS system and the input matrices. Therefore, the proposed approach greatly reduces the number of LMI conditions and improves feasibility by providing more degrees of freedom compared to recently published studies. Moreover, local stability and stabilization conditions are considered to handle the time derivatives of membership functions appearing in the stabilization synthesis of the TS closed‐loop system with PDC controller. Finally, several examples are presented to demonstrate the advantages of the proposed approaches.     

Non-destructive evaluation of the internal fruit quality of black mulberry (Morus nigra L.) using visible-infrared spectroscopy and genetic algorithm

The present study aims at assessing a non-destructive optical method for determining the internal quality of mulberry juice. First, UV-IR spectra (300–1100 nm) were acquired for each sample with a spectral resolution of 2 nm. Then the calibration set, composed of 70 and 38 samples, was used as the validation set. Next, two types of pre-processing multiplicative scatter correction)MSC(and standard normal variate)SNV(were used before analysing the data with multivariate calibration methods of PLS and GA-PLS. The following results were obtained including the correlation coefficient (r) of 0.94, 0.89, 0.98, and 0.95 and root mean square error of validation (RMSEV) 1.31°Brix, 0.52, 0.014, and 0.014 for total soluble solid (TSS), titratable acidity (TA), ascorbic acid (AA), and total anthocyanin content (AC) of mulberry juice, respectively. After that, GA-PLS was applied to select the efficient spectral regions. Model using 31 variables and 15 factors presented and yielded the best prediction results. The best combinations of 21 spectral intervals among 40 intervals selected by GA-PLS also yielded good results with RMSEV = 0.03096, r = 0.96; RMSEV = 0.062, r = 0.98, RMSEV = 0.041, r = 0.98; RMSEV = 0.0006, r = 0.96 for TSS, AA, TA, and AC of mulberry juice, respectively. Finally, it was concluded that using the UV-IR measurement technique, spectral range (300–1100 nm), it was possible to assess the quality characteristics of mulberry juice.     

Removal of Cetylpyridinium Bromide by Adsorption onto Maghnite: Application to Paper Deinking

The removal of cetylpyridinium bromide (CPB) from aqueous solutions was investigated using a mineral adsorbent called Maghnite (a bentonite obtained from Maghnia, West Algeria). The adsorption kinetics of CPB on Maghnite is pseudo-second order and the adsorption isotherm follows essentially the model of Redlich–Peterson. The results obtained show that CPB is adsorbed on Maghnite with an adsorption capacity of 0.438 mmol/g (168.4 mg/g). Physical data indicate that CPB is efficient for the deinking of newspaper solutions, only when the natural Maghnite is associated to CPB. These results are of practical interest, since CPB shows a double action—to protect and to optimize aquatic environment.     

Synthesis, characterization polymerization and antibacterial properties of novel thiophene substituted acrylamide

Ethyl 2-acrylamido-4,5,6,7-tetrahydrobenzo [b] thiophene-3-carboxylate (ETTCA) has been synthesized and its structure has been elucidated by elemental analysis and spectral tools. Free radical polymerization of (ETTCA) has been conducted in several solvents using azobisisobutyronitrile (AIBN) as an initiator. The kinetic parameters of polymerization of the ETTCA were investigated, and it was found that the polymerization reaction follows the conventional free radical scheme. The overall activation energy of polymerization ΔE was determined (ΔE = 45.11 kJ mol⁻¹). The copolymerization of ETTCA with three conventional monomers was carried out in dioxane at 65 °C. The monomer reactivity ratios for the copolymerization of ETTCA with methyl methacrylate (MMA), vinyl acetate (VA) and vinyl ether (VE) were calculated. Thermal stability of the ETTCA polymer and its copolymers were investigated by thermogravimetric analysis. It has been found that the prepared polymer (PETTCA) and its copolymers with VA have moderate biological activity and highly dependent on the copolymer composition.     

Dye removal from colored textile wastewater using chitosan in binary systems

In this paper, the removal of two anionic dyes from textile effluent in single and binary systems was investigated. Direct Red 23 and Acid Green 25 were used as anionic dyes. The surface characteristics of chitosan were investigated using Fourier transform infrared. The effects of operational parameters such as chitosan dosage, initial dye concentration, salt and pH on dye removal were studied. The isotherms of dye adsorption were investigated. It was found that the isotherm data of Direct Red 23 and Acid Green 25 in single and binary systems followed Tempkin isotherm. In addition adsorption kinetics of dyes was studied in single and binary systems and rate sorption was found to conform to pseudo-second order kinetics with a good correlation. Results indicated that chitosan could be used as a biosorbent to remove the anionic dyes from contaminated watercourses in both single and binary systems of pollutants.