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861.
Electrodeposition of conducting polyaniline (Pani) was made under potentiostatic condition at pH 1.0 in different electrolyte media (H2SO4 and HClO4) in the absence and presence of two organic dopants, disodium salts of naphthalene-1,5-disulphonic acid (NSA) and of catechol-3,5-disulphonic acid (CSA). The rate and yield of Pani deposition were dependent on the acid medium and the dopant employed. NSA in H2SO4 caused an increase in rate and yield but CSA decrease when compared to the rate and yield of H2SO4 alone. In HClO4 medium, both the dopants showed a decrease. With regard to DC electrical conductivity, both the dopants exhibited an enhancement in H2SO4 medium but NSA a decline in HClO4. Characterisation of the electrosynthesised polymer samples by various instrumental techniques (cyclic voltammetric: CV, FTIR, UV-Visible: UV-Vis, EPR, XRD, TGA and DTG methods) revealed that between the two acid media, H2SO4 was the better one. Further, it enlightened the role of two organic dopants in relation to the acid media. The advantageous role of NSA in H2SO4 had origin on its molecular characteristics such as non-polarity, larger π-electron cloud etc., while CSA could not perform such a role because of its easily oxidisable hydroxyl groups. In HClO4, however, both the dopants could play only an unfavourable role owing to its greater polarity and oxidizing power than H2SO4. 相似文献
862.
A. Pizzinat B.S. Marks L. Palmieri C.R. Menyuk A. Galtarossa 《Photonics Technology Letters, IEEE》2003,15(6):819-821
We consider the two Wai-Menyuk models of birefringence in periodically spun fibers, and we show that the differential group delay differs significantly for the two models when the spin period approaches or exceeds the fiber beat length. When the fiber correlation length is large, we explain this difference quantitatively, and we explain it qualitatively for any fiber correlation length. 相似文献
863.
Sensitivity analysis of simulations for magnetic particle inspection using the finite-element method 总被引:2,自引:0,他引:2
Lee J.Y. Lee S.J. Jiles D.C. Garton M. Lopez R. Brasche L. 《IEEE transactions on magnetics》2003,39(6):3604-3606
Magnetic particle inspection (MPI) is widely used for nondestructive evaluation in aerospace applications in which interpretation of inspection results is currently limited to empirical knowledge and experience-based approaches. Advances in computational magnetics, particularly the use of finite-element calculations, have enabled realistic numerical simulations of magnetic particle inspection to be undertaken with complicated geometries. In this paper, we report a sensitivity analysis using finite-element-method simulations of magnetic particle inspection for defects with various sizes and geometries. As a result, improved quantitative understanding of the MPI technique and factors that affects its sensitivity and reliability has been achieved. These results can be used to optimize conditions for conducting these inspections and should lead to improvement in analysis and interpretation of experimental results. 相似文献
864.
A review of optical, chemical, and biological sensors to detect metabolic activity at the single-cell level is presented in the context of the development of lab-on-a-chip research instrumentation. The sensors reviewed include optical sensors, at both research and commercial levels, that can optically detect intracellular metabolites including adenosine triphosphate, nicotinamide-adenine dinucleotide, reduced flavin adenine dinucleotide, and other metabolites, including oxygen, carbon dioxide, and glucose. Methods to optically detect pH changes which are a general indicator of activity in extracellular space are also briefly reviewed. Performance metrics such as sensitivity, sensor size, drift, time response, and sensing range are included when available. Highly suitable optical sensor technologies for monitoring cellular metabolic activity include luminescent (fluorescent, phosphorescent, and chemiluminescent) and colorimetric optical probes. Different approaches to extracting luminescent and colorimetric information are reviewed, including benchtop techniques, fiber-optic approaches, and the use of probes encapsulated by biologically localized embedding. A brief discussion of alternate optical sensor technologies, such as surface plasmon resonance and infrared absorption spectroscopy, is also presented. 相似文献
865.
Gkatzianas M.A. Balanis C.A. Diaz R.E. 《Microwave and Wireless Components Letters, IEEE》2004,14(5):219-221
This paper proposes an alternative expression for the in-cell capacitance of a photoelectrical cell (PEC)-mounted slot, which is the conceptual cornerstone of the Gilbert-Holland subcell finite difference time domain (FDTD) model. By treating a slightly modified electrostatic problem, the extraneous charge singularity on the PEC edges touching the cell, which is characteristic of the originally proposed model, is removed. The latter offers better physical grounds for a new expression of the capacitance and the effective permittivity used in the update equations. High resolution standard FDTD simulation results are presented in support of the new expression. 相似文献
866.
867.
Peretto L. Sasdelli R. Tinarelli R. 《IEEE transactions on instrumentation and measurement》2003,52(4):1143-1147
A statistical approach to estimate the trend, over a long time interval, of electrical parameters is proposed in this paper. The trend is determined by processing a limited number of parameter values measured at instants randomly chosen. Experimental results are reported, which show the good performance of the method proposed when it is applied to estimate customers' loads profiles and the trend of some parameters providing information on power quality. 相似文献
868.
The stress-whitened damage zone that formed ahead of a semicircular notch during slow tensile loading has been measured from
optical micrographs of translucent blends of poly(vinyl chloride) (PVC) with experimental chlorinated polyethylene (CPE) resins.
When the zone was small, the plane strain condition applied and from the elastic stress distribution a constant mean stress
condition was found at the boundary of the crescent-shaped zone. The critical mean stress did not depend on the chlorine content
or the chlorine distribution of the experimental CPE resin used in the blend. While the critical mean stress decreased as
the amount of CPE in the blend was increased, the critical volume strain, calculated from the bulk modulus, was independent
of composition and was thought to be the controlling parameter for stress-whitening. When the zone was larger, the shape was
qualitatively described by concepts of stress redistribution in the presence of a plastic zone ahead of the notch. Macroscopic
flow and necking were only detected near the maximum in the stress-displacement curve. 相似文献
869.
R. R. Zahran 《Journal of Materials Science》1991,26(21):5693-5697
The corrosion behaviour of experimentally prepared copper-reinforced carbon electrodes in dilute hydrochloric acid is investigated. The electrodes are not only directly attacked by the acid, but they are also subjected to galvanic corrosion. The baking temperature and time are the most crucial processing variables. A minimum in the corrosion rate is always achieved when the electrodes are baked at 400 °C for 1.5 h, the level depending on the copper content. The corrosion resistance increases progressively with the baking temperature as long as the baking time is less than 1.5 h. Baking for more than 1.5 h results in increasing corrosion rate. The presence of copper increases the corrosion resistance of the prepared electrodes. 相似文献
870.