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101.
Pijush Kanti Mandal Rabindranath Majumdar Kalyan Kumar Mukherjee Omprakash Chakrabarti Himadri Sekhar Maiti 《Journal of Porous Materials》2009,16(2):157-163
Stems of Jute (Corchorus capsularis L.) and sticks of Cane (Calamus rotang L.), plants of immense economic importance in the Indian subcontinent, were converted into carbonaceous perform (C-preform)
maintaining the circular cylindrical shapes in lengths of 0.02–0.05 m by controlled thermal processing. Plant material precursors
were characterized by analysis of elemental (C, H, N) and molecular (cellulose, hemicellulose, lignin) compositions, by determination
of Bulk Density (BD) and ash content and by optical microscopy and X-ray diffractometry (XRD). C-preforms were also characterized
by measurement of BD and by Scanning Electron Microscopy (SEM) and XRD. The C-preforms were further subjected to infiltration
with Si-melt (1823–1923 K) under vacuum. Spontaneous infiltration and reaction yielded composite ceramics preserving the morphology
of native Jute Stem (JS) and Cane Stick (CS) precursors on macro and micro scale. The materials were found to be duplex composites
with Si and β-SiC as crystalline phases. The end ceramics were characterized by measurement of BD, and also by SEM and by
XRD. Measured mean BD of the Si/SiC composites derived from JS and CS were 2190 Kg m−3 and 2250 Kg m−3. The respective volume fractions of large diameter (>100 μm) bulk pores were 0.134 and 0.204, in the composites derived from
JS and CS. Taking into account the measured volume fraction internal pores of 0.11 and 0.149, the volume fractions of SiC
were calculated to be 0.136 and 0.307 in the composites derived from JS and CS respectively, closely tallying with those calculated
from the C-preform bulk densities. The cellular Si/SiC ceramics derived from JS and CS having special morphologies with long
and large porous channels and oriented growth of constituent phases are likely to be suitable for devices such as high temperature
insulators, catalyst support structures for gas phase reactions at elevated temperatures, molten metal filters and others. 相似文献
102.
This paper presents computer generated design data in terms of load capacity and oil flow for multirecess hydrostatic journal bearings. The Reynolds equation for a finite bearing was solved on a high speed digital computer satisfying appropriate boundary conditions and using the finite difference method. Results for various L/D ratios, recess to bearing area ratios, number of recesses etc are presented for capillary and orifice compensated bearings. 相似文献
103.
Amit Arya Dipak K. Majumdar Dharam Pal Pathak Anil K. Sharma Alok R. Ray 《Drug development and industrial pharmacy》2017,43(2):305-318
Colon-targeted microparticles loaded with a model anti-inflammatory drug were fabricated using especially designed acrylic acid–butyl methacrylate copolymers. Microparticles were prepared by oil-in-oil solvent evaporation method using Span 80 as emulsifier. Microparticles were found to be spherical in shape, hemocompatible and anionic with zeta potential of ?27.4 and ?29.0?mV. Entrapment of drug in the microparticles was confirmed by Fourier transform infrared (FTIR) spectroscopy. However, X-ray diffraction (XRD) and differential scanning calorimetry (DSC) revealed amorphous nature of microparticles due to the dilution effect of amorphous polymer. The microparticles released less than 5% drug at pH 1.2, while more than 90% of the drug load was released at pH 7.4. This suggested the colon targeting nature of the formulations. In experimentally developed colitis in Wistar rats, the microparticle formulation showed significant reduction (p?.05) in the disease activity score (disease symptoms), the colon-to-body weight ratio (tissue edema) and the myeloperoxidase, tumor necrosis factor (TNF)-α and interleukin (IL)-1β activities. 相似文献
104.
Patial Payal Deshwal Manish Kumar Naveen 《Journal of Materials Science: Materials in Electronics》2022,33(15):11768-11782
Journal of Materials Science: Materials in Electronics - Present study portrays, physicochemical investigations of pristine and Pd2+ modified ZnO nanoflowers (NFs) compositional series... 相似文献
105.
The concept of deep dictionary learning (DDL) has been recently proposed. Unlike shallow dictionary learning which learns single level of dictionary to represent the data, it uses multiple layers of dictionaries. So far, the problem could only be solved in a greedy fashion; this was achieved by learning a single layer of dictionary in each stage where the coefficients from the previous layer acted as inputs to the subsequent layer (only the first layer used the training samples as inputs). This was not optimal; there was feedback from shallower to deeper layers but not the other way. This work proposes an optimal solution to DDL whereby all the layers of dictionaries are solved simultaneously. We employ the Majorization Minimization approach. Experiments have been carried out on benchmark datasets; it shows that optimal learning indeed improves over greedy piecemeal learning. Comparison with other unsupervised deep learning tools (stacked denoising autoencoder, deep belief network, contractive autoencoder and K-sparse autoencoder) show that our method supersedes their performance both in accuracy and speed. 相似文献
106.
Pushkar Dasika Debadarshini Samantaray Krishna Murali Nithin Abraham Kenji Watanbe Takashi Taniguchi N Ravishankar Kausik Majumdar 《Advanced functional materials》2021,31(13):2006278
The gate-all-around nanowire transistor, due to its extremely tight electrostatic control and vertical integration capability, is a highly promising candidate for sub-5 nm technology nodes. In particular, the junctionless nanowire transistors are highly scalable with reduced variability due to avoidance of steep source/drain junction formation by ion implantation. Here a dual-gated junctionless nanowire p-type field effect transistor is demonstrated using tellurium nanowire as the channel. The dangling-bond-free surface due to the unique helical crystal structure of the nanowire, coupled with an integration of dangling-bond-free, high quality hBN gate dielectric, allows for a phonon-limited field effect hole mobility of 570 cm2 V−1 s−1 at 270 K, which is well above state-of-the-art strained Si hole mobility. By lowering the temperature, the mobility increases to 1390 cm2 V−1 s−1 and becomes primarily limited by Coulomb scattering. The combination of an electron affinity of ≈ 4 eV and a small bandgap of tellurium provides zero Schottky barrier height for hole injection at the metal-contact interface, which is remarkable for reduction of contact resistance in a highly scaled transistor. Exploiting these properties, coupled with the dual-gated operation, we achieve a high drive current of 216 μA μm−1 while maintaining an on-off ratio in excess of 2 × 104. The findings have intriguing prospects for alternate channel material based next-generation electronics. 相似文献
107.
B.C. Majumdar 《Wear》1973,24(1):15-22
Theoretical studies of rotating externally pressurized gas bearings with multiple pressure sources have been made. The solution is obtained for finite bearings by using pressure perturbation theory. Theoretical results are compared with experimental data. The theory allows good prediction of bearing load capacity, stiffness and attitude angle. 相似文献
108.
Electrode Dependence of Tunneling Electroresistance and Switching Stability in Organic Ferroelectric P(VDF‐TrFE)‐Based Tunnel Junctions
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Sayani Majumdar Binbin Chen Qi Hang Qin Himadri S. Majumdar Sebastiaan van Dijken 《Advanced functional materials》2018,28(15)
Ferroelectric tunnel junctions (FTJs) are promising candidates for nonvolatile memories and memristor‐based computing circuits. Thus far, most research has focused on FTJs with a perovskite oxide ferroelectric tunnel barrier. As the need for high‐temperature epitaxial film growth challenges the technological application of such inorganic junctions, more easily processable organic ferroelectrics can serve as alternative if large tunneling electroresistance (TER) and good switching durability would persist. This study reports on the performance of FTJs with a spin‐coated ferroelectric P(VDF‐TrFE) copolymer tunnel barrier. The use of three different bottom electrodes, indium tin oxide (ITO), La0.67Sr0.33MnO3, (LSMO), and Nb‐doped SrTiO3 (STO) are compared and it is shown that the polarity and magnitude of the TER effect depend on their conductivity. The largest TER of up to 107% at room temperature is measured on FTJs with a semiconducting Nb‐doped STO electrode. This large switching effect is attributed to the formation of an extra barrier over the space charge region in the substrate. The organic FTJs exhibit good resistance retention and switching endurance up to 380 K, which is just below the ferroelectric Curie temperature of the P(VDF‐TrFE) barrier. 相似文献
109.
Cu-(Sn37Pb) and Cu-(Sn3.5Ag0.5Cu) solder joints were prepared at the same reflow temperature of 230 °C. The microstructural observation of the solder assemblies in scanning and transmission electron microscopes confirmed the presence of η-Cu6Sn5 in case of the former, and Cu3Sn + η-Cu6Sn5 for the latter in the reaction zone. The findings are correlated with the electrical and mechanical properties of the joints. Lead free solder-Cu joint exhibited lower reaction zone thickness and improved electrical conductivity (0.28 × 106Ω− 1 cm− 1) and shear strength ∼ 68MPa compared to conventional lead-tin solder-Cu joint. The latter showed electrical conductivity and shear strength of 0.22 × 106Ω− 1 cm− 1 and ∼ 55 MPa, respectively. The difference in reaction zone thickness is explained on the basis of melt superheat, with Sn being the primary diffusing species in the intermetallic layer. 相似文献
110.
We demonstrate two-dimensional multiplexed real-time, label-free antibody-antigen binding assays by optically detecting nanoscale motions of two-dimensional arrays of microcantilever beams. Prostate specific antigen (PSA) was assayed using antibodies covalently bound to one surface of the cantilevers by two different surface chemistries, while the nonreaction surfaces were passivated by poly(ethylene glycol)-silane. PSA as low as 1 ng/mL was detected while 2 mg/microl of bovine serum albumin induced only negligible deflection on the cantilevers. 相似文献