Electron spectroscopies and their use for materials characterization

We present here a general overview of electron spectroscopies from a practical point of view. The most frequently used ones are described and the type of structural information they can provide on materials is explained in relation to the physical processes on which they are based. Furthermore, we explore critically and in detail various tools that have been developed to allow a systematic solving of structures by these spectroscopies.     

Piezoelectric Nanogenerators for Self-Powered Nanodevices

A novel approach converts nanoscale mechanical energy into electric energy for self-powering nanodevices.In our own work, we've used piezoelectric zinc-oxide nanowire (ZnO NW) arrays to demonstrate a novel approach for converting nanoscale mechanical energy into electric energy. Here, we review the fundamental principle behind the nanogenerator, present an approach for improving its performance, and discuss some of the challenges we face in pushing this technology to reach its potential.     

Syntheses and Structural Characterization of Triorganotin Derivatives of Bis(carboxymethyl)trithiocarbonate: X-ray Crystal Structures of 2D Network Polymers

Six triorganotin(IV) complexes of the type {(R₃Sn)₂[C₃S₃(COO)₂]}_n (R = C₆H₅ 1; n-Bu 2; PhCH₂ 4; p-F-PhCH₂ 5; o-F-PhCH₂ 6) and {(R₃Sn)₂[C₃S₃(COO)₂]}_n·[EtOH] (R = Me 3) have been synthesized by the reaction of bis(carboxymethyl)trithiocarbonate with triorganotin(IV) chloride in the presence of sodium ethoxide. All complexes were characterized by elemental analysis IR, ¹H, ¹³C and ¹¹⁹Sn NMR spectroscopy. Except for 4–6, all complexes were also characterized by X-ray crystallography. The X-ray date revealed that complexes 1–3 show two-dimensional network polymeric structure in which the geometries of tin atoms are trigonal bipyramid with the axial positions occupied by carboxylic oxygen atoms.     

含-NCO双组分水性木器漆的应用研究

介绍了以-NCO交联的双组分水性木器漆常用的树脂、固化剂类型，对其在木器涂装过程中的施工时限、泡沫控制等影响生产应用的因素进行了分析研究，并提出了一些解决方案。     

火焰原子吸收光谱法测量污水中锑量的测量不确定度评定

通过火焰原子吸收光谱法对水中的锑量进行了测定,对影响测量结果的不确定度分量进行了量化的计算,从而得出影响锑量测量不确定的主要因素是测量样品消解液中的锑的质量浓度引起的不确定度.     

高职高专现代教育技术管理体制之我见

本文从教育技术的含义和发展的历史出发，分析目前高职高专院校的教育技术管理体制现状，提出应建立完善的教育技术管理体制，以推进教育技术工作的协调发展。     

Enclosing all solutions of two-point boundary value problems for ODEs

The two-point boundary value problem (TPBVP) occurs in a wide variety of problems in engineering and science, including the modeling of chemical reactions, heat transfer, and diffusion, and the solution of optimal control problems. A TPBVP may have no solution, a single solution, or multiple solutions. A new strategy is presented for reliably locating all solutions of a TPBVP. The method determines narrow enclosures of all solutions that occur within a specified search interval. Key features of the method are the use of a new solver for parametric ODEs, which is used to produce guaranteed bounds on the solutions of nonlinear dynamic systems with interval-valued parameters and initial states, and the use of a constraint propagation strategy on the Taylor models used to represent the solutions of the dynamic system. Numerical experiments demonstrate the use and computational efficiency of the method.