2-硝基-4''''-氨基二苯胺-4-磺酸的工艺改进

将3-硝基-4-氯苯磺酸与对苯二胺进行缩合反应制得2-硝基-4’-氨基二苯胺-4-磺酸。传统的合成工艺：缩合反应的收率只有83％，主含量86.4％，必须精制后才能使用。本实验对缩合工艺的反应条件如温度，缚酸剂，抑制剂以及加料方式等进行了较为详细的探讨，通过正交实验，选择了最佳缩合反应条件，m（硝化物）：m（对苯二胺）=1.10：1，分次加料，分段保温，获得纯度94.7％的产品。收率提高了8％-10％，减少了废物的排放量，并省去精制步骤。     

民法法典化视野下的社员权

社员权问题学界少有论及,在目前民法法典化这个大背景之下研究社员权有着其独特的价值。社员权产生于日耳曼法,正式确立于近代。所谓社员权,系指社员基于其社员身份而对社团和其他社员所享有的权利。作为基本私权利的一个种类,社员权在未来民法典中应当占有一席之地。未来民法典中的社员权法应当包括社员权法通则、建筑物区分所有人的社员权、集体经济组织成员的社员权以及合作社成员的社员权共四部分。     

Analysis of junction temperatures in high-power GaN-based LEDs

We presented the analysis of the incomplete conduction in bonding medium in high power GaN-based light-emitting diode (LED) packages. A numerical study was carried out with parametric model to understand the junction temperature variation due to bonding medium defects. Transient thermal measurement was performed to evaluate LED’s junction temperature. Thermal resistance from chip to lead frame was 20 K/W in our sample LED. It was suggested that only 60% of the surface area of the bonding medium was involved...     

Dynamic equivalent method of interconnected power systems with consideration of motor loads

The existing equivalent methods usually only deal with static load models and neglect the dynamic characteristics of loads such as induction motors.This paper presents a dynamic equivalent method which considers motor dynamics.At first,the clustering criterion of motor loads is given.The motors with similar dynamic characteristics are classified into one group.Then,reduction of motors in the same group is carried out.Finally,parameters of the equivalent motor are calculated and the equivalent system is thus...     

多维超几何分布的最可能成功数

超几何分布是一种重要的离散型概率分布,本文利用反证法以及比较法求出了三维超几何分布的最可能成功次数,并在此基础上,求出了多维超几何分布的最可能成功次数.     

Relation between structural evolution of the Longmenshan orogenic zone and sedimentation of its foreland basin

In order to determine the area for oil and gas exploration in China's north Sichuan basin, we have divided the time during which the Longmenshan foreland basin was formed into five periods, based on the sedimentary response relationship of the fore-land basin to structural evolution: 1) a late Triassic Noric period; 2) an early-Middle Jurassic period; 3) a late Jurassic to early Cre-taceous period; 4) a late Cretaceous to Paleogene-Neogene period and 5) the Quaternary period. As well, we analyzed the sedimen-tary environment and lithologic features of every basin-forming period. The results show that there are several favorable source-reservoir-cap assemblages in our study area, making it a major region for future oil and gas exploration in China's northern Sichuan basin.     

丰田召回启示录

全球范围丰田八种类型860万辆汽车被召回,引发世界媒体高度关注。丰田代表了21世纪管理趋势,不曾想丰田神话,最后竟然是由丰田自己打破。丰田“召回门”的警示将对所有企业产生深远影响。争抢世界第一,代价有时很昂贵;过分关注成本,产品质量难保证;及时化解危机,态度比技术更重要;美国不想第二,竞争变得很复杂。     

满族服饰文化中的灵物崇拜

文章通过对满族萨满文化的宗教信仰和灵物崇拜的研究,从满族人民的精神文化领域揭示满族服饰的意义,以便更好的传承满族服饰,让满族服饰文化源远流长。