Controlled Synthesis of Ag2S,Ag2Se,and Ag Nanofibers by Using a General Sacrificial Template and Their Application in Electronic Device Fabrication

Nanofiber bundles of Ag₂S, Ag₂Se, and Ag have been successfully synthesized by making use of Ag₂C₂O₄ template nanofiber bundles, utilizing both anion‐exchange and redox reactions. The obtained bundles were polycrystalline nanofibers composed of nanoparticles in which the precursor morphology was well‐preserved, indicating that Ag₂C₂O₄ nanofiber bundles acted as a general sacrificial template for the synthesis of silver‐based semiconductor and metal nanofibers. Dispersing media and transforming reactants were found to be key factors influencing the chemical transformation in the system. In particular, separate single‐crystalline Ag nanofibers were obtained via a nontemplate route when ascorbic acid was used as a relatively weak reductant. An electrical transfer and switching device was built with the obtained Ag₂S and Ag nanofiber bundles, utilizing the unique ion‐conductor nature of Ag₂S and revealing their potential applications in electronics.     

A 3-D Enlarged Cell Technique (ECT) for the Conformal FDTD Method

In this paper, we present an enlarged cell technique (ECT) to avoid the time step reduction encountered in the conformal finite-difference time-domain (CFDTD) method due to small irregular cells truncated by metallic boundaries. We focus our efforts on the discussion of the accuracy and stability of the ECT and its comparison with other conformal methods, especially the one called the uniformly stable conformal (USC) method. We also provide a simplified ECT, which is much easier to implement. In the ECT, a stability criterion is first constructed to identify instable irregular cells, i.e., those having so small an area to cause instability. Those instable cells are then enlarged into their adjacent cells to obtain a large, stable area. Careful treatment is performed on the communication between the intruding and intruded cells in terms of electromotive force by keeping the total electromotive force conservative. This technique is verified by several 3-D numerical experiments. Results show that the ECT is second-order accurate and numerically stable at the regular Courant time step limit.     

负载型固体碱催化合成亚苄基丙酮

研究了用固体碱 KOH/Al_2O_3催化合成苯叉丙酮,确定了合成的最佳工艺条件:n(苯甲醛)∶n(丙酮)=1∶4.催化剂用量2g,催化剂最佳负载量12mmol/g,反应温度40～45℃,反应时间为3h,产率达88%以上。     

Preparation and Properties of Rare Earth Modified Carbon Black/Natural Rubber Composites

The oxides Eu, Ho, Er and Dy were used to prepare the hydroxides of rare earth modified carbon black. Then natural rubber latex （NRL） was added into the reactor. The system reacted at 85 ℃ with stirring for 1 h to prepare powdered HAF-Ln（OH）3/NR composites. The effects of the kind and content of Ln on the particle size distribution of P [ NR/HAF-Ln （OH）3 ] and mechanical properties of its vulcanizate were studied respectively. It is found that rare earth can help to get the powder of the composite, the product particle with a diameter less than 0.9mm will be get when the composites containing the compound of Ho, Er and Dy with dosage of 1.0, 1.0, O. 5 percent, respectively. The adding of Ln can improve the tensile strength and tear strength of the vulcanizate effectively, what＇s more, Er and Dy can decrease the permanent set of vulcanizate significantly. The SEM studies shows that P[ NR/HAF-Dy （OH）3 ] vulcanizate shows superior mechanical properties that depend primarily on the absence of free carbon black, the fine dispersion of carbon black in the rubber matrix and better polymer-filler interaction.     

无纸化建造

本文通过分析先锋建筑师借鉴汽车制造领域的无纸化技术进行的建造实践,揭示了无纸化建造的操作过程,并探讨了无纸化建造的意义,那就是无纸化不仅改变了传统的设计方法,而且改变了传统的建造方式,这将是人类的建造技术发展史上的一场伟大的变革.文章最后探讨了无纸化建造在中国的实践意义.     

河北省水安全现状分析及对策探讨

从水资源与水环境两方面分析了河北省水安全的现状,指出影响水安全的因素在于自然因素、人为因素及人与自然的不协调因素,并针对水安全问题可能引发的健康安全、粮食安全、经济安全、生态环境安全进行了讨论,最后探讨了解决河北省水安全问题的对策。     

苏北-南黄海盆地构造演化

苏北及南黄海盆地是由多期、多类盆地叠加的复合残留盆地,地质概况基本相似,成因演化近同,自元古界下扬子板块形成后,主要经历了古-中生代地台、中生代前陆盆地、走滑拉分盆地时期以及新生代断陷、坳陷盆地时期.在古生代-中生代发展过程中是一个整体,晚白垩世盆地演化出现分化,发育伸展盆地群,形成一系列叠置在中、古生代盆地之上的箕状断陷,箕状断陷的发育及分布明显受中-古生界内部先存逆冲断裂的控制.     

新的启迪

说点心里的话，建筑设计对青年人来讲是一条漫长的道路。建筑是一个载体，有精神一面，也有物质一面。有些建筑师拿着模型或未建成的设计来炒作，为了求名，生怕别人不知道。这对个人是小事，但若贻误了青年学子，那就是不可取的。     

韶关电厂9#200MW机组DEH控制系统的改造

在对韶关电厂200MW机组DEH系统改造过程中，控制系统采用数字式电液控制系统(DEH)，汽机基本控制部分采用一对互为冗余数据处理单元(DPU)完成，并采用专用的硬件来实现超速控制和超速保护功能。汽机保护系统(ETS)采用独立的系统可编程控制器PLC来实现。     

Structured optimal and robust control with multiple criteria: a convex solution

In this paper, the design of controllers that incorporate structural and multiobjective performance requirements is considered. The control structures under study cover nested, chained, hierarchical, delayed interaction and communications, and symmetric systems. Such structures are strongly related to several modern-day and future applications including integrated flight propulsion systems, platoons of vehicles, micro-electro-mechanical systems, networked control, control of networks, production lines and chemical processes. It is shown that the system classes presented have the common feature that all stabilizing controllers can be characterized by convex constraints on the Youla-Kucera parameter. Using this feature, a solution to a general optimal performance problem that incorporates time domain and frequency domain constraints is obtained. A synthesis procedure is provided which at every step yields a feasible controller together with a measure of its performance with respect to the optimal. Convergence to the optimal performance is established. An example of a multinode network congestion control problem is provided that illustrates the effectiveness of the developed methodology.