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111.
生产电子工业用高纯氮的制氮装置 ,其要点和难点是一氧化碳和氢的清除。采用一氧化碳转换炉和特殊的冷箱内流程组织 ,可以生产纯度为 99 9999%以上的高纯氮。对制取电子工业用高纯氮制氮装置与常规制氮装置加氮终端净化器两种流程进行了比较。 相似文献
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A Ml (NiCoMnA1)5 hydrogen storage alloys was prepared by double-roller rapid quenching.Its microstructure, electrochemically and kinetic characteristic were studied.A uniform crystal phase with CaCu5 structure could be detected by XRD analyses, whose average grain size is 30 ~ 50 nm and the ratio of c/a of nano-crystal hydrogen storage alloy is larger.The hydrogen absorption/desertion p - C isotherms of alloy show that its fiat-performance is perfect and the magnetic stagnant effect is very little.An simulate cell is used for electrochemical measurement.Electrode is 10C, the capacity decreasing rate via the 450 cycles at 7C is less than 20%. 相似文献
116.
Wei-Cheng Tian Pang S.W. Chia-Jung Lu Zellers E.T. 《Journal of microelectromechanical systems》2003,12(3):264-272
The design, fabrication, and testing of a preconcentrator-focuser (PCF), consisting of a thick micromachined Si heater packed with a small quantity of a granular adsorbent material are described. The PCF is developed to capture and concentrate vapors for subsequent focused thermal desorption and analysis in a micro gas chromatograph. The microheater contains an array of high-aspect-ratio, etched-Si heating elements, 520 /spl mu/m (h)/spl times/50 /spl mu/m (w)/spl times/3000 /spl mu/m (l), bounded by an annulus of Si and thermally isolated from the remaining substrate by an air gap. This structure is sandwiched between Pyrex glass plates with inlet/outlet ports that accept capillary tubes for sample flow and is sealed by anodic bonding (bottom) and rapidly annealed glass/metal/Si solder bonding (top). The large microheater surface area allows for high adsorption capacity and efficient, uniform thermal desorption of vapors captured on the adsorbent within the structure. The adsorbent consists of roughly spherical granules, /spl sim/200 /spl mu/m in diameter, of a high-surface-area, graphitized carbon. Key design considerations, fabrication technologies, and results of performance tests are presented with an emphasis on the thermal desorption characteristics of several representative volatile organic compounds as a function of volumetric flow rates and heating rates. Preconcentration factors as high as 5600 and desorbed peak widths as narrow as 0.8 s are achieved from 0.25-L samples of benzene at modest heating rates. The effects of operating variables on sensitivity, chromatographic resolution, and detection limits are assessed. Testing of this PCF with a micromachined separation column and integrated sensor array is discussed briefly. 相似文献
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Many research projects require accurate delineation of different secondary succession (SS) stages over large regions/subregions of the Amazon basin. However, the complexity of vegetation stand structure, abundant vegetation species, and the smooth transition between different SS stages make vegetation classification difficult when using traditional approaches such as the maximum likelihood classifier (MLC). Most of the time, classification distinguishes only between forest/non-forest. It has been difficult to accurately distinguish stages of SS. In this paper, a linear mixture model (LMM) approach is applied to classify successional and mature forests using Thematic Mapper (TM) imagery in the Rondônia region of the Brazilian Amazon. Three endmembers (i.e., shade, soil, and green vegetation or GV) were identified based on the image itself and a constrained least-squares solution was used to unmix the image. This study indicates that the LMM approach is a promising method for distinguishing successional and mature forests in the Amazon basin using TM data. It improved vegetation classification accuracy over that of the MLC. Initial, intermediate, and advanced successional and mature forests were classified with overall accuracy of 78.2% using a threshold method on the ratio of shade to GV fractions, a 7.4% increase over the MLC. The GV and shade fractions are sensitive to the change of vegetation stand structures and better capture biophysical structure information. 相似文献
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OBJECTIVE: To study the correlation of development and survival with amplification of c-erbB2 oncogene in endometrial carcinoma. METHODS: The amplification and expression of c-erbB2 oncogene were determined from formalin-fixed, paraffin-embedded tissues of 25 normal, 31 hyperplastic, and 72 malignant samples of the endometrium in 128 patients, using differential polymerase chain reaction (DPCR) and an immunohistochemical technique. RESULTS: Amplified c-erbB2 (2 to 12 copies) were found in two of 25 (8.0%) normal, 15 of 31 (48.4%) hyperplastic, and 45 of 72 (62.5%) malignant samples. When the results of DPCR were compared with those of the immunohistochemical method, the negative findings concide well with one another, i.e., nonamplification was associated with the absence of immunoreactivity. It was noted that the amplified c-erbB2 was found more significantly in complex and a typical hyperplasias than in simple hyperplasias. The high-level c-erbB2 amplification (at least five copies) was significantly correlated with the histological grade of endometrial carcinoma and vascular or lymphatic invasion. No correlation was seen between c-erbB2 amplification and overall survival in the present group of patients. CONCLUSIONS: The amplified c-erbB2 may play a potential role in the early development of some endometrial carcinomas. The high-level c-erbB2 amplification may identify a subset of aggressive endometrial carcinoma that involves vascular or lymphatic invasiveness and poor cell differentiation playing the role of a marker for clinical prognosis. 相似文献