Facile synthesis of ordered nanocrystalline alumina thin films with tunable mesopore structures

Mesoporous alumina layers have attracted attention for their potential use in ultrafiltration of salts, as a heterogeneous catalyst support, an adsorbent in environmental cleanup, and in petroleum refinement. The ability to control the fast hydrolysis rate of the inorganic precursors using simple and inexpensive routes is important for that potential to be realized. Herein, we introduce a novel and facile route to synthesize mesoporous alumina thin films from the combination of inexpensive and commercially available copolymer with aluminum chloride or nitrate (salts) in an EtOH–surfactant–NH₃ · H₂O–salts (EsNs) system through the evaporation-induced self-assembly (EISA) method. Mesoporous alumina layers obtained utilizing the EsNs system have ordered and tunable pore structures. The ability to easily control the mesophases of the alumina layers within a short time provides distinct advantages over previously reported synthesis procedures. Most importantly, we demonstrate that the binding of surfactant and NH₃ · H₂O for the formation of hydrogen bond between them in the EsNs system controls the fast hydrolysis rate of the inorganic species. This allows for the synthesis of nanocrystalline alumina layers via the aluminum oxo-clusters’ assembly with the surfactant. Such simple route may be applied in the synthesis of other non-silica mesostructured oxides.     

浅析当今写意青花的题材选择

青花装饰是景德镇的传统装饰方法之一，其中的写意青花又以其简约萧疏的艺术特征获得了人们的普遍喜爱。针对时代的变化影响，研究了当今写意青花在题材选择上与传统写意青花的差异。     

郑411块超稠油试油试采工艺技术应用

郑411块沙三段地层疏松出砂、原油粘度高，属中深层超稠油，常规试油试采方法难以突破出油关，采用APR全通径氮气垫测试、地层与井筒复合防砂、水平井配合直井蒸汽吞吐、氮气泡沫封堵调剖和井筒加热举升稠油等配套工艺技术，取得了较好的效果，为中深层超稠油油藏的开发提供了技术思路。     

Study on a Distributed Wavelength Routing Algorithm in WDM Optical Transport Networks

A new design scheme for a distributed algorithm for routing and wavelength assignment (RWA) is developed in this paper, and the communication rules between the nodes to exchange signaling packets are discussed. The Adaptive-Alternate-Routing-Least-Load (AARLL) algorithm is implemented in the distributed scheme for the first time. Under dynamic traffic circumstances, the influence of the race condition, which does not exist in centralized scheme, on the network performance is analyzed and the analyzed results show that the race condition has a major impact on network performance only under light traffic load, while under medium and heavy traffic load the impact is very small. To analyze the performance loss caused by adopting the distributed algorithm for RWA, the capacity loss factor (CLF) is introduced and the calculated results show that CLF does not exceed 6% under medium traffic load.     

分步重复投影光刻机整机控制管理软件

计算机分系统是光刻机整机控制和管理的中枢，直接反映和影响整机的性能和介绍了计算机硬件接口控制原理，描述了分步重复投影光刻机系统软件的主要设计思想和软件的主要功能。     

六通道瞬态光学高温计

六通道瞬态光学高温计是在可见光和近红外光谱范围内 ,把光源的热辐射取出六个波段进行测量。每个波段信号通过各自的光纤传输、光电倍增管探测和记录仪器记录。系统的时间分辨率小于 30 ns,冲击温度测量范围为 2 30 0～ 90 0 0 K,测量误差小于 5 % ,给出了以碘化钠、硝基甲烷和空气为样品的若干实验结果     

岩石爆破中爆炸能量分布理论与控制方法研究进展

文中对岩石爆破过程中爆炸能量分布理论与控制方法的发展现状进行了综述，分析了爆炸能量分布理论与控制方法有待进一步研究的问题，并指出了该课题的研究具有重要的理论和实践意义。     

用热分析法研究硝化棉的熔化过程

用ＭＤＳＣ，显微镜温台熔点测定仪和固体原位反应池／快速扫描傅立叶变换红外光谱联用装置考察了硝化棉的熔化过程。ＭＤＳＣ曲线表明吸热过程是可逆的，它系由ＮＣ和部分分解凝聚相产物的混合物的固液相变所引起。由ＮＣ的ＭＤＳＣ曲线得到的熔点，熔化含，熔化熵，分解含和分解反应热温熵分别为４７６．８４Ｋ，２０５．６Ｊ．ｇ＾－１，０．４３１２Ｊ．ｇ＾－１．Ｋ＾－１，－２４７５．０Ｊ．ｇ＾－１，－５．２４２Ｊ．ｇ＾－     

与性能相关的容错计算系统可靠性指标

对于某些容错计算系统，由于成功与故障之间没有明确的界限，用传统的可靠性指标难以准确地评价其容错性能，为此一些学者提出了若干与性能相关的可靠性指标。本文将这些指标概括成三类（即基于瞬时性能的指标、基于累积收益的指标和率模可靠性指标）加以介绍，并简要介绍了它们的求解方法。     

厚膜导体的金属迁移研究

金属迁移能导致混合微电路发生灾难性失效。本文介绍一种简单易行的测试方法－水滴试验法，来测量厚膜电路的实际金属迁移率。用引方法测量时，发现Ｐｄ－Ａｇ导体的迁移率最大，Ｐｔ－Ａｕ导体的金属迁移率最小。