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991.
K M Cooper L Ribeiro P Alves V Vozikis S Tsitsamis G Alfredsson T L?vgren M Tuomola H Takalo A Iitia S S Sterk M Blokland D G Kennedy 《Food Additives & Contaminants》2003,20(9):804-812
Many zeranol immunoassay test kits cross-react with toxins formed by naturally occurring Fusarium spp. fungi, leading to false-positive screening results. This paper describes the evaluation and application of recently published, dry reagent time-resolved fluoroimmunoassays (TR-FIA) for zeranol and the toxin alpha-zearalenol. A ring test of bovine urine fortified with zeranol and/or alpha-zearalenol in four European Union National Reference Laboratories demonstrated that the TR-FIA tests were accurate and robust. The alpha-zearalenol TR-FIA satisfactorily quantified alpha-zearalenol in urine fortified at 10-30 ng ml(-1). The specificity-enhanced zeranol TR-FIA accurately quantified zeranol in the range 2-5 ng ml(-1) and gave no false-positive results in blank urine, even in the presence of 30 ng ml(-1) alpha-zearalenol. Zeranol TR-FIA specificity was demonstrated further by analysing incurred zeranol-free urine samples containing natural Fusarium spp. toxins. The TR-FIA yielded no false-positive results in the presence of up to 22 ng ml(-1) toxins. The performance of four commercially available zeranol immunoassay test kits was more variable. Three kits produced many false-positive results. One kit produced only one potential false-positive using a protocol that was longer than that of the TR-FIA. These TR-FIAs will be valuable tools to develop inspection criteria to distinguish illegal zeranol abuse from contamination arising from in vivo metabolism of Fusarium spp. toxins. 相似文献
992.
993.
Jean Poerre 《钢铁》2003,38(Z1):101-103
全球变暖给钢铁工业带来了巨大的挑战,挑战涉及使用碳的多少和能量利用率.低强度生产可以短期内达到减轻排放,使处于京都协议要求的水平.从中期看,更多地使用废钢也有助于减轻排放.但是为了实现更多地减少温室气体GHG的排放,也即等于实现京都协议之后的排放目标,钢铁工业必须设想有一个新的生产面貌,这形成了未来时期对它的最大挑战.碳的收集和吸收,碳使用中的代用剂,工艺流程中绿色来源的电和氢的应用,这些在未来10年中是必须要发展的,希望通过广泛地国际合作加以实现. 相似文献
994.
O'Driscoll Michael P.; Poelmans Steven; Spector Paul E.; Kalliath Thomas; Allen Tammy D.; Cooper Cary L.; Sanchez Juan I. 《Canadian Metallurgical Quarterly》2003,10(4):326
This study examined organizational family-responsive policies, perceptions of the organization as family supportive, and supervisor support as issues that may be salient to the experience of conflict between paid employment (work) and family roles. Data were collected from 355 managerial personnel in New Zealand. Although work-family conflict and psychological strain were strongly linked, the availability of organizational policies had no significant association with levels of conflict or strain, whereas policy usage was related only to work-to-family interference and not to family-to-work interference. On the other hand, perceptions of the organization as family supportive and supervisor support for work-family balance displayed significant relationships with key variables, highlighting the importance of these variables for interventions designed to ameliorate the negative impact of work-family conflict on managerial well-being. Implications for the effective implementation of family-responsive interventions are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
995.
Malik Mary L.; Beutler Larry E.; Alimohamed Shabia; Gallagher-Thompson Dolores; Thompson Larry 《Canadian Metallurgical Quarterly》2003,71(1):150
The definition of an empirically supported treatment (EST) arguably embodies 2 untested assumptions: (a) that different manualized renditions of the same therapy are functionally equivalent and (b) that therapies can be reliably applied independently of therapist, setting, and format. These assumptions were tested as applied to cognitive therapy (CT), using process data from a large multisite study (N=235) that included 3 cognitive and 6 alternative therapies. Although the non-CTs were more variable than the CTs on 2 of 4 dimensions studied (directiveness and emotional arousal), there was considerable variation among the 3 CTs, even when implemented in the current context of rigorous training, manualization, and adherence checks. Results are discussed as related to the assumptions underlying EST criteria. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
996.
A motivational model of rural students' intentions to persist in, versus drop out of, high school. 总被引:1,自引:0,他引:1
Using self-determination theory, the authors tested a motivational model to explain the conditions under which rural students formulate their intentions to persist in, versus drop out of, high school. The model argues that motivational variables underlie students' intentions to drop out and that students' motivation can be either supported in the classroom by autonomy-supportive teachers or frustrated by controlling teachers. LISREL analyses of questionnaire data from 483 rural high school students showed that the provision of autonomy support within classrooms predicted students' self-determined motivation and perceived competence. These motivational resources, in turn, predicted students' intentions to persist, versus drop out, and they did so even after controlling for the effect of achievement. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
997.
Thin-film nickel coatings on fiber materials 总被引:1,自引:0,他引:1
L. M. Lyn’kov V. A. Bogush E. A. Senkovets S. M. Zavadskii 《Technical Physics Letters》2003,29(8):641-642
Vacuum deposition of thin films onto fiber materials is a promising method of obtaining electromagnetic screens. We have studied the structure and the electromagnetic properties of machine-knitted fabric coated with nickel by means of magnetron sputtering. When the fabric is irradiated from the metal-coated side, the reflection coefficient is higher by a factor of 1.4 as compared to the case when the same source of electromagnetic radiation is situated on the opposite side (facing the uncoated surface), while the absorption coefficient in both cases is the same. 相似文献
998.
999.
Titanium oxides were reduced to metallic titanium using the liquid calcium floating on the molten CaCl2. A part of Ca dissolved into CaCl2 and reacted with TiO2 settled below CaCl2. The by-product CaO also dissolved by about 20 mol pct into CaCl2, which was effective in reducing the oxygen concentration in the obtained Ti particles. The compositional region in the Ca-CaCl2-CaO system was examined for the less oxygen contamination in Ti and the better handling in leaching. A large amount of the
residual calcium oxidized the titanium powder in leaching. The metallic Ti powder less than 1000 mass ppm oxygen could be
obtained only for 3.6 ks using 5 to 7 mol pct Ca-CaCl2 at 1173 K. The powder was slightly sintered like sponge, and contained approximately 1500 ppm Ca. The anatase phae, the intermediate
product in the refining process of TiO2, could be also supplied as raw material as well as rutile. 相似文献
1000.
The corrosion behaviour of nitrogen-containing austenitic stainless steel in methanol containing different concentrations
of H2SO4, HCl, LiCl and H2SO4 + HCl has been investigated using a potentiostatic polarization method. The cathodic reaction in the H2SO4, HCl and H2SO4 + HCl solutions was proton reduction whereas in the neutral LiCl solution, oxygen reduction was the predominant cathodic
reaction. Active, passive and transpassive behaviours were observed only for higher concentrations of H2SO4 (0.01–2.0 M) due to the inherent water content. A cathodic loop, characterized by measured negative current in the anodic
region, was also observed in solutions, in which the concentration of H2SO4 was 1.0 M or higher. The relative stability of the passive films decreased as the H2SO4 concentration increased, and thus the steel suffered from mild pitting corrosion. In the chloride environment, the rate of
corrosion increased as the Cl− ion concentration increased. The presence of acid along with Cl− ions enhanced corrosion, and the corrosion rate increased significantly. The steel suffered from mild intergranular corrosion
in acidic chloride solutions of methanol. In the H2SO4 + HCl solutions, passive films were only formed when the H2SO4 to HCl concentration ratio was greater than ∼10:1. 相似文献