基于local-area的Internet路由级拓扑抽象算法

通过分析Internet的本地聚集特性,给出了local-area和connect-area的定义,并基于此,为提高并行网络模拟性能,提出一种新型拓扑抽象算法——基于local -area的拓扑抽象(TABLA)算法.TABLA算法在给定的聚合粒度下,迭代搜索网络内的local-area,对拓扑进行抽象.模拟结果表明在...     

2011年闽东茶区春季茶青中稀土残留的检测与分析

采用电感耦合等离子体质谱(ICP-MS)技术,对60份茶青中残留稀土元素含量进行了测定,并对测定结果进行了分析。参照国家标准GB2762—2005《食品中污染物限量》(其中茶叶稀土的限量指标为≤2.0mg/kg,以La、Ce、Pr、Nd、Sm的氧化物总量计)对茶青中的稀土残留量进行评价分析,所测的闽东茶区春季茶青样品稀土合格率高达100%。     

基于Morlet小波分频的保边滤波去噪方法

进行保边滤波需要已知反射倾角和边界信息,通常这些信息由全频率地震资料估算得到,但噪声的存在往往会降低估算的准确性.地震资料的各个频率成分具有不同的信噪比,Morlet小波具有良好的局部性能,所以用Morlet小波可以将地震数据按照倍频程分为几个分频体.对于信噪比不是太低(一般指大于2.5 )的地震资料,会有2-3个分频体具有较高的信噪比.扫描上述分频体,确定它们的倾角以及边界信息,然后利用倾角及边界信息对上述分频体以及与其频率接近的分频体进行平滑,并根据是否存在边界采取不同的滤波手段,保证滤波算法的稳定性,最后将平滑后的各频段地震记录合成,得到去噪后的地震记录.理论模型和实际资料处理表明,对于信噪比大于2.5的地震资料,该方法能有效去除噪声.     

Controlled synthesis of monodisperse silver nanocubes via a solvothermal method

Silver nanostructures have been synthesized via a simple solvothermal method by adding sodium sulfide (Na₂S) into the solution. The morphologies of products are controlled by the concentration of Ag₂S formed in the initial stage. A low-concentration Ag₂S (12.5 ~ 50 μM) acts as the catalysis, leading to the formation of silver nanocubes with controllable sizes. However, a high-concentration Ag₂S (100 μM) mainly acts as the controlling agent. It facilitates the synthesis of silver nanowires. Reaction conditions, the reaction temperature and the molar ratio of the repeating unit of PVP to AgNO₃ (R), have also been investigated. A possible mechanism is proposed to interpret the synthesis of silver nanocubes and nanowires. Finally, our results indicate that this strategy provides a simple route to prepare silver nanocubes with adjustable sizes.     

Large-scale synthesis of silver nanowires via a solvothermal method

Silver nanostructures have been synthesized through a simple solvothermal method by reducing silver nitrate (AgNO₃) with ethylene glycol (EG) and using poly(vinylpyrrolidone) (PVP) as an adsorption agent. Different concentrations of ferric chloride (FeCl₃) are added into the solution. It is found that AgCl colloids formed in the initial stage greatly influence the final morphologies of the products. When a low-concentration FeCl₃ solution is used, there is a mixture of silver nanoparticles and nanowires. However, when a high-concentration FeCl₃ solution (100 μM) is used, large amounts of AgCl colloids appear, resulting in decreasing free Ag⁺ during initial formation of silver seeds and slowly releasing of Ag⁺ to the solution in the subsequent reaction. This leads to the formation of silver nanowires. Furthermore, an increase in the concentration of FeCl₃ from 100 to 300 μM results in the synthesis of silver nanowires with larger sizes. In addition, Fe(III) is reduced to Fe(II) form which in turn reacts with and removes adsorbed atomic oxygen from the surface of silver seeds. In this case, uniform silver nanowires can be obtained.     

食品添加剂二氧化碳中氧标准物质重量制备方法及重量制备不确定度的研究

研究了食品添加剂二氧化碳中氧标准物质重量制备的实验方法及不确定度评价研究的内容.采用中国计量科学研究院设计加工的气体充填装置制备了二氧化碳中氧标准物质,该装置低压系统真空度达到7×10-3Pa;气体称量装置采用美国Mettler SB16001电子天平(16 kg、0.1 g)和上海第二天平仪器厂TG320B高精密天平...     

Ni/YSZ and Ni–CeO2/YSZ anodes prepared by impregnation for solid oxide fuel cells

In this paper, Ni/YSZ and Ni–CeO₂/YSZ anodes for a solid oxide fuel cell (SOFC) were prepared by tape casting and vacuum impregnation. By this method, the Ni content in the anode could be reduced compared to the traditional tape casting method. It was found that adding CeO₂ into the Ni/YSZ anode by a Ni(NO₃)₂ and Ce(NO₃)₃ mixed impregnation could further enhance cell performance. This was investigated in H₂ at 1073 K. XRD patterns indicated that CeO₂ and Ni were separate phases, and the CeO₂ addition could enhance the Ni dispersion on the YSZ framework surface which was observed by SEM images. It was shown that adding CeO₂ into the Ni anodes could decrease the cell polarization resistance. The maximum power density for cells with 25 wt.% Ni, 5 wt.% CeO₂–25 wt.% Ni/YSZ, or 10 wt.% CeO₂–25 wt.% Ni/YSZ anode was 230 mW cm⁻², 420 mW cm⁻² and 530 mW cm⁻², respectively, in H₂ at 1073 K. The OCV for these cells was 1.05–1.09 V, indicating that a dense electrolyte film was obtained by co-firing porous YSZ layer and dense YSZ layer.     

Combustion and emission characteristics of a two-stroke diesel engine operating on alcohol

Though, as a renewable energy resource, alcohol fuel has many advantages in China, it is difficult for diesel engines to operate on alcohol due to its low cetane number and high latent heat of vaporization. This paper proposes an approach to its ignition problem by combining internal exhaust gas recirculation (EGR) with injection of small diesel fuel. Based on this approach, a two-stroke single-cylinder diesel engine was developed. Preliminary studies demonstrated that the engine can run on alcohol with almost zero level of smoke and low exhaust gas temperature, and that the engine operating on alcohol has lower nitrogen oxide (NO_x) emissions and 2–3% higher effective thermal efficiency than that operating on diesel fuel in moderate and high load zones.     

生物质半焦气化的反应动力学

利用热重分析仪研究了CO2气氛下的生物质半焦的反应性。研究发现，所研究的4种生物质半焦都表现出了相同的反应性趋势。其反应性随着转化率的增加而增加。这可能是由于生物质焦样中的碱金属含量，尤其是钾的含量较高的原因。对比生物质气化反应动力学参数研究表明，4种焦样的气化行为可以用收缩核模型来描述，并求出了4种生物质焦样的反应动力学参数。在不同的CO2分压下进行了花生壳焦样的反应性实验研究，发现焦样的反应性正比于反应气体浓度，求出了花生壳焦样的反应动力学方程式。     

轮转调度下实时流量到达时间间隔抖动的容忍分析

研究了AFDX交换机在采用轮转调度策略,并保证消息传输实时性的前提下,对消息到达时间间隔抖动的容忍能力.采用实时通信中的周期性任务模型,依据实时性保证原则,推导出在已知的轮转调度策略下,交换机允许消息到达最小时间间隔,及交换机对消息抖动的容忍度的数学表达式.最后给出在给定的实时流量下,到达时间间隔抖动容忍度的计算实例,...