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81.
82.
J. R. Díaz-Estrada E. Camps L. Escobar-Alarcón J. A. Ascencio 《Journal of Materials Science》2007,42(4):1360-1368
Deposition of Ti was carried out by laser ablation onto hydroxyapatite porous discs in an Ar atmosphere. Ti nanoparticles
were deposited onto HAp surface in order to modify its roughness and morphology as it is observed by scanning electron microscopy
(SEM) and scanning probe microscopy (SPM). A homogeneous distribution of Ti over the disc surface was corroborated by elemental
mapping. A comparison of the hydroxyapatite hardness before and after deposition was performed using SPM nanoindentation.
Transmission Electron Microscopy (TEM) showed that the Ti nanoparticles obtained were covered by an oxygen shell. It is shown
that surface modifications of the covered HAp by Ti result in better mechanical properties, reducing the possible damage to
the HAp ceramic by friction or impacts as it often happens in meniscus, bone junctions and the inclusion of prosthesis for
human treatments. 相似文献
83.
In this paper we consider A(θ)-stable finite difference methods for numerical solutions of dissipative partial differential equations of parabolic type.
Combining two rational approximation methods with different orders of accuracy, where the lower order method is applied n
0 times (n
0 fixed) at each time step, we prove the existence of a second order method which is contractive for all time steps. Moreover,
we shed light on the conditions on the lower order method which are sufficient (and sometimes necessary) to obtain the optimal
order of accuracy. For the one-dimensional heat equation we construct a family of numerical methods which are contractive
in the maximum norm for all values of the discretization parameters. We also present numerical examples to illustrate our
results.
Received: May 2002 / Accepted: January 2003 相似文献
84.
M. Del C. Ruiz J. A. González J. B. Rivarola 《Metallurgical and Materials Transactions B》2004,35(3):439-448
The mechanism and kinetics of β-Ta2O5 chlorination, mixed with sucrose carbon, have been studied by a thermogravimetric technique. The investigated temperature
range was 500 °C to 850 °C. The reactants and reaction residues were analyzed by scanning electronic microscopy (SEM), X-ray
diffraction (XRD), and Brunauer-Emmett-Teller method for surface area (BET). The effect of various experimental parameters
was studied, such as carbon percentage, temperature, chlorine partial pressure, and flow, use of the multiple sample method,
and carbon previous oxidation. The carbon percentage and previous treatment have an effect on the system reactivity. The temperature
has a marked effect on the reaction rate. In the 500 °C to 600 °C temperature interval, the apparent activation energy is
144 kJ/mol of oxide, while at higher temperatures, the activation energy decreases. With high chorine partial pressures, the
order of reaction is near zero. The kinetic contractile plate model, X=kt, considering carbon oxidation as the controlling stage, is the one with the best fit to the experimental data. A probable
mechanism for the carbochlorination of β-Ta2O5 is proposed: (1) activation of chlorine on the carbon surface, (2) chlorination of Ta2O5, (3) oxidation of carbon, and (4) recrystallization of β-Ta2O5. 相似文献
85.
Peter Eaton Andrea Ragusa Caroline Clavel Cristina T Rojas Paul Graham Raúl V Durán Soledad Penadés 《IEEE transactions on nanobioscience》2007,6(4):309-318
Glyconanoparticles which present carbohydrate and amino groups motifs at their surface were produced. These particles were highly stable and soluble in aqueous solutions. The presence of the carbohydrate groups also allowed the inclusion of more strongly binding groups, without affecting solubility. The binding of a model DNA, plasmid by these nanoparticles was studied by atomic force microscopy, transmission electron microscopy, and gel electrophoresis. Significant differences between the nanoparticles based on their affinities for the DNA were found, with implications for their potential use as nonviral gene delivery agents. 相似文献
86.
András Ványolos Balázs Dóra Attila Virosztek 《Journal of Superconductivity and Novel Magnetism》2007,20(7-8):643-645
We report of a theoretical study on quasi-one dimensional unconventional charge density wave (UCDW) driven by electron–phonon
interaction. Within mean field theory, we find that the wavevector dependence of the coupling leads to a momentum dependent
single particle gap on the Fermi surface. The presence of small energy single particle excitations around the gap nodes significantly
changes the optical conductivity compared to the conventional CDW result. In addition to that, the collective phase excitation
arising from fluctuation of the order parameter leads to further qualitative changes of the conductivity and results in an
effective mass that is nonmonotonic in temperature.
相似文献
87.
Corrosion rates were measured at the exposed spots of rebars near three corners of Muddy Creek Bridge located in northern West Virginia using a 3LP device. Also, chloride contents of the concrete samples taken from the vicinity of the spots were analyzed using a wet chemical method that had been developed in this study. The average corrosion rate over the three spots was 4.66 mA/m2, which is in the range of corrosion damage possible in 10–15 years. The average chloride content of the concrete over the three spots was 703 parts per million (ppm), which is well above the threshold limit value of 260 ppm. Although the corrosion rate measurement method using a 3LP device is by manual operation, it is found to be reliable and effective, and, thus, recommended for future studies of this kind of research. The wet chemical method developed in this study is found to be effective. 相似文献
88.
We present some new lower bounds on the optimal information rate and on the optimal average information rate of secret sharing schemes with homogeneous access structure. These bounds are found by using some covering constructions and a new parameter, the k-degree of a participant, that is introduced in this paper. Our bounds improve the previous ones in almost all cases. 相似文献
89.
Francisco Jos Alguacil Concepcin Caravaca María Isabel Martín 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2003,78(10):1048-1053
The transport of chromium(VI) through a flat‐sheet supported liquid membrane containing Cyanex 921 as a carrier has been investigated. The permeation of the metal is investigated as a function of various experimental variables: hydrodynamic conditions, concentration of chromium(VI) and HCl in the feed phase, carrier concentration and diluent in the membrane and strippant concentration in the stripping phase. The mass transfer coefficient and the thickness of the aqueous boundary layer were calculated from the experimental data. Furthermore, the selectivity of Cyanex 921‐based flat‐sheet supported liquid membrane towards different metal ions and the behaviour of the system against other carriers are presented. Copyright © 2003 Society of Chemical Industry 相似文献
90.