Effects of Y and Ce on Microstructures and Properties of Nb-Si System Composites

The effects of yttrium and cerium on microstructures and properties of Nb-Si system composites were investigated by scanning electron microscopy( SEM), energy dispersive spectrum(EDS), X-ray diffraction(XRD) and high temperature oxidation experiments.It is found that the coarse primary silicide phase became finer and more homogeneous with Y and Ce addition.The results of high temperature oxidation experiments show that the oxidation rates of NbSi system composites with an appropriate amount of Y and Ce decrease compared with those of alloys without Y or Ce addition, and oxidation products mainly distribute along the phase boundaries between the Nb solid solution and silicide.     

基于嵌入式Linux的远程数据采集系统

以嵌入式微控制器为核心,将传感器网络收集来的数据通过无线电发射机发送到远程接收机,从而实现远程数据采集.系统的优势是充分利用了短波无线链路资源,适合于工作在无人区等场合.以ARM7为控制器,功耗小,性能稳定,维护方便;通信方式采用串口通信,连接线少,实现相对简单.系统设计主要应用嵌入式μCLinux系统设计、无线电发射、调制解调器等方面的知识,文中给出了调制解调器拨号协议、系统原理和软件流程等.     

基于DSP+CPLD的高精度信号发生器

介绍了基于直接数字式频率合成(DDS)原理的全数字信号发生器(DSP),利用DSP芯片快速、高精度的运算优势以及CPLD芯片灵活的编程逻辑、大容量存储功能的特点,采用通用可编程芯片以及数字波形合成技术,形成高稳定、高精度、高动态的数字合成信号.该信号发生器可产生0～25 kHz的正弦波、三角波和方波,输出电压峰峰值为0～5 V,频率步进1 Hz,幅度步进0.001 V.     

基于PCI总线的高速多路数据传输卡设计

介绍了一套基于外部设备互连(PCI)总线的高速多路数据传输卡的设计,采用基于PCI内核与PCI用户逻辑相结合的新型设计方案,在顶层通过仿真来验证PCI接口以及用户逻辑设计正确与否.降低了设计的复杂程度,提高了电路的集成度和系统的性能,并根据PCI卡对外部设备驱动能力较弱的特点,在传输卡中加入了长线驱动功能,采用低电压差分信号(LVDS)技术,既降低了系统功耗,又实现长距离的计算机双向通信.     

WCDMA系统中SPT数字滤波器的一种设计方法

相对于传统的数字滤波器实现方法,符号的2次幂和(SPT)滤波器用移位寄存器替代乘法器,因而资源消耗少、速度快,更加适于专用集成电路(ASIC)设计.介绍了一种适用于宽带码分多址(WCDMA)前向信道中给定基带成形滤波器单位脉冲响应后设计SPT滤波器的方法.相对于传统的理想SPT系数优化方法,此方法更适于给定单位脉冲响应后SPT滤波器的设计,计算复杂度低;仿真结果显示,相对于更加简单的四舍五入方法,此算法在性能上又有可观的增益.     

（E）-2-壬烯酸合成方法的改进

(E)-2-壬烯酸是有机合成的一种重要中间体,我们利用Knoevenagel反应机理,改进了(E)-2-壬烯酸的合成工艺,在不使用脱水剂条件下,使用少量吡啶作催化剂,获得了83%的反应收率。     

各向异性损伤理论与复合材料层板损伤的实验研究(一)-各向异性损伤理论

本文讨论了各向异性损伤力学的基本概念并介绍了以应变等效性假设为基础的Lemaitre模型和以能量等效性假设为基础的Cordebois模型.在此基础上作者导出了两种损伤模型的损伤能释放率的表达式.文中作者定义了一维损伤时弹性材料板单元的一些损伤定义,并导出了两种模型在一维损伤时损伤能释放率Y₂的简单表达式,从而为复合材料层板损伤测量的实验研究提供了理论基础,     

Monodispersed thermoresponsive hydrogel microspheres with a volume phase transition driven by hydrogen bonding

We report the synthesis and characterization of monodispersed thermoresponsive hydrogel microspheres with a volume phase transition driven by hydrogen bonding. The prepared microspheres, composed of poly(acrylamide-co-styrene) (poly(AAM-co-St)) cores and poly(acrylamide)/poly(acrylic acid) (PAAM/PAAC) based interpenetrating polymer network (IPN) shells, were featured with high monodispersity and positively thermoresponsive volume phase transition characteristics with tunable swelling kinetics, i.e. the particle swelling was induced by an increase rather than a decrease in temperature. The monodisperse poly(AAM-co-St) seeds were prepared by emulsifier-free emulsion polymerization, the PAAM or poly(acrylamide-co-butyl methacrylate) (poly(AAM-co-BMA)) shells were fabricated on the seeds by free radical polymerization, and the core-shell microspheres with PAAM/PAAC based IPN shells were finished by a method of sequential IPN synthesis. The microsphere size increased with increasing both AAM and BMA dosages. The increase of hydrophilic monomer AAM dosage resulted in a better monodispersity, but the increase of hydrophobic monomer BMA dosage led to a worse monodispersity. With increasing the crosslinker methylenebisacrylamide (MBA) dosage, the mean diameter of the microspheres decreased and the monodispersity became better. An equimolar composition of AAC and AAM in the IPN shells of the microspheres resulted in a more complete shrinkage for the microspheres at temperatures lower than the upper critical solution temperature. Both BMA and MBA additions depressed the swelling ratio of the hydrodynamic diameter of the microspheres.     

催化重整装置的扩能改造

介绍湛江东兴炼油厂的重整装置由200kt／a扩能至300kt／a中有关催化重整反应动力学模拟计算软件的应用、反应工艺技术的改造、装置标定的情况。结合装置实际情况，采用两段装填、两段混氢技术提升了装置的技术水平。标定结果表明，改造后的装置达到了预期目的。     

互联网市场:理性的高速发展——直击“2007中国互联网市场年会”

<正>2006岁末,美国《时代》周刊年度风云人物的揭晓让人意外之余又都颇感认同——全球逾10亿“互联网使用者”共同获此殊荣。的确,历经十几年的发展,“互联网”已密切融入人们的生活。与此同时,互联网市场也发展成为今天涵盖基础接人服务、电子商务、网络游戏、即时通讯、网络搜索等诸多领域的庞大产业。那么目前我国互联网产业整体发展状况以及未来的发展趋势究竟如何呢?透过1月19日于北京成功举办的“2007中国互联网市场年会”,我们可以对此有一个比较深入的了解。