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Journal of Porous Materials - Nitrogen and oxygen co-doped hierarchical porous carbons (NOPCs) is prepared by the pyrolysis of polyethylene glycol-200 (PEG) and triazine carbon forming agent (CFA)... 相似文献
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Qiu Jun Wang Yueting Wu Peng Jiang Shan Cui Kaibo Chen Guowei Liu Dongliang Cui Guangwen 《Journal of Porous Materials》2021,28(6):1675-1687
Journal of Porous Materials - The dynamics and thermodynamics of adsorption of hexadecyl ammonium with different numbers of carbon chains in montmorillonite (Mt) with different layer charge density... 相似文献
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The “hardness” components in sea water can be considerably reduced by means of a new economical fixed bed technique called “Reciprocating Flow Ion Exchange”, when used in conjunction with a closed cycle exchanger-evaporator system. Removal of 87.9% of the calcium and 54.5% of the magnesium in sea water has been obtained with an overall flow rate of 5.0 U. S. g. p. m./sq. ft. Results from bench scale and a 5,000 g. p. d. pilot plant were identical. The virtually continuous cyclic steady-state process requires a small amount of exchanger (0.5 to 2% of the usual ion exchange methods, such as conventional fixed beds or fluidized beds). The effects of variation in operating parameters are discussed. 相似文献
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Isothermal crystallization kinetics were investigated by differential scanning calorimetry (DSC) for poly(p-phenylene sulfide) (PPS) doped with amorphous carbon or crystalline graphite particles. Both types of carbon forms have been found to affect the crystallization behavior of PPS to different extents. The crystalline graphite particles have a more pronounced effect on the overall rate as well as mechanisms of PPS crystallization than do the amorphous carbon particles. Relative contributions and competition from crystallizations of two different crystals in the later-stage crystallization of PPS have been found to cause the phenomenon of deviation from linearity in the Avrami plots. A sequential crystallization model has been shown to describe well the crystallization behavior of the PPS doped with the particles. © 1995 John Wiley & Sons, Inc. 相似文献
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Preparation of Titanium Nitride/Alumina Laminate Composites 总被引:2,自引:0,他引:2
Jing-Xian Zhang Zheng-Ren Huang Dong-Liang Jiang Shouhong H. Tan Zhijian Shen Mats Nygren 《Journal of the American Ceramic Society》2002,85(5):1133-1138
A preparation route for TiN/Al2 O3 laminate composites has been described. A water-based process using Al2 O3 and TiN slurries with solids contents of 40 and 35 vol%, respectively, was used to make TiN and Al2 O3 tapes. The removal of the binder was monitored by weight-loss measurements in a thermogravimetry unit. Bodies composed of Al2 O3 and TiN tapes were densified at temperatures of 1400° and 1500°C using the Spark Plasma Sintering® (SPS) technique. Densities of >98% of the theoretical densities were approached. Crack-free and almost fully densified TiN/Al2 O3 compacts were prepared by heating the burned-out green bodies to the final sintering temperature (1500°C) at a rate of 100°C/min, and with a holding time of 5–10 min, under a pressure of 75 MPa. The microstructures of the obtained compacts were studied using scanning electron microscopy. Grain sizes in the sintered Al2 O3 and TiN compacts were similar to those of the precursor powders. Hardness and indentation fracture toughness were measured at room temperature, and the monolithic compacts as well as the laminate composites exhibited anisotropic mechanical behavior; i.e., the cracks propagated much more easily in a direction parallel to the laminas than perpendicular to them. 相似文献
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A number of methods of surface preparation of tantalum for encapsulation in silicone rubber and for structural adhesive bonding were explored. The only ones which could be generally useful were boiling for 24 hours in distilled water (28% improvement) or boiling for 4 hours in 20% sodium hydroxide solution followed by boiling for 2 hours in dilute hydrochloric acid (34% improvement). An alternative, which could sometimes be used, was heating in air for at least 2 hours at 100°C. 相似文献
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在真空粉末绝热低温贮罐的制造过程中、通过吸附器分子筛的活化、夹层真空系统的处理和充装珠光砂等工艺方法的改进,可较大地缩短产品的制造周期并提高产品的质量。 相似文献