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石墨镶嵌Co纳米晶的形成及其特性 总被引:5,自引:0,他引:5
用直流碳弧法在阳极石墨棒中加入金属Co产生石墨镶嵌Co纳米晶,研究在复合石墨棒中加入不同的Co含量对石墨镶嵌Co纳米晶的形貌、结构特性及晶粒尺寸分布的影响,探讨石墨镶嵌Co纳米晶的形成原因及碳弧法中氦气压力和Co含量对掺Co阳极石墨棒所产生的碳灰的C60/70产率的影响。结果表明,复合阳极棒中的Co含量决定了石墨镶嵌Co纳米晶的数量和晶凿直径分布,碳弧法中的He气压力仍是影响掺Co阳极棒所产生的碳 相似文献
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The volatilization behavior of Cu, Pb, Sn, Sb, Ni, Zn, Mn, Co, Cr, Cd during pyrolysis of waste printed circuit boards was investigated in a bench-scale fixed-bed pyrolysis system. It was found that volatility of heavy metals increases with operating temperature elevating, and bromine and vacuum have an obvious promoting effect on volatility of most of heavy metals. Over 99% weight of Cu and Ni are still remained in solid residue after pyrolysis, about 20% weight of Sb, Zn and Cd are transfered into liquid and gas during a pyrolysis process at 600 ℃, volatilization fractions of Pb, Sn, Mn, Co, Cr are less than 10% at the same conditions. The contents of heavy metals in liquid and gas products depend on not only volatility of metals, but also their initial contents in printed circuit boards, pyrolysis liquid and gas are primarily contaminated by Cu, Pb, Sn, Sb and Zn, their contents in liquid vary from 10^2 to 10^3 pg/mL, Mn, Co, Cr, Cd were detected only at very low level, less than 10 μg/mL. 相似文献
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Considering that the controller feedback gain and the observer gain are of additive norm-bounded variations, a design method of observer-based H-infinity output feedback controller for uncertain Delta operator systems is proposed in this paper. A sufficient condition of such controllers is presented in linear matrix inequality (LMI) forms. A numerical example is then given to illustrate the effectiveness of this method, that is, the obtained controller guarantees the closed-loop system asymptotically stable and the expected H-infinity performance even if the controller feedback gain and the observer gain are varied. 相似文献
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Topical Web crawling is an established technique for domain-specific information retrieval. However, almost all the conventional topical Web crawlers focus on building crawlers using different classifiers, which needs a lot of labeled training data that is very difficult to label manually. This paper presents a novel approach called clustering-based topical Web crawling which is utilized to retrieve information on a specific domain based on link-context and does not require any labeled training data. In order to collect domain-specific content units, a novel hierarchical clustering method called bottom-up approach is used to illustrate the process of clustering where a new data structure, a linked list in combination with CFu-tree, is implemented to store cluster label, feature vector and content unit. During clustering, four metrics are presented. First, comparison variation (CV) is defined to judge whether the closest pair of clusters can be merged. Second, cluster impurity (CIP) evaluates the cluster error. Then, the precision and recall of clustering are also presented to evaluate the accuracy and comprehensive degree of the whole clustering process. Link-context extraction technique is used to expand the feature vector of anchor text which improves the clustering accuracy greatly. Experimental results show that the performance of our proposed method overcomes conventional focused Web crawlers both in Harvest rate and Target recall. 相似文献