Mechanical properties of austenitic stainless steel with high niobium contents

To better understand the influence of the microstructural characteristics on the mechanical properties of Fe-Cr₂₂-Ni₂₅-Nb_x austenitic stainless steel (ASS-Nb_x), the mechanical properties were investigated. Nb addition was conducted with four different amounts: 0, 0.29, 0.58 and 0.86%. With the increasing Nb content, the mean grain size for the Fe-Cr-Ni-based alloys decreased, while the size of Nb precipitate increased. Owing to the different microstructural characteristics, their mechanical properties were altered. The highest tensile strength was obtained for ASS-Nb_0.29 alloy. However, with the increasing Nb content in ASS-Nb_0.29–0.86 alloys, the tensile strength decreases despite the grain refinement. The mechanical properties of the ASS-Nb alloys were influenced by the Nb precipitation hardening and the grain boundary cohesive strength, arising from the size of Nb precipitations.     

Involvement of cytochrome b5 in the oxidative desaturation of linoleic acid to γ-linolenic acid in rat liver microsomes

The effects of antibodies against microsomal electron-transport components on the in vitro activity of Δ⁶-desaturation of linoleic acid to γ-linolenic acid have been studied in intact microsomal membranes of rat liver. Reduced nicotinamide adenine dinucleotide (NADH) or reduced nicotinamide adenine dinucleotide phosphate (NADPH) (0.87 mM) served as electron donors, and effectively prompted the Δ⁶-desaturase activities with yields of about 1.1 to 1.3 nmol per mg of protein in 10 min. Of the two antibodies studied under the same in vitro conditions, i.e., rabbit antisera preparations against rat liver microsomal hydrophilic parts of cytochrome b₅ and NADPH-cytochrome c reductase, only the antibody against cytochrome b₅ demonstrated a marked ability to inhibit the Δ⁶-desaturase activity. This evidence supports a participation of cytochrome b₅ in the Δ⁶-desaturation of linoleic acid and suggests a pathway analogous to the Δ⁹-desaturation of stearyl-CoA.     

A new etching technique for revealing the plastic deformation zone in an Al–Cu–Mg alloy

A new etching technique for revealing the plastic deformation zone in an Al–Cu–Mg alloy has been developed. The etching with the proposed etching agent was conducted on the deformed sample after being heated to 673 K for 3 h. With this etching technique, the plastic deformation zone was clearly observed even under low magnification. This was due to the change of microstructural characteristics in the plastic deformation zone after the heating process, in which there is significant precipitation of Al₂Cu and Mg₂Si, caused by the high energy arising from the severe deformation.     

Influence of domain orientation on the mechanical properties of lead zirconate titanate piezoelectric ceramics

The influence of domain orientation on the mechanical properties of lead zirconate titanate (PZT) piezoelectric ceramics has been investigated using un-poled and poled PZT ceramics. High mechanical properties, e.g., high elastic modulus and compressive strength, were obtained for the polarized PZT ceramics due to strain hardening caused by more severe domain switching during the loading process, while low mechanical properties for the un-poled ceramics. Fracture mechanics of the ceramics were influenced by the direction of the tetragonal lattice structure since cracks propagate along the long axis of the tetragonal structure (c-axis). Using X-ray diffraction and electron back scatter diffraction analysis, the domain switching characteristics could be clarified.     

Hydrogen embrittlement characteristics of hot-stamped 22MnB5 steel

Hydrogen embrittlement (HE) characteristics of 22MnB5 steel (U-bent specimen) manufactured using hot-stamping process at various temperatures were experimentally and numerically investigated. Steel resistance to HE was examined through delayed failure tests under static and cyclic loading during hydrogen charging. First, the low cyclic loading caused severe HE, in which a clear difference in the extent of HE was obtained depending on the hot-stamped sample, which directly affected the microstructural characteristics and stress–strain distribution. The hot-stamped samples with large martensite phase showed low resistance to HE compared with those with small martensite phase because of the high concentration of hydrogen trapped in the phase boundaries. Moreover, the dual phase (ferrite and martensite) of the hot-stamped samples reduced their resistance to HE, which is caused by the hydrogen trapped in the laminar-shaped pearlite phase. The resistance to HE was improved by low-temperature heating at 200 °C for 1 h because of the generation of ε-carbides as trap sites as they render the hydrogen non-diffusible. Furthermore, the internal strain in the U-bent sample could accelerate HE because of the high concentration of hydrogen. These results were verified by experimental and numerical analyses. Thus, the hydrogen trapping mechanism was proposed as a valid mechanism for HE in 22MnB5.     

Analysis of eddy currents in laminated silicon steel sheets of permanent magnet‐type MRI by 3d finite element method using multinode technique

We developed a method, called the multinode technique, that can take into account any electrical isolation of conductors using the multinodes of the electric scalar potentials. The eddy currents in the laminated silicon steel sheets can be calculated using this method without the mesh of the interlaminar air gap. It is quantitatively clarified that the eddy currents in the laminated silicon steel sheets in a permanent magnet‐type MRI system have effects on the time variations of the flux distributions. © 2006 Wiley Periodicals, Inc. Electr Eng Jpn, 156(1): 61–69, 2006; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20208     

A study of the effects of vibration on the electric power generation properties of lead zirconate titanate piezoelectric ceramic

To better understand how the electric power generated from PZT piezoelectric ceramics is affected by mechanical loading conditions the power generation was examined during cyclic loading under various loading conditions. The electric power generation was continuously examined using a monitoring system that we have recently developed. This system revealed that the electric power increased with increase of the applied load but then decreased when the applied load exceeded a certain level. In addition, greater electric power was generated with a simple beam configuration compared with a cantilevered beam. The change of electric power generation was directly related to the stress direction; high stress in the tetragonal structure parallel to the c-axis gave rise to high electric power generation. On the other hand, material failure, including domain switching and crack generation, caused a reduction of the electric power generated. Based upon our experimental data, suitable loading conditions to give high piezoelectric energy generation have been clarified.     

Different expression of Bcl-2 protein in gastric adenomas and carcinomas

In order to cast light on the possible role of bcl-2 protein (Bcl-2) expression in gastric tumorigenesis, 33 cases of gastric adenomas and carcinomas originating from the same stomachs were immunohistochemically investigated for Bcl-2 protein (Bcl-2) expression, accumulation of p53 protein and cell proliferation as determined by the Ki-67 labeling index (LI). Bcl-2 expression was detected in 24/33 (72.7%) adenomas and in 6/33 (18.2%) carcinomas, the difference being statistically significant (P = 0.0001). Only 4 of 33 (12.1%) cases exhibited expression in both adenoma and carcinoma lesions in the same stomachs. Immunoreactivity was decreased in areas of cellular and structural atypia in adenoma lesions (P < 0.008), and appeared to be positively linked to the tumor progression and the degree of differentation in carcinomas, although it did not reach statistical significance. Accumulation of p53 protein was rare in the adenomas but was found in 15/33 (45.5%) of carcinoma lesions, with a significant dissociation from Bcl-2 immunoreactivity. No apparent relation between Ki-67 LI and either adenoma grading or carcinoma typing was noted, although average Ki-67 LI of the highest labeling areas in carcinomas was statistically higher than in adenomas (P = 0.0001). These results indicate that the regulation of Bcl-2 expression may differ between gastric adenomas and carcinomas, may be correlated with tumor differentiative features. In addition, p53 accumulation may play an important role in the onset of malignancy.     

Asbestos and DNA double strand breaks

A radiosensitive DNA repair-deficient xrs-5 cell line was used to study asbestos cytotoxicity and DNA double strand breaks (DSBs). Although xrs-5 cells did not show any increase in sensitivity to chrysotile fibers in short-term (4-h) treatment when compared with wild-type CHO cells, longer-term exposure (24 h) gave significantly lower cell survival accompanied by a cell growth delay as well as a higher DNA DSB induction in this mutant cell line. These results suggest an important role played by DNA DSBs at the initial stage of asbestos injury.