CO毒化AB5型合金分形特征研究

研究了三种贮氢合金 L a Ni5、L a Ni4 .7Al0 .3、Ml Ni4 .5Al0 .5被 10 0× 10 - 6 CO毒化后的分形特征 ,求出这三种合金在含 10 0× 10 - 6 CO的氢中循环 ,分维分别为 0 .2 5 4 7、0 .170 9、0 .0 72 5。可以较好的解释合金被毒化的宏观现象。     

钢轨试验方法的研究

结合即将颁布的新国家标准GB2585<铁路用热轧钢轨>和国家标准TB/T2344-2003<43 Kg/m-75 Kg/m热轧钢轨订货技术条件>,通过对武钢生产的U71Mn重轨进行拉伸性能、布氏硬度、脱碳层分布情况、非金属夹杂物以及显微组织等试验方法的研究,分析了U71Mn重轨在新旧标准要求下的质量水平,为改善U71Mn的质量、符合新标准提供了重要的检验理论依据.     

Microfabricated preconcentrator-focuser for a microscale gas chromatograph

The design, fabrication, and testing of a preconcentrator-focuser (PCF), consisting of a thick micromachined Si heater packed with a small quantity of a granular adsorbent material are described. The PCF is developed to capture and concentrate vapors for subsequent focused thermal desorption and analysis in a micro gas chromatograph. The microheater contains an array of high-aspect-ratio, etched-Si heating elements, 520 /spl mu/m (h)/spl times/50 /spl mu/m (w)/spl times/3000 /spl mu/m (l), bounded by an annulus of Si and thermally isolated from the remaining substrate by an air gap. This structure is sandwiched between Pyrex glass plates with inlet/outlet ports that accept capillary tubes for sample flow and is sealed by anodic bonding (bottom) and rapidly annealed glass/metal/Si solder bonding (top). The large microheater surface area allows for high adsorption capacity and efficient, uniform thermal desorption of vapors captured on the adsorbent within the structure. The adsorbent consists of roughly spherical granules, /spl sim/200 /spl mu/m in diameter, of a high-surface-area, graphitized carbon. Key design considerations, fabrication technologies, and results of performance tests are presented with an emphasis on the thermal desorption characteristics of several representative volatile organic compounds as a function of volumetric flow rates and heating rates. Preconcentration factors as high as 5600 and desorbed peak widths as narrow as 0.8 s are achieved from 0.25-L samples of benzene at modest heating rates. The effects of operating variables on sensitivity, chromatographic resolution, and detection limits are assessed. Testing of this PCF with a micromachined separation column and integrated sensor array is discussed briefly.     

Facile synthesis of ordered nanocrystalline alumina thin films with tunable mesopore structures

Mesoporous alumina layers have attracted attention for their potential use in ultrafiltration of salts, as a heterogeneous catalyst support, an adsorbent in environmental cleanup, and in petroleum refinement. The ability to control the fast hydrolysis rate of the inorganic precursors using simple and inexpensive routes is important for that potential to be realized. Herein, we introduce a novel and facile route to synthesize mesoporous alumina thin films from the combination of inexpensive and commercially available copolymer with aluminum chloride or nitrate (salts) in an EtOH–surfactant–NH₃ · H₂O–salts (EsNs) system through the evaporation-induced self-assembly (EISA) method. Mesoporous alumina layers obtained utilizing the EsNs system have ordered and tunable pore structures. The ability to easily control the mesophases of the alumina layers within a short time provides distinct advantages over previously reported synthesis procedures. Most importantly, we demonstrate that the binding of surfactant and NH₃ · H₂O for the formation of hydrogen bond between them in the EsNs system controls the fast hydrolysis rate of the inorganic species. This allows for the synthesis of nanocrystalline alumina layers via the aluminum oxo-clusters’ assembly with the surfactant. Such simple route may be applied in the synthesis of other non-silica mesostructured oxides.     

浅析当今写意青花的题材选择

青花装饰是景德镇的传统装饰方法之一，其中的写意青花又以其简约萧疏的艺术特征获得了人们的普遍喜爱。针对时代的变化影响，研究了当今写意青花在题材选择上与传统写意青花的差异。     

龙滩水电站尾水调压井桥机拆除

龙滩水电站尾水调压井施工桥机在完成其施工吊装使命后需要拆除，为保证其完好率，需采取无破坏法整机拆除。介绍了在狭小空间大型设备的整机拆除方法和天锚系统的设计、布局。     

基于ANSYS的铸嘴流体耦合场三维有限元仿真分析

作者用大型有限元分析软件ANSYS对铸嘴内稳态层流铝熔体进行仿真分析。实现了三维建模。解决了三维热一流耦合求解的问题，得到铝流体的速度、压力及温度的分布图。分析了铸嘴出口速度和温度的分布规律及其对连续铸轧的影响。     

六通道瞬态光学高温计

六通道瞬态光学高温计是在可见光和近红外光谱范围内 ,把光源的热辐射取出六个波段进行测量。每个波段信号通过各自的光纤传输、光电倍增管探测和记录仪器记录。系统的时间分辨率小于 30 ns,冲击温度测量范围为 2 30 0～ 90 0 0 K,测量误差小于 5 % ,给出了以碘化钠、硝基甲烷和空气为样品的若干实验结果     

与性能相关的容错计算系统可靠性指标

对于某些容错计算系统，由于成功与故障之间没有明确的界限，用传统的可靠性指标难以准确地评价其容错性能，为此一些学者提出了若干与性能相关的可靠性指标。本文将这些指标概括成三类（即基于瞬时性能的指标、基于累积收益的指标和率模可靠性指标）加以介绍，并简要介绍了它们的求解方法。