Computer-controlled ion-selective electrode switch

The construction of a microcomputer-controlled electrode switch for use in potentiometric determinations is described. This can be coupled to most of the analytical equipment usually found in laboratories, to enable a setting up of automatic systems capable of performing sequential determinations with several ion-selective electrodes. The assessment of its analytical usage and behaviour are discussed.     

压缩弯曲小半径中频弯管工艺的研究

在分析了感应加热小半径弯管形变机理的基础上，提出了压缩弯曲的成型工艺，研制出了小半径中频弯管设备，并进行了大量的工艺实验和实验研究，取得了满意的结果。     

轴对称空间问题的塑性解法

本文从理想材料轴对称弹塑性问题的所有基本方程出发,研究了全塑性时轴对称空间问题的塑性应变分布规律和应力场,并推导了控制应力分布的定解方程,给出了全塑性轴对称问题的通用解法。     

2005电梯贸易顺差显现国际市场前景光明

加入WTO以后，我国的电梯行业发展势如破竹。国内市场国际化开辟了中国电梯行业全面发展的新纪元国际市场国内化彻底打破了国际市场的贸易壁垒，中国电梯走出国门，寻找更大的发展空间，前景一片光明。     

封闭插接母线施工工艺

从工艺原理、流程、操作要点、质量要求等不同侧面介绍了封闭插接母线的施工方法，提出了应注意的安全事项，通过效益分析表明，此法具有工期短、节省人力、工序先进、效益显著等优点。     

Structure evolution of conductive polymer composites revealed by solvent vapor induced time-dependent percolation

The authors of this paper synthesized a series of amphiphilic triblock copolymers of polystyrene-b-poly(ethylene glycol)-b-polystyrene (PS-PEG-PS) having different PEG/PS ratios with nearly identical molecular weights of the entire copolymers. The interfacial interactions in the composites consisting of carbon black and the copolymers can thus be tailored. When these conducting composites are exposed to certain solvent vapors, their electrical resistances greatly increase, showing the gas sensitivity. The present work indicated that this switching behavior is controlled by the structural relaxation of the composites because matrix swelling acts as the main mechanism. The response time has been correlated with absolute temperature by Arrhenius equation, and the estimated activation energy reflects mobility of the fillers involved in the solvent induced expansion of the surrounding polymer. Therefore, by using the gas sensibility of the conductive composites, the structure evolution of the composite materials in solid state and the effect of filler/matrix interfacial interaction on the relaxation property of the matrix polymer has been inspected. It was found that lower activation energy represents stronger interfacial interaction in case good solvent of the matrix was used for the test.     

拉普拉斯变换的图形分析

以单边指数函数为例，分析了拉普拉斯变换象函数F(s)在其收敛域内随σ和ω的变化规律，通过|F(s)|曲面图来观察这些规律，并解释了图中某些特定点及剖面的含义，以形象化的方式加深对拉普拉斯变换的认识。借助MATLAB的绘图功能绘制出F(s)的曲面图、剖面图及信号的频谱图，从中可以观察到频域与复频域的关系以及系统函数的零极点分布等。     

互联网业务流量监测技术的应用和设计

对互联网业务流量监测技术的应用及现状进行了分析，并针对NetFlow技术，对互联网业务流量监测系统建设方案设计中需要考虑的几个重要问题进行了讨论。     

Simultaneous HPLC quantification of total cholesterol,tocopherols and β-carotene in Barrosã-PDO veal

A simple, rapid and sensitive procedure for the simultaneous determination of total cholesterol, tocopherols and β-carotene in meat is described. The method involves a direct saponification of the meat, a single n-hexane extraction and the analysis of the extracted compounds by normal-phase HPLC, using fluorescence (tocopherols) and UV–Vis photodiode array (cholesterol and β-carotene) detections in tandem. Rates of recovery of spiked meat samples were 93% for cholesterol, 83–86% for (α-, β- and -γ) tocopherols and 89% for β-carotene. Repeatabilities were high (CV < 6%) for all determined compounds, except for δ-tocopherol. This tocopherol, which is not usually present in meat, showed a much lower recovery percentage (73%) and repeatability (12.8%). This methodology was applied for the quantification of total cholesterol, tocopherols and β-carotene in three muscles (longissimus thoracis, longissimus lumborum and semitendinosus) of the Portuguese traditional Barrosã-PDO veal, obtained from autochthonous calves fed extensively during summer (with the least abundant green pastures) and slaughtered in early autumn (October). Barrosã-PDO veal showed median contents of total cholesterol (0.50–0.56 mg/g) and, depending on the analysed muscle, moderate to high contents of α-tocopherol (3.3–3.9 μg/g) and β-carotene (0.07–0.09 μg/g), suggesting an high sensorial and hygienic quality.     

真空蒸发沉积VOPc薄膜及磁场对薄膜结构与性能的影响

用真空蒸发制备了酞菁氧钒 (VOPc)薄膜 ,并在磁场中进行了热处理。用X光电子能谱、X射线衍射、紫外 可见吸收光谱、原子力显微镜等手段对制备的薄膜进行了表征。结果表明沉积的酞菁氧钒薄膜为α 型 ,成分接近酞菁氧钒的分子式。制备的薄膜在磁场中进行了热处理 ,发现磁场使酞菁氧钒薄膜性质发生改变 :UV VIS吸收谱Q带发生红移 ;XRD谱图衍射峰强度明显增强 ,峰位略有变化 ;原子力显微镜 (AFM)分析发现晶粒大小无明显变化。以上结果说明磁场的存在使得VOPc分子在热处理过程中发生了定向的排列