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991.
Rachmat Adhi Wibowo Stefan A. Moeckel Hyesun Yoo Christina Hetzner Astrid Hoelzing Peter Wellmann Rainer Hock 《Materials Chemistry and Physics》2013
A combined in-situ investigation using X-ray diffraction and differential scanning calorimetry during annealing was carried out to investigate the formation of intermetallic compounds in the stacked elemental layers and to reveal its influences on the crystallization of kesterite Cu2ZnSnSe4. The Mo/Cu/Zn, Mo/Cu/Sn/Zn, Mo/Cu/Zn/Se and Mo/Cu/Sn/Zn/Se stacked films were prepared with a composition resembling a typical kesterite Cu-poor and Zn-rich metallic composition. In-situ experiments during annealing of pure metallic stacked films reveal a dynamic intermetallic compounds formation of Cu5Zn8 → CuZn → Cu2Zn → Cu3Zn and Cu6Sn5 → Cu41Sn11. The CuZn and Cu5Zn8 layer formed at the interface of metals/Se may prevent the stacked metallic layers from selenization below 320 °C. On the other side, the dynamic formation of Cu–Zn phases in the stacked films is found to be an origin of a ZnSe gradual formation starting from 320 °C. Phase analysis suggests that the ternary Cu2SnSe3 phase forms almost immediately after the formation of Cu2Se and SnSe. The formation of Cu2SnSe3 is indicated by the consumption of SnSe by the Cu2Se which occurs at 530–540 °C. Crystallization of kesterite takes place above 540 °C. On a phenomenological basis of present results, consequences for the thin film kesterite fabrication for solar cell application are discussed. 相似文献
992.
993.
A parallelized resolved method for the simulation of the dynamics of immersed bodies within fluids is presented. The algorithm uses a FDM (fictitious domain method) and combines the Lagrangian DEM (discrete element method) for tracking the bodies with a CFD (computational fluid dynamics) method for calculating the dynamics of the fluid phase. First the CFD-calculation is carried out, disregarding the solid bodies. Afterwards, the velocity information from the bodies is included and the force, the fluid imposes onto the bodies, is computed. The last step consists of a correction-operation which ensures the fulfillment of the conservation equation. Dynamic local mesh refinement is used for minimizing the number of fluid cells. The CFD-DEM coupling is realized within the Open Source framework CFDEMcoupling (www.cfdem.com), where the DEM software LIGGGHTS (www.liggghts.com) is linked against an OpenFOAM~-based CFD solver. While both LIGGGHTS and the CFD solver were already parallelized, only a recent improvement of the algorithm permits the fully parallel computation of resolved problems. This parallelization permits the treatment of large-scale problems. The enclosed validation and application examples show the dynamics of the flow around settling and rotating spheres as well as an investigation of the settling of spheres regarding the Boycott effect. 相似文献
994.
Dietz J Koch J Kaur A Raja C Stein S Grez M Pustowka A Mensch S Ferner J Möller L Bannert N Tampé R Divita G Mély Y Schwalbe H Dietrich U 《ChemMedChem》2008,3(5):749-755
The interaction of the nucleocapsid NCp7 of the human immunodeficiency virus type 1 (HIV-1) Gag polyprotein with the RNA packaging signal Psi ensures specific encapsidation of the dimeric full length viral genome into nascent virus particles. Being an essential step in the HIV-1 replication cycle, specific genome encapsidation represents a promising target for therapeutic intervention. We previously selected peptides binding to HIV-1 Psi-RNA or stem loops (SL) thereof by phage display. Herein, we describe synthesis of peptide variants of the consensus HWWPWW motif on membrane supports to optimize Psi-RNA binding. The optimized peptide, psi-pepB, was characterized in detail with respect to its conformation and binding properties for the SL3 of the Psi packaging signal by NMR and tryptophan fluorescence quenching. Functional analysis revealed that psi-pepB caused a strong reduction of virus release by infected cells as monitored by reduced transduction efficiencies, capsid p24 antigen levels, and electron microscopy. Thus, this peptide shows antiviral activity and could serve as a lead compound to develop new drugs targeting HIV-1. 相似文献
995.
Andreas Stelzer Stefan Scheiblhofer Stefan Schuster Rüdiger Teichmann 《Measurement》2008,41(5):579-588
A wireless sensor marking system based on surface acoustic wave (SAW) identification tags is presented. The proposed solution is compatible with existing measurement systems and can be applied directly in the sensor or by means of a unique sensor identification cable (SIC). The SAW tag operates completely passive, and withstands temperatures up to 400 °C as well as shocks up to 35 000 m/s2. It contains a unique serial identification number, which is encoded on the high-temperature stable SAW device by means of metallic reflector gratings. The interrogation unit uses the sensor cable for transmission but is not directly connected to it, thus the identification system can be even used with high impedance measurement equipment, e.g. charge amplifiers. Interrogation is done in frequency-domain based on well-known radar principles and is realized in a low-cost add-on circuit to the existing sensor evaluation circuitry. Furthermore, by simply enhancing the evaluation software, a temperature measurement of the SAW tag itself, and thus often of the sensor or the sensor environment can be done without additional hardware requirements. 相似文献
996.
A new discretization for simultaneous aggregation, breakage, growth and nucleation is presented. The new discretization is an extension of the cell average technique developed by the authors [J. Kumar, M. Peglow, G. Warnecke, S. Heinrich, and L. Mörl. Improved accuracy and convergence of discretized population balance for aggregation: The cell average technique. Chemical Engineering Science 61 (2006) 3327-3342.]. It is shown that the cell average scheme enjoys the major advantage of simplicity for solving combined problems over other existing schemes. This is done by a special coupling of the different processes that treats all processes in a similar fashion as it handles the individual process. It is demonstrated that the new coupling makes the technique more useful by being not only more accurate but also computationally less expensive. At first, the coupling is performed for combined aggregation and breakage problems. Furthermore, a new idea that considers the growth process as aggregation of existing particle with new small nuclei is presented. In that way the resulting discretization of the growth process becomes very simple and consistent with first two moments. Additionally, it becomes easy to combine the growth discretization with other processes. The new discretization of pure growth is a little diffusive but it predicts the first two moments exactly without any computational difficulties like appearance of negative values or instability etc. The numerical scheme proposed in this work is consistent only with the first two moments but it can easily be extended to the consistency with any two or more than two moments. Finally, the discretization of pure and coupled problems is tasted on several analytically solvable problems. 相似文献
997.
Chamakuri Nagaiah Gerald Warnecke Stefan Heinrich Mirko Peglow 《Computers & Chemical Engineering》2008,32(12):2877-2890
The numerical computations of temperature and concentration distributions inside a fluidized bed with spray injection in three-dimensions are presented. A continuum model, based on rigorous mass and energy balance equations developed from Nagaiah et al., is used for the three-dimensional simulations. The three-dimensional model equation for nozzle spray is reformulated in comparison to Heinrich. For solving the non-linear partial differential equations with boundary conditions a finite element method is used for space discretization and an implicit Euler method is used for time discretization.The time-dependent behavior of the air humidity, air temperature, degree of wetting, liquid film temperature and particle temperature is presented using two different sets of experimental data. The presented numerical results are validated with the experimental results. Finally, the parallel numerical results are presented using the domain decomposition methods. 相似文献
998.
Thomas Richter Stefan Denneler Carsten Schuh Ender Suvaci Ralf Moos 《Journal of the American Ceramic Society》2008,91(3):929-933
A promising way to improve the performance of piezoelectric ceramics is grain orientation by templated grain growth. In this work lead-based piezoelectric ceramics Pb(Mg1/3 Nb2/3 )0.68 Ti0.32 O3 (PMN–32PT) and Pb(Mg1/3 Nb2/3 )0.42 (Ti0.638 Zr0.362 )0.58 O3 (PMN–37PT–21PZ) ceramics were textured via templated grain growth process. For texturization (001)-oriented BaTiO3 (BT) platelets (approximately 10 μm × 10 μm × 2 μm) were utilized as templates. The texturized ceramics were accomplished by aligning the templates by tape casting. The template growth into the matrix resulted in textured ceramics with Lotgering factors between 0.94 and 0.99 for both compositions. Consequences of the texture are enhanced dielectric and piezoelectric properties. Unipolar strain-field measurements of textured ceramics showed 0.25% strain s 33 at 3 kV/mm. Large signal d 33 * of up to 878 pm/V were determined directly from strain measurements. Compared with randomly oriented ceramics in texturized samples unipolar strain s 33 and large signal d 33 * was enhanced by a factor of up to 1.8. 相似文献
999.
1000.
Chlor-alkali electrolysis with oxygen depolarized cathodes: history,present status and future prospects 总被引:1,自引:0,他引:1
Imad Moussallem Jakob Jörissen Ulrich Kunz Stefan Pinnow Thomas Turek 《Journal of Applied Electrochemistry》2008,38(9):1177-1194
The historical development, current status and future prospects of chlor-alkali electrolysis with oxygen depolarized cathodes
(ODCs) are summarized. Over the last decades, membrane chlor-alkali technology has been optimized to such an extent that no
substantial reduction of the energy demand can be expected from further process modifications. However, replacement of the
hydrogen evolving cathodes in the classical membrane cells by ODCs allows for reduction of the cell voltage and correspondingly
the energy consumption of up to 30%. This replacement requires the development of appropriate cathode materials and novel
electrolysis cell designs. Due to their superior long-term stability, ODCs based on silver catalysts are very promising for
oxygen reduction in concentrated NaOH solutions. Finite-gap falling film cells appear to be the technically most mature design
among the several ODC electrolysis cells that have been investigated.
相似文献
Thomas TurekEmail: |