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931.
932.
The ultrafast deprotonation of 2‐(2′‐hydroxyphenyl)benzothiazole (HBT) hosted in nanometer‐sized FAU and MFI zeolites is reported. Samples are prepared via in‐situ incorporation of HBT in the precursor colloidal solutions resulting in the formation of nanometer‐sized zeolites under hydrothermal treatment. The diameter of the zeolite particles formed in the crystalline suspensions is determined by dynamic light scattering and high‐resolution transmission microscopy to lie in the range 40–100 nm. It is shown that the HBT loading does not influence the degree of the zeolite crystallinity but does change the size and the morphology of the individual zeolite nanoparticles. Colloidal suspensions containing the crystalline nanoparticles are well suited for optical investigations since they are sufficiently transparent and clear. The photochemical properties of the HBT guest in the zeolite‐host systems are studied with femtosecond transient transmission spectroscopy. Depending on the acid–base properties either the enol or the keto tautomer of HBT is found to be hosted in the internal voids of the zeolites; upon UV excitation, the HBT‐keto tautomer is converted to the enol form in both MFI‐ and FAU‐type hosts. The HBT photoconversion takes place via an ultrafast deprotonation within 1.5 ps as detected by femtosecond transient absorption spectroscopy.  相似文献   
933.
The direct-injection spark-ignition engine has emerged as a focus of research in improving fuel economy and controlling emissions. This engine can operate in multiple modes, including a stratified charge mode with an air-fuel ratio as large as 50:1. Operating in stratified mode results in improved fuel economy and reduced CO/sub 2/ emissions. The stratified charge mode is employed during low speed and load conditions, such as during engine idle. The idle speed control problem is cast as a two-input-two-output control problem and a baseline feedback controller is developed based on an existing topology from the literature. Significant delays, however, inhibit our ability to improve the transient response via feedback alone. An improved scheme employing reference feedforward is proposed and several potential topologies are presented. A reference feedforward algorithm is derived and nonlinear simulation results are shown in which the system transient responses are improved considerably.  相似文献   
934.
[110]-surface strained-SOI CMOS devices   总被引:1,自引:0,他引:1  
We have newly developed [110]-surface strained-silicon-on-insulator (SOI) n- and p-MOSFETs on [110]-surface relaxed-SiGe-on-insulator substrates with the Ge content of 25%, fabricated by applying the Ge condensation technique to SiGe layers grown on [110]-surface SOI wafers. We have demonstrated that the electron and the hole mobility enhancement of [110]-surface strained-SOI devices amounts to 23% and 50%, respectively, against the mobilities of [110]-surface unstrained MOSFETs. As a result, the electron and the hole mobility ratios of [110]-surface strained-SOI MOSFETs to the universal mobility of (100)-surface bulk-MOSFETs increase up to 81% and 203%, respectively. Therefore, the current drive imbalance between n- and p-MOS can be reduced. Moreover, both the electron and the hole mobilities of the [110]-surface strained-SOIs strongly depend on the drain current flow direction, which is qualitatively explained by the anisotropic effective mass characteristics of the carriers on a [110]-surface Si. As a result, the [110]-surface strained-SOI technology with optimization of the current flow directions of n- and p-MOS is promising for realizing higher speed scaled CMOS.  相似文献   
935.
936.
Erosion and corrosion of metallic materials in particle containing aqueous solutions The combined effect and mutual influence, respectively, of erosion and corrosion of metallic materials in particle containing flows was investigated. Materials under investigation are carbon steel of different hardness levels, ferritic chromium steel, austenitic stainless steel and brass. Corrosive medium was deionized water, acid (pH 4.5), alkaline (pH 10) and chloride (3% NaCl) solution. Quartz particles were used as abrasive at various particle concentrations, grain sizes and flow velocities. For comparison, tests were performed with pure water and under conditions of idle corrosion. Mechanical or corrosive influences dominate depending on material and test conditions, in some cases, synergistic effects of both mechanisms cause an increased mass loss.  相似文献   
937.
Given the heightened interest in nutritional aspects of exercise, and an increase in athletic participation by women, it appeared timely to review the nutritional implications of exercise in women. The initial part of this paper contains a compilation of published studies on the nutrient intakes of female athletes. These reveal that most groups of athletes have adequate nutrient intakes, and that their vitamin and mineral intakes appear to be superior to those of nonathletic women. The average energy intake of athletes in studies summarized in this paper was 2069 kcal, and for certain groups of athletes, energy intakes were even lower. How these women manage to train intensely while consuming energy intakes similar to those of sedentary women is not readily apparent, and for this reason, the remainder of the paper discusses energy balance as affected by activity. Methodological considerations related to assessment of the components of the energy balance equation (food intake, energy expenditure, and body energy stores) are presented, with a focus on considerations in women. The effects of activity on each of these components are then discussed in an attempt to determine whether some form of energy conservation may occur. Finally, effects of activity on the menstrual cycle are reviewed. The observed changes are discussed in relation to nutrition 1) in terms of how nutrition may play a role in their causation; and 2) in terms of their nutritional implications for the amenorrheic athlete, specifically as regards energy balance and bone density.  相似文献   
938.
939.
Segregation of reactive metals at the bonding interface has been observed in various ceramic and/or metal joints bonded with reactive metal-bearing braze alloys. When a d.c. of 20 mAcm−2 is applied to the ceramic/braze/ceramic system at a brazing temperature of, say, 1373 K, the electric field assists the segregation at the braze-ceramic interface on the cathode side and suppresses the segregation at the interface on the anode side. This may imply that reactive metal atoms in the braze can migrate as a cation. E.m.f. measurement on the ceramic (AIN or ZrB2)-metal foil systems with increasing temperature shows that a negative e.m.f. to the ceramic pole appears from about 900 K for AIN and from 500 K for ZrB2, as does the thermally stimulated current in polymers. These temperatures coincide well with those where the electrical conductivity of AIN and ZrB2, respectively, begins to increase with increasing temperature. Therefore, it is considered that the polarization of the ceramics may take place and assist the migration, and consequently segregation, of reactive metals in braze alloys to the braze-ceramic interface during brazing.  相似文献   
940.
An investigation of the effect of reaction conditions on product distribution in the skeletal isomerisation reaction of linear butenes has been carried out. The main reaction routes over ferrierite have been identified. Beside the main product isobutene, major by-product formation occurs. The unwanted reactions include dimerisation of butene to form octenes, hydrogen transfer yielding small amounts of saturated C3 and C4 hydrocarbons and disproportionation producing propene and pentenes. The most abundant by-products were pentene and propene, though these were not formed in equimolar amounts as could be expected. Oligomerisation experiments of propene over ferrierite produced large amounts of butene and pentene, revealing the presence of adsorbed nonene. The cracking of this surface species to hexene and propene is the most likely reaction route for the excess propene formation. This additional path to propene formation operates mainly at temperatures above 623 K.  相似文献   
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