电位滴定法研究~(99)Tc-HMDP和~(99)Tc-HEDP中Tc的氧化态

~(99)Tc-HMDP和~(99)Tc-HEDP溶液是在相应的螫合剂存在下,用过量SnCl_2还原~(99)TcO_4-制得。用标准I_2液对SnCl_2进行了剩余量电位滴定,确定了在pH～3的介质中,~(99)Tc-HMDP和~(99)Tc-HE-DP中~(99)Tc的氧化态均为+4。全部实验在N_2气流中进行。~(99)Tc-HMDP和~(99)Tc-HEDP的紫外光谱表明:在用I_2滴定的过程中,~(99)Tc只处于一种氧化态+4;将它们放置在空气中,一小时后仍较稳定。     

Speech Enhancement via Residual Dense Generative Adversarial Network

Generative adversarial networks (GANs) are paid more attention to dealing with the end-to-end speech enhancement in recent years. Various GAN-based enhancement methods are presented to improve the quality of reconstructed speech. However, the performance of these GAN-based methods is worse than those of masking-based methods. To tackle this problem, we propose speech enhancement method with a residual dense generative adversarial network (RDGAN) contributing to map the log-power spectrum (LPS) of degraded speech to the clean one. In detail, a residual dense block (RDB) architecture is designed to better estimate the LPS of clean speech, which can extract rich local features of LPS through densely connected convolution layers. Meanwhile, sequential RDB connections are incorporated on various scales of LPS. It significantly increases the feature learning flexibility and robustness in the time-frequency domain. Simulations show that the proposed method achieves attractive speech enhancement performance in various acoustic environments. Specifically, in the untrained acoustic test with limited priors, e.g., unmatched signal-to-noise ratio (SNR) and unmatched noise category, RDGAN can still outperform the existing GAN-based methods and masking-based method in the measures of PESQ and other evaluation indexes. It indicates that our method is more generalized in untrained conditions.     

云计算安全：概念、现状与关键技术

随着云计算的广泛应用,云计算安全问题逐渐凸显出来。文章首先阐述了云计算安全相关概念,并对云计算的安全问题和云计算安全特征进行分析,然后对云计算安全的现状和典型的云计算安全体系架构进行了介绍,并对云计算安全的关键技术进行分析,最后给出了结论。     

高灰度级TFT-LCD显示系统的实现

提出了一种以FPGA为核心控制器的高灰度级TFT-LCD显示系统的设计方案。该系统采用幅值-帧速率控制调制-空间混合灰度调制方法,首先将10 bit的R、G、B信号分割成高8 bit数据和低2 bit数据,低2 bit数据经过空间处理后平均分到4个相邻的8 bit数据上,然后把这8 bit数据继续分割成高6 bit数据和低2 bit数据,其中高6 bit数据用于幅值调制,低2 bit数据用于帧速率控制调制,从而实现1 024个灰度等级显示。试验结果表明,该系统具有良好的显示效果和较高的显示灰度等级。     

一种并行冗余遥控锁定投放控制系统

以海上无人演练战场等复杂环境下实现对大负载作战单元的遥控布放为需求,提出了一种包含短波、超短波和卫星无线信道,以及本地端手动控制的多并行冗余锁定投放控制系统.设计了一种新型锁定投放装置,使用恒流源驱动的直流减速电机推动锁闩执行布放任务,具有功耗小、负载大等优点;在锁定投放装置的控制器中并行集成了以上几种投放控制接口,能以互为备份的方式执行任意种或多种投放控制指令,提高了系统的鲁棒性.该锁定投放控制系统已多次执行海上任务,工作稳定可靠.     

Low‐voltage and high‐transmittance blue‐phase liquid‐crystal device with slanted electrodes

Abstract— A low‐voltage (～10 V_rms) and high‐transmittance (～90%) polymer‐stabilized blue‐phase liquid‐crystal (BPLC) device with a slanted‐electrodes structure is proposed. Unlike the vertical‐field‐switching (VFS) mode in which oblique incident light and a vertical field are employed, the proposed device utilizes normal incident light and an oblique field. The slanted electrodes generate a strong and uniform oblique electric field, which contributes in obtaining low voltage and high transmittance. Moreover, no couple films or prism sheets are needed, which helps to enhance the optical efficiency and simplify of the device structure. This device has great potential application for emerging BPLC displays and photonic devices.     

基于柯西面方法的EAST真空场仿真

研究真空场等离子击穿优化问题,在托卡马克等离子体放电中,合适的真空场是保证等离子体击穿的重要条件.合适的真空场是通过调节极向场线圈实现的.对于传统的一体化设计的EAST极向场系统,没有专门的补偿线圈来保证放电初期的真空场分布.为了指导极向场线圈电流的调节以获得合适的真空场分布来保证等离子体稳定击穿性能,提出一种新的基于等离子体真空区域的边界积分方程的方法来计算等离子体区域的真空场.方法在EAST上进行仿真,结果表明,在提供有足够数量的磁测量信号的情况下,改进方法能准确的对真空区域的磁场、磁通进行计算.通过将计算得出的磁场、磁通分布与实验其它一些诊断信号进行对比,表明磁场信号、磁通信号很好的吻合了实验结果,为EAST等离子放电系统优化设计提供了重要的参考.     

网格研究及其开发环境*

探讨了网格研究的基础理论、核心问题、具体研究内容和难点;仿真是研究网格资源管理和调度问题的重要方法,分析和评价了目前主要仿真工具的特点及应用;GT3已经成为网格项目开发的主流工具,给出了建立GT3 Core网格服务开发平台的方法;介绍了基于CGSP(China Grid Support Platform)的网格开发环境.以期有助于网格的创新研究和应用开发.     

Effect of supports on the redox performance of pyrite cinder in chemical looping combustion

Chemical looping combustion (CLC) is a clean and efficient flame-free combustion technology,which combust the fuels by lattice oxygen from a solid oxygen carrier with inherent CO2 capture.The develop-ment of oxygen carriers with low cost and high redox performance is crucial to the whole efficiency of CLC process.As the solid by-product from the sulfuric acid production,pyrite cinder presented excellent redox performance as an oxygen carrier in CLC process.The main components in pyrite cinder are Fe2O3,CaSO4,Al2O3 and SiO2 in which Fe2O3 is the active component to provide lattice oxygen.In order to sys-tematic investigate the functions of supports (CaSO4,Al2O3 and SiO2) in pyrite cinder,three oxygen car-riers (Fe2O3-CaSO4,Fe2O3-Al2O3 and Fe2O3-SiO2) were prepared and evaluated in this study.The results showed that Fe2O3-CaSO4 displayed high redox activity and cycling stability in the multiple redox cycles.However,both Fe2O3-Al2O3 and Fe2O3-SiO2 experienced serious deactivation during redox reactions.It indicated that the inert Fe-Si solid solution (Fe2SiO4) was formed in the spent Fe2O3-SiO2 sample,which decreased the oxygen carrying capacity of this sample.The XPS results showed that the oxygen species on the surface of Fe2O3-CaSO4 could be fully recovered after the 20 redox cycles.It can be concluded that CaSO4 is the key to the high redox activity and cycling stability of pyrite cinder.     

微粉对矾土基超低水泥浇注料性能的影响

以高铝矾土熟料为主原料 ,加入 2 %的铝酸钙水泥及总量为 6 %的Al2 O3 微粉和SiO2 微粉 ,配制了矾土基超低水泥浇注料 ,研究了微粉对浇注料的烧结性能、力学性能及热震稳定性的影响。结果表明 :(1 )SiO2 微粉对浇注料的促烧结作用优于Al2 O3 微粉。这是因为与Al2 O3 微粉相比 ,由气相沉积生成的SiO2微粉的粒度小 ,比表面积大 ,活性较高。 (2 )随着SiO2微粉加入量的增加 ,在 1 1 0 0℃和 1 4 0 0℃处理后的常温强度以及在 1 30 0℃和 1 4 0 0℃下的高温抗折强度和抗热震性明显提高。这是由于引入的SiO2 微粉在高温下与Al2 O3 反应生成的针状莫来石穿插进入刚玉骨架 ,起着明显的强化和韧化作用