Spectrophotometric determination of some antioxidants with potassium permanganate and metol

New spectrophotometric methods for the assay of some antioxidants have been developed using potassium permanganate and metol (p-N-methyl amino phenol). Metol is oxidised at pH 3.0 with potassium permanganate and coupled with antioxidants to give λ_max at 560 nm for propyl gallate and gallic acid and 510nm for butylated hydroxy anisole. The method is simple, sensitive, reproducible and accurate within ±1% and applicable to the assay of antioxidants (gallic acid, propyl gallate and butylated hydroxy anisole) in oils and fats.     

Flood risk mapping at European scale.

The aim of this article is to illustrate a framework for flood risk mapping at pan-European scale produced by the Weather-Driven Natural Hazards (WDNH) action of the EC-JRC-IES. Early results are presented in the form of flood risk index maps. We assess several flood risk factors that contribute to the occurrence of flood disasters. Among the causal factors of a flood disaster one is triggering a natural event in the form of extreme precipitation and consequently extreme river discharge and extreme flood water levels. The threatening natural event represents the hazard component in our assessment. Furthermore exposure and vulnerability are anthropogenic factors that contribute also to flood risk. In the proposed approach, flood risk is considered on the light of exposure, vulnerability and hazard. We use a methodology with a marked territorial approach for the assessment of the flood risk. Hence, based on mathematical calculations, risk is the product of hazard, exposure and vulnerability. Improvements on datasets availability and spatial scale are foreseen in the next phases of this study. This study is also a contribution to the discussion about the need for communication tools between the natural hazard scientific community and the political and decision making players in this field.     

Deconvolution of infrared spectra using various milk proteins as an example

The theory of deconvolution of infra-red spectra is presented and illustrated using milk protein spectra. The advantage of this method is impressively demonstrated and its relevance for dairy farming shown using a simple example, the cooling of milk.     

Longitudinal analysis of semiconductor lasers with low reflectivity facets

An analysis is made of longitudinal effects in semiconductor lasers with low facet reflectivities. For this purpose, a self-consistent model is used based on the beam propagation method, which takes into account both the lateral and longitudinal dimension. The calculations show that longitudinal effects have a significant influence on the output fields in the laser.     

The heater test at the Grimsel Rock Laboratory: The thermo-mechanical response of the rock mass to a heat flux

The Grimsel Test Site (Felslabor Grimsel — FLG) is situated at a depth of 450 m in the Juchlistock massif of the Bernese Oberland. It is managed by the National Cooperative for the Storage of Radioactive Waste (NAGRA-Switzerland).By means of a heater test, the power output of canisters filled with high-level waste is simulated. This heater test is performed by the German Gesellschaft für Strahlen- und Umweltforschung — GSF. Two electrical heaters, with a heatable length of 6 m, a diameter of 0.3 m and an available power of 4 kW/m, are installed in two vertical boreholes. One of them is located in the granite adjacent to a strongly fractured lamprophyre vein, the other one directly within this disturbed zone. They are operating since August 1986.The thermo-mechanical reaction of the rock mass is registered by a large number of measurement devices which are installed in an array of instrument boreholes around the heaters. They record the deformation and the alteration of rock stresses, the pore water pressure and the water conductivity caused by heating.     

Operation of an experimental facility for fabrication of fuel elements and fuel assemblies of the bor-60 containing vibrocompacted fuel

Translated from Atomnaya Énergiya, Vol. 67, No. 5, pp. 320–323, November, 1989.     

Adjuvant arthritis: influence of the adjuvant volume and composition on the non-specific inflammation

Adjuvant-induced arthritis is an animal model of chronic inflammatory disease widely used in anti-inflammatory and immunosuppressive drugs testing. When the development and the inhibition of the induced arthritis are measured by the injected paw oedema, it is difficult to delineate the immunological contribution from the persistent non-specific primary section. To study the influence of volume and composition of the injected adjuvant upon the primary non-specific inflammation, we devised a 3X4 factorial experiment on a strain of inbred rats with a low susceptibility to adjuvant-induced arthritis. The injection of mineral oil alone produces a persistent oedema. The injection of mycobacteriae in suspension in saline induces a rapid inflammatory response followed by a fast decrease of the oedema. When complete adjuvant is used, there is always a very strong interaction between the effects of the two components of the adjuvant, i.e. the measured oedemas are much greater than the calculated values, For a given injected volume, the inflammation is maximum when the concentration of mycobacteriae is 2.5 mg/ml. All the rats injected with complete adjuvant present a transient oedema of the non-injected hind paw. This oedema is very small and proportional to the amount of mycobacteria injected.     

Can heat pipes solve the problems of drift and vibration of cryoholders?

Drift and vibration are the main factors limiting the resolution that can be attained with liquid-nitrogen (LN₂)-cooled cryoholders. Tests with a Gatan holder show that resolution is usually anisotropic. We propose that the metallic heat-conducting element could be replaced by a heat pipe, because such a device can, in principle, minimize drift. The vibration problem could be combatted by using supercooled cryogens.